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1. 发明授权

US07452195B2 Apparatus for preparation of aqueous emulsion from curable silicone composition and suspension of cured silicone particles 失效
标题翻译：用于由可固化硅氧烷组合物制备水性乳液的装置和固化的硅氧烷颗粒的悬浮液
公开(公告)号：US07452195B2
公开(公告)日：2008-11-18
申请号：US11680934
申请日：2007-03-01
申请人： Kazuhiko Ando , Keiji Yoshida , Toyohiko Yamadera , Yoshitsugu Morita , Mitsuo Hamada
发明人： Kazuhiko Ando , Keiji Yoshida , Toyohiko Yamadera , Yoshitsugu Morita , Mitsuo Hamada
IPC分类号： B29B9/06
CPC分类号： B01F3/0807 , B01F5/061 , B01F5/0682 , B01F5/0688 , B01F7/00758 , B01F13/103 , C08J3/03 , C08J2383/04
摘要： Method for preparation of an aqueous emulsion from a curable silicone composition consisting of (A) an organopolysiloxane having at least two silicon-bonded hydroxyl groups, (B) an organohydrogensiloxane, and (C) a curing catalyst, said method being characterized by (i) continuously supplying component (A), component (B) and component (C), or a mixture of components (A) and (B) and component (C) through individual inlet ports into a continuous mixer and mixing said components at a temperature not exceeding 10° C., (ii) continuously supplying the obtained mixture and (D) an aqueous solution of a surface-active agent to an emulsifier, and emulsifying the components at a temperature not exceeding 20° C. An apparatus for the preparation of an aqueous emulsion of a curable silicone composition comprising of a continuous mixer for mixing components (A) through (C), a distribution unit connected to the lower part of the mixer, and an emulsifier. Method for preparation of a suspension of cured silicone particles by allowing such emulsion to stand at room temperature, or heating the aforementioned emulsion.
摘要翻译：由（A）具有至少两个与硅键合的羟基的有机聚硅氧烷，（B）有机氢硅氧烷和（C）固化催化剂）组成的可固化有机硅组合物制备水乳液的方法，所述方法的特征在于（i ）将组分（A），组分（B）和组分（C）或组分（A）和组分（B）和组分（C）的混合物通过各个入口端连续供给到连续混合器中，并在所述组分不超过10℃，（ii）将所得混合物和（D）表面活性剂的水溶液连续供给到乳化剂中，并在不超过20℃的温度下乳化该组分。的可固化硅氧烷组合物的水性乳液，其包含用于混合组分（A）至（C）的连续混合器，与混合器的下部连接的分配单元和乳化剂。通过使这种乳液在室温下放置或加热上述乳液来制备固化的硅氧烷颗粒的悬浮液的方法。

2. 发明申请

US20070155893A1 Method For Preparation Of Aqueous Emulsion From Curable Silicone Composition And Suspension Of Cured Silicone Particles, And Apparatus Therefor 失效
标题翻译：由固化硅酮组合物和固化硅氧烷颗粒悬浮液制备水性乳液的方法及其设备
公开(公告)号：US20070155893A1
公开(公告)日：2007-07-05
申请号：US11680934
申请日：2007-03-01
申请人： Kazuhiko Ando , Keiji Yoshida , Toyohiko Yamadera , Yoshitsugu Morita , Mitsuo Hamada
发明人： Kazuhiko Ando , Keiji Yoshida , Toyohiko Yamadera , Yoshitsugu Morita , Mitsuo Hamada
IPC分类号： C08L83/00
CPC分类号： B01F3/0807 , B01F5/061 , B01F5/0682 , B01F5/0688 , B01F7/00758 , B01F13/103 , C08J3/03 , C08J2383/04
摘要： Method for preparation of an aqueous emulsion from a curable silicone composition consisting of (A) an organopolysiloxane having at least two silicon-bonded hydroxyl groups, (B) an organohydrogensiloxane, and (C) a curing catalyst, said method being characterized by (i) continuously supplying component (A), component (B) and component (C), or a mixture of components (A) and (B) and component (C) through individual inlet ports into a continuous mixer and mixing said components at a temperature not exceeding 10° C., (ii) continuously supplying the obtained mixture and (D) an aqueous solution of a surface-active agent to an emulsifier, and emulsifying the components at a temperature not exceeding 20° C. An apparatus for the preparation of an aqueous emulsion of a curable silicone composition comprising of a continuous mixer for mixing components (A) through (C), a distribution unit connected to the lower part of the mixer, and an emulsifier. Method for preparation of a suspension of cured silicone particles by allowing such emulsion to stand at room temperature, or heating the aforementioned emulsion.
摘要翻译：由（A）具有至少两个与硅键合的羟基的有机聚硅氧烷，（B）有机氢硅氧烷和（C）固化催化剂）组成的可固化有机硅组合物制备水乳液的方法，所述方法的特征在于（i ）将组分（A），组分（B）和组分（C）或组分（A）和组分（B）和组分（C）的混合物通过各个入口端连续供给到连续混合器中，并在所述组分不超过10℃，（ii）将所得混合物和（D）表面活性剂的水溶液连续供给到乳化剂中，并在不超过20℃的温度下乳化该组分。的可固化硅氧烷组合物的水性乳液，其包含用于混合组分（A）至（C）的连续混合器，与混合器的下部连接的分配单元和乳化剂。通过使这种乳液在室温下放置或加热上述乳液来制备固化的硅氧烷颗粒的悬浮液的方法。

3. 发明授权

US07202301B2 Method for preparation of aqueous emulsion from curable silicone composition and suspension of cured silicone particles, and apparatus therefor 有权
标题翻译：由可固化硅氧烷组合物制备水性乳液的方法和固化的硅氧烷颗粒的悬浮液及其设备
公开(公告)号：US07202301B2
公开(公告)日：2007-04-10
申请号：US10475451
申请日：2002-04-26
申请人： Kazuhiko Ando , Keiji Yoshida , Toyohiko Yamadera , Yoshitsugu Morita , Mitsuo Hamada
发明人： Kazuhiko Ando , Keiji Yoshida , Toyohiko Yamadera , Yoshitsugu Morita , Mitsuo Hamada
IPC分类号： C08G77/06
CPC分类号： B01F3/0807 , B01F5/061 , B01F5/0682 , B01F5/0688 , B01F7/00758 , B01F13/103 , C08J3/03 , C08J2383/04
摘要： Method for preparation of an aqueous emulsion from a curable silicone composition consisting of (A) an organopolysiloxane having at least two silicon-bonded hydroxyl groups, (B) an organohydrogensiloxane, and (C) a curing catalyst, said method being characterized by (i) continuously supplying component (A), component (B) and component (C), or a mixture of components (A) and (B) and component (C) through individual inlet ports into a continuous mixer and mixing said components at a temperature not exceeding 10° C., (ii) continuously supplying the obtained mixture and (D) an aqueous solution of a surface-active agent to an emulsifier, and emulsifying the components at a temperature not exceeding 20° C. An apparatus for the preparation of an aqueous emulsion of a curable silicone composition comprising of a continuous mixer for mixing components (A) through (C), a distribution unit connected to the lower part of the mixer, and an emulsifier. Method for preparation of a suspension of cured silicone particles by allowing such emulsion to stand at room temperature, or heating the aforementioned emulsion.
摘要翻译：由（A）具有至少两个与硅键合的羟基的有机聚硅氧烷，（B）有机氢硅氧烷和（C）固化催化剂）组成的可固化有机硅组合物制备水乳液的方法，所述方法的特征在于（i ）将组分（A），组分（B）和组分（C）或组分（A）和组分（B）和组分（C）的混合物通过各个入口端连续供给到连续混合器中，并在所述组分不超过10℃，（ii）将所得混合物和（D）表面活性剂的水溶液连续供给到乳化剂中，并在不超过20℃的温度下乳化该组分。的可固化硅氧烷组合物的水性乳液，其包含用于混合组分（A）至（C）的连续混合器，与混合器的下部连接的分配单元和乳化剂。通过使这种乳液在室温下放置或加热上述乳液来制备固化的硅氧烷颗粒的悬浮液的方法。

4. 发明授权

US5973060A Silicone rubber particulate composition and methods for the preparation thereof 失效
公开(公告)号：US5973060A
公开(公告)日：1999-10-26
申请号：US245517
申请日：1999-02-05
申请人： Kouichi Ozaki , Norio Matsuda , Makoto Tanoue , Toyohiko Yamadera , Mitsuo Hamada
发明人： Kouichi Ozaki , Norio Matsuda , Makoto Tanoue , Toyohiko Yamadera , Mitsuo Hamada
IPC分类号： C08J3/12 , C08L83/04 , C08L83/00 , C08J9/28
CPC分类号： C08J3/12 , C08L83/04 , C08G77/12 , C08G77/16 , C08G77/20 , C08J2383/04
摘要： A silicone rubber particulate composition useful as an additive for cosmetics, rubbers, resins and paints is disclosed, said composition comprising:(A) a silicone rubber particulate having an average particle size of 0.1 to 1,000 .mu.m;(B) a water-absorptive resin particulate having a water-free average particle size of 0.1 to 1,000 .mu.m; and(C) water,wherein said component (B) is present at a level of 0.01 to 5 weight percent measured on a water-free basis relative to component (A) and said water is present at a level of 10 to 10,000 weight parts for each 100 weight parts of component (B).

5. 发明授权

US4999131A Method and apparatus for the preparation of a water based dispersion of a viscous liquid 失效
标题翻译：用于制备粘性液体的水基分散体的方法和装置
公开(公告)号：US4999131A
公开(公告)日：1991-03-12
申请号：US307641
申请日：1989-02-07
申请人： Koji Shimizu , Toyohiko Yamadera , Mitsuo Hamada
发明人： Koji Shimizu , Toyohiko Yamadera , Mitsuo Hamada
IPC分类号： C08J3/02 , B01F3/10 , B01F5/04 , B01F15/02 , B01J13/00 , C08L83/04
CPC分类号： B01F7/00758 , B01F13/103 , B01F3/0807 , B01F5/0451 , Y10S516/924
摘要： A method and apparatus is provided for the preparation of liquid dispersions comprising the uniform dispersion of a viscous liquid formed of strands, threads or columns, such as a silicone polymer in water.

6. 发明授权

US06353033B1 Method and apparatus for cutting high viscosity liquid material 失效
标题翻译：切割高粘度液体材料的方法和设备
公开(公告)号：US06353033B1
公开(公告)日：2002-03-05
申请号：US09628468
申请日：2000-07-31
申请人： Koichi Ozaki , Toru Imaizumi , Koichi Ishida , Toyohiko Yamadera , Mitsuo Hamada
发明人： Koichi Ozaki , Toru Imaizumi , Koichi Ishida , Toyohiko Yamadera , Mitsuo Hamada
IPC分类号： B01F1700
CPC分类号： B26F3/00 , F16K1/02 , F17D1/14 , Y10S516/924
摘要： Method and apparatus for cutting high viscosity liquid material, said apparatus comprising a cylinder divided into upper and lower tanks by a partition with a central discharge opening, a moveable and elevatable liquid supply pipe with a distal end positioned opposite the discharge opening, the liquid supply pipe being mounted so that it can be raised until its distal end contacts the partition around the discharge opening, and then lowered until there is no contact, means for raising and lowering the liquid supply pipe, the upper tank having peripheral injection ports for injecting a low viscosity liquid into the upper tank, means for feeding high viscosity liquid material into the lower tank and flowing it into the upper tank, means for feeding low viscosity liquid into the liquid supply pipe and for feeding low viscosity liquid into the peripheral injection ports, the high viscosity liquid material flowing from the lower tank into the upper tank when the liquid supply pipe is lowered, the high viscosity liquid material being pushed upwardly into the upper tank by the low viscosity liquid when the liquid supply pipe is raised, whereby the high viscosity liquid material being pushed upwardly in the upper tank is cut into blocks by the low viscosity liquid being injected into the upper tank.
摘要翻译：用于切割高粘度液体材料的方法和装置，所述装置包括通过具有中心排出口的分隔件分成上部和下部罐的圆筒，具有与排出口相对的远端的可移动和可升高的液体供应管，液体供应管被安装成可以升高直到其远端接触排放口周围的隔板，然后降低直到不接触，用于升高和降低液体供给管的装置，上部罐具有用于注入的周边注入口低粘度液体进入上部罐，用于将高粘度液体材料进入下部罐并将其流入上部罐的装置，用于将低粘度液体供给到液体供给管中并将低粘度液体供给到外部喷射口中的装置，当液体供应管较低时，高粘度液体材料从下槽流入上罐 d，当液体供应管升高时，高粘度液体材料被低粘度液体向上推入上罐，由此通过低粘度液体将在上槽中向上推的高粘度液体材料切成块注入上水箱。

7. 发明授权

US6117933A Silicone rubber particulate composition and methods for the preparation thereof 失效
标题翻译：硅橡胶颗粒组合物及其制备方法
公开(公告)号：US6117933A
公开(公告)日：2000-09-12
申请号：US337570
申请日：1999-06-22
申请人： Kouichi Ozaki , Norio Matsuda , Makoto Tanoue , Toyohiko Yamadera , Mitsuo Hamada
发明人： Kouichi Ozaki , Norio Matsuda , Makoto Tanoue , Toyohiko Yamadera , Mitsuo Hamada
IPC分类号： C08J3/12 , C08L83/04 , C08K5/09
CPC分类号： C08J3/12 , C08L83/04 , C08G77/12 , C08G77/16 , C08G77/20 , C08J2383/04
摘要： A silicone rubber particulate composition useful as an additive for cosmetics, rubbers, resins and paints is disclosed, said composition comprising:(A) a silicone rubber particulate having an average particle size of 0.1 to 1,000 .mu.m;(B) a water-absorptive resin particulate having a water-free average particle size of 0.1 to 1,000 .mu.m; and(C) water,wherein said component (B) is present at a level of 0.01 to 5 weight percent measured on a water-free basis relative to component (A) and said water is present at a level of 10 to 10,000 weight parts for each 100 weight parts of component (B).
摘要翻译：公开了一种可用作化妆品，橡胶，树脂和油漆的添加剂的硅橡胶颗粒组合物，所述组合物包含：（A）平均粒度为0.1-1000μm的硅橡胶颗粒; （B）无水平均粒径为0.1〜1000μm的吸水性树脂粒子; 和（C）水，其中所述组分（B）以相对于组分（A）在无水基础下测量的0.01至5重量％的水平存在，并且所述水以10至10,000重量份的量存在对于每100重量份组分（B）。

8. 发明授权

US06435707B1 Continuous mixing apparatus with upper and lower bladed disk impellers and a notched blade 失效
标题翻译：连续混合装置具有上下叶片式叶轮和缺口叶片
公开(公告)号：US06435707B1
公开(公告)日：2002-08-20
申请号：US09993594
申请日：2001-11-05
申请人： Hideyuki Mori , Toyohiko Yamadera , Mitsuo Hamada
发明人： Hideyuki Mori , Toyohiko Yamadera , Mitsuo Hamada
IPC分类号： B01F726
CPC分类号： B01F5/223 , B01F3/08 , B01F7/166 , B01F2003/125
摘要： Continuous mixing apparatus provide rapid production of a mixture of high uniformity, low viscosity, low density, high stability after mixing, without an increase in amounts of subsequently supplied liquids. Continuous production of liquid or liquid containing mixtures consists of (i) continuously loading the apparatus casing with materials of different types which are flowable such as different liquids or a powder and a liquid, (ii) mixing the components between independently rotating upper and lower bladed disk turbine impellers to form a coarse mixture, and (iii) mixing the coarse mixture with an additional portion of a liquid being continuously supplied to the casing. The apparatus includes upper and lower bladed disk turbine impellers disposed in a mixing chamber within a casing. The impellers are capable of being rotated independently at different rotational speeds. A plurality of blades are attached to the impellers. Upper and lower ring shaped baffles extend from the inner wall of the casing. A material loading opening is provided in the upper part of the casing and a liquid supply pipe extends through a side wall of the casing. A discharge opening in the bottom of the mixing chamber unloads the mixture.
摘要翻译：连续混合装置可以快速生产高均匀性，低粘度，低密度，混合后高稳定性的混合物，而不增加随后供应的液体的量。连续生产含液体或液体的混合物包括：（i）将设备外壳连续地装载不同类型的材料，如不同液体或粉末和液体，（ii）将独立旋转的上下叶片盘式涡轮叶轮形成粗混合物，和（iii）将粗混合物与另外部分液体混合，将其连续地供给至壳体。该装置包括设置在壳体内的混合室中的上叶片和下叶片的圆盘涡轮叶轮。叶轮能够以不同的转速独立旋转。多个叶片连接到叶轮。上下环形挡板从外壳的内壁延伸。在壳体的上部设置有材料装载口，液体供给管延伸穿过壳体的侧壁。混合室底部的排放口卸载混合物。

9. 发明授权

US06218466B1 Method for the continuous preparation of liquid silicone rubber base 失效
标题翻译：连续制备液体硅橡胶基料的方法
公开(公告)号：US06218466B1
公开(公告)日：2001-04-17
申请号：US09383433
申请日：1999-08-27
申请人： Mitsuo Hamada , Koich Ishida , Atsushi Komatsu , Hidetoshi Kurusu , Hideyuki Mori , Toyohiko Yamadera
发明人： Mitsuo Hamada , Koich Ishida , Atsushi Komatsu , Hidetoshi Kurusu , Hideyuki Mori , Toyohiko Yamadera
IPC分类号： C08K336
CPC分类号： C08J3/203 , B01F7/00208 , B01F7/00775 , B01F2215/0481 , B01F2215/0495 , B29B7/402 , B29B7/7495 , B29B7/90 , C08G77/12 , C08G77/20 , C08J2383/04 , C08L83/04 , C08L83/00
摘要： A method is provided that can very rapidly produce a liquid silicone rubber base in which even microfine electrically conductive filler with specific surface of at least 0.5 m2/g will be homogeneously dispersed in liquid organopolysiloxane without small lump or clump formation. The method for the continuous preparation of liquid silicone rubber base, including the steps of continuously supplying to a continuous mixing apparatus (A) 100 weight parts polyorganosiloxane that has a viscosity at 25° C. of 100 to 500,000 mPa·s comprising at least 2 silicon-bonded alkenyl groups in each molecule, (B) 0 to 200 weight parts electrically nonconductive inorganic filler, and (C) 0.1 to 700 weight parts electrically conductive filler with a specific surface of at least 0.5 m2/g wherein the combined quantity of components (B) and (C) is from 5 to 700 weight parts where the continuous mixing apparatus has a cylindrical body casing with a material feed opening at the top of the body casing, a mixture discharge outlet at the bottom of the body casing, and a rotating disk within the casing such that the ratio of the diameter of the rotating disk to the inside diameter of the cylindrical body casing is 0.80 to 0.95; mixing components (A) through (C) therein by the rotation of the rotating disk to form a mixture; and discharging the mixture through the said discharge outlet.
摘要翻译：提供了一种能够非常快速地制备液体硅橡胶基质的方法，其中甚至具有至少0.5m 2 / g的比表面积的极细导电填料将均匀分散在液体有机聚硅氧烷中，而没有小块或块形成。连续的方法液体硅橡胶基料的制备，包括连续混合装置（A）的连续混合装置（A）的步骤，100重量份在25℃下的粘度为100至500,000mPa.s的聚有机硅氧烷，其包含至少2个硅键合的烯基每个分子，（B）0-200重量份非导电无机填料，和（C）0.1-700重量份比表面积至少为0.5m 2 / g的导电填料，其中组分（B）和（C ）为5〜700重量份，其中连续混合装置具有在主体壳体的顶部具有材料供给口的圆筒体壳体，排出的混合物壳体底部的弧形出口和壳体内的旋转盘，使得旋转盘的直径与筒体的内径的比率为0.80〜0.95;混合成分（A）〜（C ）通过旋转盘的旋转而形成混合物; 并通过所述排出口对混合物进行放电。

10. 发明授权

US5945043A Hollow silicone resin particles and method for the preparation thereof 失效
标题翻译：中空硅树脂颗粒及其制备方法
公开(公告)号：US5945043A
公开(公告)日：1999-08-31
申请号：US892489
申请日：1997-07-14
申请人： Mitsuo Hamada , Koichi Ozaki , Toyohiko Yamadera
发明人： Mitsuo Hamada , Koichi Ozaki , Toyohiko Yamadera
IPC分类号： B01J2/04 , B01J13/04 , C08G77/04 , B29B9/12
CPC分类号： B01J13/043 , Y10T428/1372 , Y10T428/1386 , Y10T428/1397 , Y10T428/2982 , Y10T428/2985
摘要： Novel hollow silicone resin particles, having an average particle size of 0.1 to 100 .mu.m are disclosed. The silicone resin particles comprise a skin formed from thermoplastic silicone resin configured in the shape of a hollow capsule. The hollow thermoplastic silicone resin particles are prepared by spraying a dispersion of water and thermoplastic silicone resin dissolved in solvent into hot gas. The hot gas evaporates the solvent and water and at the same time causes solidification of the thermoplastic silicone resin while it is in the spray state, so as to form a plurality of hollow particles therefrom.
摘要翻译：公开了平均粒径为0.1〜100μm的新型中空硅树脂颗粒。有机硅树脂颗粒包括由中空胶囊形状的热塑性硅树脂形成的皮肤。中空热塑性有机硅树脂颗粒通过将溶解在溶剂中的水和热塑性有机硅树脂的分散体喷雾到热气中来制备。热气体蒸发溶剂和水，同时在热塑性硅树脂处于喷射状态时使其固化，从而形成多个中空颗粒。

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