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1. 发明授权

US08741252B2 Process for producing porous object and apparatus therefor 有权
标题翻译：生产多孔物体的方法及其设备
公开(公告)号：US08741252B2
公开(公告)日：2014-06-03
申请号：US11547472
申请日：2005-04-25
申请人： Katsumi Watanabe , Masahiro Yamagata
发明人： Katsumi Watanabe , Masahiro Yamagata
IPC分类号： C01B33/12 , H01M8/06
CPC分类号： C01B33/1585
摘要： Disclosed is a process for producing porous materials by replacing a first solvent in a wet material containing the first solvent with a second solvent in a high pressure condition and drying the resulting wet material which process comprises a mixed solvent feeding step for feeding a mixed solvent composed of a solvent identical to or of the same kind as the first solvent and the second solvent to the wet material.
摘要翻译：公开了一种多孔材料的制造方法，其特征在于，在高压条件下用第二溶剂置换含有第一溶剂的湿物质中的第一溶剂，干燥所得到的湿物质，该方法包括：混合溶剂供给步骤，与第一溶剂和第二溶剂相同或相同类型的溶剂加到湿材料中。

2. 发明授权

US08573962B2 High-pressure treatment apparatus 有权
标题翻译：高压处理设备
公开(公告)号：US08573962B2
公开(公告)日：2013-11-05
申请号：US12988680
申请日：2009-06-05
申请人： Masahiro Yamagata , Katsumi Watanabe
发明人： Masahiro Yamagata , Katsumi Watanabe
IPC分类号： B29C43/10 , B22F3/15
CPC分类号： B01J3/03 , B01J3/008 , B01J3/04 , B01J2219/00094 , B01J2219/00162 , B08B7/0021 , B30B11/002 , F27B17/0016 , Y10T29/49805
摘要： The objective is to provide a high-pressure treatment apparatus with which the pressure or temperature in a treatment chamber can be efficiently adjusted in a short period of time without an overall significant increase in the size or complication of the apparatus. The high-pressure treatment apparatus has a pressure-resistant container having pressure-resistant walls surrounding a treatment chamber, a lid member that closes an open end of the pressure-resistant container, a supply means that supplies a process fluid into the treatment chamber, a partition wall that is thinner than the pressure-resistant wall and is provided along the inside surface of said pressure-resistant container to form a partitioned chamber with said inside surface, and a heat transfer control means. Said heat transfer control means controls heat transfer between said treatment chamber and said partitioned chamber by heating or cooling a heating medium outside the container and feeding said heating medium into said partitioned chamber.
摘要翻译：目的是提供一种高压处理设备，其中可以在短时间内有效地调节处理室中的压力或温度，而不会显着增加设备的尺寸或复杂性。高压处理装置具有耐压性容器，该耐压容器具有围绕处理室的耐压壁，封闭耐压容器的开口端的盖构件，将处理流体供给到处理室的供给单元，分隔壁比所述耐压壁更薄，并且沿着所述耐压容器的内表面设置以形成具有所述内表面的分隔室，以及传热控制装置。所述传热控制装置通过加热或冷却容器外部的加热介质并将所述加热介质供入所述分隔室来控制所述处理室和所述分隔室之间的热传递。

3. 发明申请

US20110030186A1 HIGH-PRESSURE TREATMENT APPARATUS 有权
标题翻译：高压处理设备
公开(公告)号：US20110030186A1
公开(公告)日：2011-02-10
申请号：US12988680
申请日：2009-06-05
申请人： Masahiro Yamagata , Katsumi Watanabe
发明人： Masahiro Yamagata , Katsumi Watanabe
IPC分类号： B23P17/00
CPC分类号： B01J3/03 , B01J3/008 , B01J3/04 , B01J2219/00094 , B01J2219/00162 , B08B7/0021 , B30B11/002 , F27B17/0016 , Y10T29/49805
摘要： The objective is to provide a high-pressure treatment apparatus with which the pressure or temperature in a treatment chamber can be efficiently adjusted in a short period of time without an overall significant increase in the size or complication of the apparatus. The high-pressure treatment apparatus has a pressure-resistant container having pressure-resistant walls surrounding a treatment chamber, a lid member that closes an open end of the pressure-resistant container, a supply means that supplies a process fluid into the treatment chamber, a partition wall that is thinner than the pressure-resistant wall and is provided along the inside surface of said pressure-resistant container to form a partitioned chamber with said inside surface, and a heat transfer control means. Said heat transfer control means controls heat transfer between said treatment chamber and said partitioned chamber by heating or cooling a heating medium outside the container and feeding said heating medium into said partitioned chamber.
摘要翻译：目的是提供一种高压处理设备，其中可以在短时间内有效地调节处理室中的压力或温度，而不会显着增加设备的尺寸或复杂性。高压处理装置具有耐压性容器，该耐压容器具有围绕处理室的耐压壁，封闭耐压容器的开口端的盖构件，将处理流体供给到处理室的供给单元，分隔壁比所述耐压壁更薄，并且沿着所述耐压容器的内表面设置以形成具有所述内表面的分隔室，以及传热控制装置。所述传热控制装置通过加热或冷却容器外部的加热介质并将所述加热介质供入所述分隔室来控制所述处理室和所述分隔室之间的热传递。

4. 发明授权

US07080651B2 High pressure processing apparatus and method 失效
标题翻译：高压加工设备及方法
公开(公告)号：US07080651B2
公开(公告)日：2006-07-25
申请号：US10147742
申请日：2002-05-16
申请人： Ikuo Mizobata , Yusuke Muraoka , Kimitsugu Saito , Ryuji Kitakado , Yoichi Inoue , Yoshihiko Sakashita , Katsumi Watanabe , Masahiro Yamagata , Hisanori Oshiba
发明人： Ikuo Mizobata , Yusuke Muraoka , Kimitsugu Saito , Ryuji Kitakado , Yoichi Inoue , Yoshihiko Sakashita , Katsumi Watanabe , Masahiro Yamagata , Hisanori Oshiba
IPC分类号： B08B3/04
CPC分类号： B08B9/0321 , B08B7/0021 , Y10S134/902
摘要： When the hatch of a substrate washing chamber 5 is opened to receive a substrate, certain valves are closed, and one valve is opened, to supply CO2 to purge the substrate washing chamber 5 to and exclude air. When the hatch is closed, another valve is opened to vent substrate washing chamber 5 so that the CO2 expels any gas and unwanted air from the substrate washing chamber 5 and the conduits. Thereafter, supercritical CO2 is used to wash the substrate and clean the circulation line. The flow of supercritical CO2 is sent to the substrate washing chamber 5. After flowing through the circulation line, including a circulation channel 11, it passes through a bypass channel 12 to a decompressor 7. Any chemicals or organic substances left in the circulation line are continuously sent to separation/recovery bath 8 together with the flow.
摘要翻译：当基板清洗室5的开口打开以接收基板时，某些阀关闭，并且一个阀打开以供应CO 2以清洗基板清洗室5并排除空气。当舱口关闭时，打开另一个阀以排放基板清洗室5，使得CO 2从基板清洗室5和导管排出任何气体和不需要的空气。此后，使用超临界CO 2 2洗涤基底并清洁循环线。超临界CO 2 2的流动被送到衬底洗涤室5。在流过包括循环通道11的循环管线之后，它通过旁路通道12到达减压器7。残留在循环管线中的任何化学物质或有机物质与流动一起连续地送到分离/回收槽8中。

5. 发明申请

US20070272126A1 Process For Producing Porous Object And Apparatus Therefor 有权
标题翻译：生产多孔物体及其设备的方法
公开(公告)号：US20070272126A1
公开(公告)日：2007-11-29
申请号：US11547472
申请日：2005-04-25
申请人： Katsumi Watanabe , Masahiro Yamagata
发明人： Katsumi Watanabe , Masahiro Yamagata
IPC分类号： C04B16/08
CPC分类号： C01B33/1585
摘要： Disclosed is a process for producing porous materials by replacing a first solvent in a wet material containing the first solvent with a second solvent in a high pressure condition and drying the resulting wet material which process comprises a mixed solvent feeding step for feeding a mixed solvent composed of a solvent identical to or of the same kind as the first solvent and the second solvent to the wet material.
摘要翻译：公开了一种多孔材料的制造方法，其特征在于，在高压条件下用第二溶剂置换含有第一溶剂的湿物质中的第一溶剂，干燥所得到的湿物质，该方法包括：混合溶剂供给步骤，与第一溶剂和第二溶剂相同或相同类型的溶剂加到湿材料中。

6. 发明授权

US07111630B2 High pressure processing apparatus and method 失效
标题翻译：高压加工设备及方法
公开(公告)号：US07111630B2
公开(公告)日：2006-09-26
申请号：US10879318
申请日：2004-06-28
申请人： Ikuo Mizobata , Yusuke Muraoka , Kimitsugu Saito , Ryuji Kitakado , Yoichi Inoue , Yoshihiko Sakashita , Katsumi Watanabe , Masahiro Yamagata , Hisanori Oshiba
发明人： Ikuo Mizobata , Yusuke Muraoka , Kimitsugu Saito , Ryuji Kitakado , Yoichi Inoue , Yoshihiko Sakashita , Katsumi Watanabe , Masahiro Yamagata , Hisanori Oshiba
IPC分类号： B08B3/04
CPC分类号： B08B9/0321 , B08B7/0021 , Y10S134/902
摘要： When the hatch of a substrate washing chamber 5 is opened to receive a substrate, certain valves are closed, and a valve is opened, supply CO2 to purge the substrate washing chamber 5 to and exclude air. When the hatch is closed, another valve is opened to vent substrate washing chamber 5 so that the CO2 expels any gas and unwanted air from the substrate washing chamber 5 and the conduits. Thereafter, super critical CO2 is used to wash the substrate and clean the circulation line. The flow of supercritical CO2 is sent to the substrate washing chamber 5. After flowing through the circulation line, including a circulation channel 11, it passes through a bypass channel 12 to a decompressor 7. Any chemicals or organic substances left in the circulation line are continuously sent to a separation/recover bath 8 together with the flow.
摘要翻译：当基板清洗室5的开口被打开以接收基板时，某些阀关闭，并且阀打开，供应CO 2以清洗基板清洗室5并排除空气。当舱口关闭时，打开另一个阀以排放基板清洗室5，使得CO 2从基板清洗室5和导管排出任何气体和不需要的空气。此后，使用超临界CO 2 2来洗涤基底并清洁循环线。超临界CO 2 2的流动被送到衬底洗涤室5。在流过包括循环通道11的循环管线之后，它通过旁路通道12到达减压器7。残留在循环管线中的任何化学物质或有机物质与流体一起被连续地送到分离/回收槽8中。

7. 发明授权

US06823880B2 High pressure processing apparatus and high pressure processing method 失效
标题翻译：高压加工设备及高压加工方法
公开(公告)号：US06823880B2
公开(公告)日：2004-11-30
申请号：US10131193
申请日：2002-04-25
申请人： Yoshihiko Sakashita , Katsumi Watanabe , Masahiro Yamagata , Hisanori Oshiba , Shogo Sarumaru , Yusuke Muraoka , Kimitsugu Saito , Ikuo Mizobata , Ryuji Kitakado
发明人： Yoshihiko Sakashita , Katsumi Watanabe , Masahiro Yamagata , Hisanori Oshiba , Shogo Sarumaru , Yusuke Muraoka , Kimitsugu Saito , Ikuo Mizobata , Ryuji Kitakado
IPC分类号： B08B1500
CPC分类号： H01L21/67017 , B08B7/0021 , H01L21/67126 , Y10S134/902
摘要： A high-pressure processing apparatus includes a processing vessel including a processing chamber formed therein to perform a certain process onto an object in the processing chamber; fluid feeding means which feeds a high-pressure fluid into the processing chamber; fluid discharging means which discharges the high-pressure fluid from the processing chamber; an agitating unit which is arranged in the processing chamber and is operative to flow the high-pressure fluid over the object by relative rotation to the processing vessel; a communicating channel which is formed in the processing vessel to communicate inside and outside of the processing chamber; a rotary driving member which is coupled to the agitating unit via a shaft portion provided in the communicating channel; and a sealing portion which is provided between the shaft portion and the processing vessel to disconnect the processing chamber from the rotary driving member. The fluid discharging means includes a fluid discharging port formed in a certain position of the communicating channel closer to the processing chamber than the sealing portion to discharge the high-pressure fluid.
摘要翻译：高压处理装置包括：处理容器，其包括形成在其中的处理室，以对处理室中的物体执行一定的处理; 流体供给装置，其将高压流体供给到处理室中; 从处理室排出高压流体的流体排出装置; 搅拌单元，其布置在处理室中并且可操作以通过相对于处理容器的旋转将高压流体流过物体; 形成在所述处理容器中以在所述处理室内部和外部连通的连通通道; 旋转驱动构件，其经由设置在所述连通通道中的轴部联接到所述搅拌单元; 以及密封部，其设置在所述轴部和所述处理容器之间，以将所述处理室与所述旋转驱动构件断开。流体排出装置包括形成在与密封部分相比更靠近处理室的连通通道的特定位置中以排出高压流体的流体排放口。

8. 发明申请

US20050051194A1 Method for high-pressure processing 失效
标题翻译：高压处理方法
公开(公告)号：US20050051194A1
公开(公告)日：2005-03-10
申请号：US10915320
申请日：2004-08-11
申请人： Yoshihiko Sakashita , Takahiko Ishii , Masahiro Yamagata , Tetsuya Yoshikawa
发明人： Yoshihiko Sakashita , Takahiko Ishii , Masahiro Yamagata , Tetsuya Yoshikawa
IPC分类号： G03F7/42 , A01J11/04 , B08B5/04 , B08B7/00 , H01L21/027 , H01L21/304
CPC分类号： B08B7/0021 , G03F7/422
摘要： An object is subjected to high-pressure processing by bringing at least a high-pressure fluid into contact with the object under pressure in a high-pressure processing chamber, and then the high-pressure processing chamber is depressurized while the temperature in the chamber is controlled to be maintained above a temperature achieved by an adiabatic expansion, the adiabatic expansion starting from the pressure and temperature at the end of the high-pressure processing step. To control in such a way, the temperature in the high-pressure processing chamber is controlled so as to suppress or recover a temperature descent caused by an adiabatic expansion during the depressurizing step. This solves a problem in which the temperature is decreased to the vapor-liquid phase coexistence region or a region in which a solid is deposited.
摘要翻译：通过在高压处理室中使至少一个高压流体与压力物体接触而对物体进行高压处理，然后高压处理室在室内的温度为控制为保持高于通过绝热膨胀实现的温度，绝热膨胀从高压加工步骤结束时的压力和温度开始。为了以这种方式进行控制，控制高压处理室中的温度以抑制或恢复在减压步骤期间由绝热膨胀引起的温度下降。这解决了温度降低到气相共存区域或其中沉积固体的区域的问题。

9. 发明申请

US20090275776A1 PROCESS AND EQUIPMENT FOR THE DECOMPOSITION AND RECOVERY OF ISOCYANATE COMPOUNDS 有权
标题翻译：异氰酸酯化合物的分解和还原过程和设备
公开(公告)号：US20090275776A1
公开(公告)日：2009-11-05
申请号：US11995397
申请日：2006-07-12
申请人： Fumihiko Kasuya , Masahiro Yamagata , Shigetoshi Suzuki , Tadashi Yoshida
发明人： Fumihiko Kasuya , Masahiro Yamagata , Shigetoshi Suzuki , Tadashi Yoshida
IPC分类号： C07C263/18 , B01J19/00 , B01J19/18 , B01J19/20
CPC分类号： B01J19/20 , B01J3/02 , B01J3/042 , B01J19/006 , B01J2219/00772 , B01J2219/185 , B01J2219/1943 , C07C209/62 , C07C2601/14 , C07C211/12 , C07C211/18 , C07C211/27 , C07C211/36 , C07C211/46 , C07C211/50 , C07C211/51 , C07C211/58
摘要： The present invention relates to a method for decomposing and recovering an isocyanate compound, which comprises: continuously mixing and dispersing into water at high pressure and high temperature an isocyanate compound having at least one isocyanate group or group derived from an isocyanate group in a molten state or solution state, supplying a liquid mixture containing the isocyanate compound and the water at high pressure and high temperature continuously to a reactor, followed by subjecting the isocyanate compound to a decomposition reaction in the reactor, and recovering a raw material for the isocyanate compound or a derivative thereof; and an apparatus for decomposing and recovering an isocyanate compound, which comprises: a reactor which brings water at high pressure and high temperature into contact with an isocyanate compound having at least one isocyanate group or group derived from an isocyanate group to cause a decomposition reaction, a water supply line which continuously supplies the water at high pressure and high temperature to a reactor, a compound supply line which continuously supplies the isocyanate compound in a molten state or solution state to the water supply line, an on-off valve which communicates the compound supply line with a vicinity of a communication portion of the water supply line to the reactor, a dehydrating device which conducts a dehydration of a decomposition reaction product discharged from the reactor, and a purification device which purifies the decomposition reaction product after the dehydration.
摘要翻译：本发明涉及一种分解和回收异氰酸酯化合物的方法，包括：在高压和高温下连续混合和分散在具有至少一种异氰酸酯基团或衍生自异氰酸酯基团的基团的异氰酸酯化合物处于熔融状态或溶液状态，将含有异氰酸酯化合物和水的液体混合物在高压高温下连续供给反应器，然后使异氰酸酯化合物在反应器中进行分解反应，并回收异氰酸酯化合物的原料或其衍生物; 以及用于分解和回收异氰酸酯化合物的装置，其包括：使高压高温水与具有至少一个异氰酸酯基的异氰酸酯化合物或衍生自异氰酸酯基团的异氰酸酯化合物接触引起分解反应的反应器，向反应器连续供给高压高温的水的供水管线，向熔融状态或溶液状态连续供给异氰酸酯化合物的供给管线，供给管路，其将化合物供给管线，与供水管路的连通部分邻近反应器，将从反应器排出的分解反应产物脱水的脱水装置，以及在脱水后净化分解反应产物的净化装置。

10. 发明授权

US07452729B2 Waste high-pressure fluid processing method 失效
标题翻译：废弃高压流体处理方法
公开(公告)号：US07452729B2
公开(公告)日：2008-11-18
申请号：US10611980
申请日：2003-07-03
申请人： Masahiro Yamagata
发明人： Masahiro Yamagata
IPC分类号： G01N30/00
CPC分类号： B01D53/04 , B01D47/14 , B01D2253/306 , Y10T436/204998 , Y10T436/25375 , Y10T436/25875
摘要： The present invention relates to a method for processing a waste high-pressure fluid, which is yielded by bringing a high-pressure fluid into contact with a processing object in a high-pressure processing vessel to make unnecessary materials on the processing object accompany it. In accordance with the present invention, a novel processing method is provided which includes the steps of draining liquid ingredients, which is obtained from a preliminarily refined waste medium-pressure fluid, having been decompressed from the waste high-pressure fluid and provided to a separating means filled with packing materials, out of a system with unnecessary materials, and refining gas ingredients, which is also obtained from the preliminarily refined waste medium-pressure fluid, in an adsorbing means including adsorbents.
摘要翻译：本发明涉及一种处理废弃高压流体的方法，该方法是通过使高压流体与高压处理容器中的处理对象接触而在加工对象上附加不必要的材料而产生的。根据本发明，提供了一种新的加工方法，其包括从已经从废弃高压流体中减压并提供给分离在包含吸附剂的吸附装置中，填充有填充材料的装置，不需要的材料的系统，以及也是从预先精制的废物中压流体获得的精炼气体成分。

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