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1. 发明授权

US08128837B2 Latent curing agent for epoxy resin and method for manufacturing the same 有权
标题翻译：环氧树脂的潜在固化剂及其制造方法
公开(公告)号：US08128837B2
公开(公告)日：2012-03-06
申请号：US12078156
申请日：2008-03-27
申请人： Daisuke Masuko , Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima
发明人： Daisuke Masuko , Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima
IPC分类号： C09K3/00 , C08L63/00 , C08G59/18 , C08G59/68
CPC分类号： C08G18/6484 , C08G18/7664 , C08G18/7671 , H05K3/323
摘要： A latent epoxy resin curing agent is provided which exhibits excellent solvent resistance and low-temperature fast-curing ability, and contains an imidazole-based compound as a main component. In the latent epoxy resin curing agent containing the imidazole-based compound as a main component, adduct particles formed through adduct reaction of an epoxy-based compound with the particulate imidazole-based compound are coated with an ethyl cellulose film. Furthermore, the surfaces of the adduct particles may be crosslinked with a polyfunctional isocyanate compound. A mixture of the epoxy-based compound, the particulate imidazole-based compound, and ethyl cellulose in a predetermined saturated hydrocarbon-based solvent is heated under stirring. Then, the epoxy-based compound and the particulate imidazole-based compound are subjected to adduct reaction to give a slurry of the adduct. After the slurry is cooled, the latent epoxy resin curing agent is filtrated.
摘要翻译：提供一种潜在的环氧树脂固化剂，其具有优异的耐溶剂性和低温快速固化能力，并且含有咪唑类化合物作为主要成分。在含有咪唑类化合物作为主要成分的潜在环氧树脂固化剂中，通过环氧类化合物与微粒状咪唑类化合物的加成反应而形成的加合物粒子被乙基纤维素膜包覆。此外，加合物颗粒的表面可以与多官能异氰酸酯化合物交联。在预定的饱和烃类溶剂中将环氧类化合物，微粒状咪唑类化合物和乙基纤维素的混合物在搅拌下加热。然后，将环氧类化合物和微粒状咪唑类化合物进行加合反应，得到加合物的淤浆。在浆液冷却后，过氧化潜在的环氧树脂固化剂。

2. 发明授权

US08211330B2 Latent curing agent for epoxy resin and method for manufacturing the same 有权
标题翻译：环氧树脂的潜在固化剂及其制造方法
公开(公告)号：US08211330B2
公开(公告)日：2012-07-03
申请号：US12078165
申请日：2008-03-27
申请人： Daisuke Masuko , Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima
发明人： Daisuke Masuko , Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima
IPC分类号： C09K3/00 , C08L63/00 , C08G59/18 , C08G59/68
CPC分类号： C08G18/6484
摘要： A latent epoxy resin curing agent is provided which can be manufactured without using an amphiphilic polymer compound requiring a painful trial and error selection process, exhibits excellent solvent resistance and low-temperature fast-curing ability, and contains an imidazole-based compound as a main component. In the latent epoxy resin curing agent containing the imidazole-based compound as a main component, the adduct particles of the epoxy-based compound and the imidazole-based compound are coated with an ethyl cellulose film, and the surface thereof is crosslinked with a polyfunctional isocyanate compound. The epoxy-based compound, the imidazole-based compound, and ethyl cellulose are dissolved in a predetermined saturated hydrocarbon-based solvent under stirring and heating. Then, the epoxy-based compound and the imidazole-based compound are subjected to adduct reaction to obtain a slurry of the adduct. After the slurry was cooled, the polyfunctional isocyanate compound is added thereto to crosslink the ethyl cellulose film.
摘要翻译：提供一种潜在的环氧树脂固化剂，其可以在不需要使用痛苦的试错误选择方法的两亲性聚合物化合物的情况下制造，显示出优异的耐溶剂性和低温快速固化能力，并且含有咪唑类化合物作为主要零件。在含有咪唑类化合物作为主要成分的潜在环氧树脂固化剂中，环氧类化合物和咪唑类化合物的加合物颗粒用乙基纤维素膜包覆，其表面与多官能团异氰酸酯化合物。环氧类化合物，咪唑类化合物和乙基纤维素在搅拌和加热下溶解在预定的饱和烃类溶剂中。然后，将环氧类化合物和咪唑类化合物进行加合反应，得到加合物的淤浆。在浆料冷却后，加入多官能异氰酸酯化合物以使乙基纤维素膜交联。

3. 发明申请

US20080161589A1 Latent Curing Agent 有权
标题翻译：潜在固化剂
公开(公告)号：US20080161589A1
公开(公告)日：2008-07-03
申请号：US11884527
申请日：2006-06-02
申请人： Katsuhiko Komuro , Tadasu Kawashima , Masahiko Ito , Daisuke Masuko
发明人： Katsuhiko Komuro , Tadasu Kawashima , Masahiko Ito , Daisuke Masuko
IPC分类号： C07F5/06
CPC分类号： C07F7/21
摘要： An aluminum chelate-based latent curing agent capable of curing a thermosetting epoxy resin under the condition of relatively low temperature in a short period of time is provided. Furthermore, a method for manufacturing the latent curing agent is provided, in which the curing conditions of the aluminum chelate-based latent curing agent can be controlled relatively easily.The aluminum chelate-based latent curing agent is prepared by reacting an aluminum chelate agent with a silsesquioxane type oxetane derivative in the presence of a water insoluble or poorly water-soluble cellulose ether, whereby latency properties are imparted thereto. This latent curing agent contains a coating layer composed of the water insoluble or poorly water-soluble cellulose ether. Preferably, the surface is treated with an isocyanate compound.
摘要翻译：提供一种能够在短时间内在相对较低温度的条件下固化热固性环氧树脂的铝螯合物系潜在性固化剂。此外，提供了一种用于制造潜在性固化剂的方法，其中可以相对容易地控制铝螯合物类潜在性固化剂的固化条件。铝螯合物系潜在性固化剂是通过使铝螯合剂与倍半硅氧烷型氧杂环丁烷衍生物在水不溶性或难溶于水的纤维素醚存在下反应制备的，由此赋予延迟性能。该潜在性固化剂含有由水不溶性或难溶于水的纤维素醚构成的涂层。优选地，用异氰酸酯化合物处理表面。

4. 发明申请

US20080249258A1 Latent curing agent for epoxy resin and method for manufacturing the same 有权
标题翻译：环氧树脂的潜在固化剂及其制造方法
公开(公告)号：US20080249258A1
公开(公告)日：2008-10-09
申请号：US12078165
申请日：2008-03-27
申请人： Daisuke Masuko , Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima
发明人： Daisuke Masuko , Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima
IPC分类号： C08G18/58
CPC分类号： C08G18/6484
摘要： A latent epoxy resin curing agent is provided which can be manufactured without using an amphiphilic polymer compound requiring a painful trial and error selection process, exhibits excellent solvent resistance and low-temperature fast-curing ability, and contains an imidazole-based compound as a main component. In the latent epoxy resin curing agent containing the imidazole-based compound as a main component, the adduct particles of the epoxy-based compound and the imidazole-based compound are coated with an ethyl cellulose film, and the surface thereof is crosslinked with a polyfunctional isocyanate compound. The epoxy-based compound, the imidazole-based compound, and ethyl cellulose are dissolved in a predetermined saturated hydrocarbon-based solvent under stirring and heating. Then, the epoxy-based compound and the imidazole-based compound are subjected to adduct reaction to obtain a slurry of the adduct. After the slurry was cooled, the polyfunctional isocyanate compound is added thereto to crosslink the ethyl cellulose film.
摘要翻译：提供一种潜在的环氧树脂固化剂，其可以在不需要使用痛苦的试错误选择方法的两亲性聚合物化合物的情况下制造，显示出优异的耐溶剂性和低温快速固化能力，并且含有咪唑类化合物作为主要零件。在含有咪唑类化合物作为主要成分的潜在环氧树脂固化剂中，环氧类化合物和咪唑类化合物的加合物颗粒用乙基纤维素膜包覆，其表面与多官能团异氰酸酯化合物。环氧类化合物，咪唑类化合物和乙基纤维素在搅拌和加热下溶解在预定的饱和烃类溶剂中。然后，将环氧类化合物和咪唑类化合物进行加合反应，得到加合物的淤浆。在浆料冷却后，加入多官能异氰酸酯化合物以使乙基纤维素膜交联。

5. 发明申请

US20090230360A1 Latent Curing Agent 审中-公开
标题翻译：潜在固化剂
公开(公告)号：US20090230360A1
公开(公告)日：2009-09-17
申请号：US12227905
申请日：2008-01-17
申请人： Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima , Daisuke Masuko
发明人： Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima , Daisuke Masuko
IPC分类号： H01B1/12 , C08L63/00 , C08L23/18
CPC分类号： C08G59/70 , C08G59/24 , C08L63/00 , H05K3/323
摘要： An aluminum chelate-based latent curing agent, which can cure a thermosetting epoxy resin at a relatively low temperature in a short time, is made latent by reacting a silsesquioxane-type oxetane derivative with an aluminum chelating agent in the presence of an alicyclic epoxy compound, and then further reacting the resultant mixture with a liquid epoxy resin and an imidazole compound or with an aromatic vinyl compound and a radical polymerization initiator.
摘要翻译：通过在脂环族环氧化合物的存在下使硅倍半氧烷型氧杂环丁烷衍生物与铝螯合剂反应，可以在短时间内在相对低的温度下固化热固性环氧树脂的铝螯合物系潜在性固化剂然后使所得混合物与液体环氧树脂和咪唑化合物或芳族乙烯基化合物和自由基聚合引发剂进一步反应。

6. 发明授权

US07557230B2 Latent curing agent 有权
标题翻译：潜在固化剂
公开(公告)号：US07557230B2
公开(公告)日：2009-07-07
申请号：US11884527
申请日：2006-06-02
申请人： Katsuhiko Komuro , Tadasu Kawashima , Masahiko Ito , Daisuke Masuko
发明人： Katsuhiko Komuro , Tadasu Kawashima , Masahiko Ito , Daisuke Masuko
IPC分类号： C07F7/02 , C11D3/39
CPC分类号： C07F7/21
摘要： An aluminum chelate-based latent curing agent capable of curing a thermosetting epoxy resin under the condition of relatively low temperature in a short period of time is provided. Furthermore, a method for manufacturing the latent curing agent is provided, in which the curing conditions of the aluminum chelate-based latent curing agent can be controlled relatively easily.The aluminum chelate-based latent curing agent is prepared by reacting an aluminum chelate agent with a silsesquioxane type oxetane derivative in the presence of a water insoluble or poorly water-soluble cellulose ether, whereby latency properties are imparted thereto. This latent curing agent contains a coating layer composed of the water insoluble or poorly water-soluble cellulose ether. Preferably, the surface is treated with an isocyanate compound.
摘要翻译：提供一种能够在短时间内在相对较低温度的条件下固化热固性环氧树脂的铝螯合物系潜在性固化剂。此外，提供了一种用于制造潜在性固化剂的方法，其中可以相对容易地控制铝螯合物类潜在性固化剂的固化条件。铝螯合物系潜在性固化剂是通过使铝螯合剂与倍半硅氧烷型氧杂环丁烷衍生物在水不溶性或难溶于水的纤维素醚存在下反应制备的，由此赋予延迟性能。该潜在性固化剂含有由水不溶性或难溶于水的纤维素醚构成的涂层。优选地，用异氰酸酯化合物处理表面。

7. 发明申请

US20080249257A1 Latent curing agent for epoxy resin and method for manufacturing the same 有权
标题翻译：环氧树脂的潜在固化剂及其制造方法
公开(公告)号：US20080249257A1
公开(公告)日：2008-10-09
申请号：US12078156
申请日：2008-03-27
申请人： Daisuke Masuko , Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima
发明人： Daisuke Masuko , Katsuhiko Komuro , Masahiko Ito , Tadasu Kawashima
IPC分类号： C08G18/58
CPC分类号： C08G18/6484 , C08G18/7664 , C08G18/7671 , H05K3/323
摘要： A latent epoxy resin curing agent is provided which can be manufactured without using an amphiphilic polymer compound requiring a painful trial and error selection process, exhibits excellent solvent resistance and low-temperature fast-curing ability, and contains an imidazole-based compound as a main component. In the latent epoxy resin curing agent containing the imidazole-based compound as a main component, adduct particles formed through adduct reaction of an epoxy-based compound with the particulate imidazole-based compound are coated with an ethyl cellulose film. Furthermore, the surfaces of the adduct particles may be crosslinked with a polyfunctional isocyanate compound. A mixture of the epoxy-based compound, the particulate imidazole-based compound, and ethyl cellulose in a predetermined saturated hydrocarbon-based solvent is heated under stirring. Then, the epoxy-based compound and the particulate imidazole-based compound are subjected to adduct reaction to give a slurry of the adduct. After the slurry is cooled, the latent epoxy resin curing agent is filtrated. If necessary, the ethyl cellulose film is crosslinked with a polyfunctional isocyanate compound.
摘要翻译：提供一种潜在的环氧树脂固化剂，其可以在不需要使用痛苦的试错误选择方法的两亲性聚合物化合物的情况下制造，显示出优异的耐溶剂性和低温快速固化能力，并且含有咪唑类化合物作为主要零件。在含有咪唑类化合物作为主要成分的潜在环氧树脂固化剂中，通过环氧类化合物与微粒状咪唑类化合物的加成反应而形成的加合物粒子被乙基纤维素膜包覆。此外，加合物颗粒的表面可以与多官能异氰酸酯化合物交联。在预定的饱和烃类溶剂中将环氧类化合物，微粒状咪唑类化合物和乙基纤维素的混合物在搅拌下加热。然后，将环氧类化合物和微粒状咪唑类化合物进行加合反应，得到加合物的淤浆。在浆液冷却后，过氧化潜在的环氧树脂固化剂。如果需要，乙基纤维素膜与多官能异氰酸酯化合物交联。

8. 发明授权

US06534172B1 Pressure-sensitive adhesive tape and process for producing the same 有权
标题翻译：胶带及其制造方法
公开(公告)号：US06534172B1
公开(公告)日：2003-03-18
申请号：US09424045
申请日：1999-11-18
申请人： Tadasu Kawashima
发明人： Tadasu Kawashima
IPC分类号： B32B712
CPC分类号： B32B38/0012 , B32B2038/0016 , B32B2307/716 , C09J7/25 , C09J2421/00 , C09J2429/005 , C09J2467/006 , C09J2479/086 , Y10T428/28 , Y10T428/2839 , Y10T428/2843 , Y10T428/2857
摘要： A technique for improving the adhesive force between a biodegradable base film and a rubbery adhesive layer. An adhesive tape is obtained by rubbing the surface of a biodegradable film 9 by a means of rubbing 7 and then applying solution of ingredients of adhesive layer thereonto, thus forming an adhesive layer. The adhesion force between the base film and the adhesive layer is improved by the rubbing treatment. When the solution of ingredients of adhesive layer is an aqueous system, it is also possible that solution of ingredients of primer layer containing an organic compound as a solvent is applied onto the rubbed surface to thereby form a primer layer followed by the formation of the adhesive layer. The adhesive layer may contain fillers, coloring agents, age resistors, etc. so long as the biodegradability is not deteriorated thereby. It is preferable that a separate film to be bonded to the surface of the adhesive layer is also a biodegradable one.
摘要翻译：一种用于改善生物降解性基底膜和橡胶粘合剂层之间的粘合力的技术。通过摩擦7将生物降解性膜9的表面摩擦，然后在其上涂覆粘合剂层的成分的溶液，获得粘合带，因此形成粘合剂层。通过摩擦处理可提高基膜与粘合剂层之间的粘附力。当粘合剂层的成分溶液是水性体系时，也可以将含有有机化合物的底漆层的成分作为溶剂的溶液施加到摩擦面上，从而形成底漆层，然后形成粘合剂层。粘合剂层可以含有填料，着色剂，耐老化剂等，只要生物降解性不会降低。要粘合到粘合剂层的表面上的单独的膜也是可生物降解的。

9. 发明申请

US20120305178A1 ANISOTROPIC ELECTRICALLY CONDUCTIVE ADHESIVE FILM AND METHOD FOR MANUFACTURING SAME 审中-公开
标题翻译：各向异性电导电胶膜及其制造方法
公开(公告)号：US20120305178A1
公开(公告)日：2012-12-06
申请号：US13491130
申请日：2012-06-07
申请人： Minoru Nagashima , Tadasu Kawashima
发明人： Minoru Nagashima , Tadasu Kawashima
IPC分类号： B05D5/12 , B32B38/04 , B32B37/12
CPC分类号： B32B7/06 , B32B7/12 , B32B27/08 , B32B27/36 , B32B2250/40 , B32B2255/26 , B32B2307/202 , B32B2307/306 , B32B2307/7163 , B32B2457/00 , C09J9/02 , H05K3/323 , Y10T156/10 , Y10T156/108 , Y10T428/14
摘要： An anisotropic electrically conductive adhesive film for establishing electrically conductive interconnection between electronic components includes a first peel film having a first peel layer on its one surface, and an adhesive layer provided on the first peel film via the first peel layer. The adhesive layer is formed of an anisotropic electrically conductive adhesive material. The adhesive film also includes a second peel film having a second peel layer on its one surface. The second peel film is provided via the second peel layer on a surface of the adhesive layer opposite to the surface of the adhesive layer provided with the first peel film. The first and second peel films have a non-contractile biodegradable film composed of a fatty acid polyester component as a base material. The first and second peel layers formed of a thermosetting silicone resin curable are provided on each top of the base material.
摘要翻译：用于在电子部件之间建立导电互连的各向异性导电粘合膜包括在其一个表面上具有第一剥离层的第一剥离膜和经由第一剥离层设置在第一剥离膜上的粘合剂层。粘合剂层由各向异性导电粘合剂材料形成。粘合膜还包括在其一个表面上具有第二剥离层的第二剥离膜。第二剥离膜通过第二剥离层设置在与设置有第一剥离膜的粘合剂层的表面相反的粘合剂层的表面上。第一剥离膜和第二剥离膜具有作为基材的脂肪酸聚酯成分构成的非收缩性生物降解性膜。在基材的每个顶部上设置由热固性硅树脂可固化形成的第一和第二剥离层。

10. 发明授权

US06379808B2 Photochromic film comprising a gas barrier deposition film 失效
标题翻译：含有阻气性沉积膜的光致变色膜
公开(公告)号：US06379808B2
公开(公告)日：2002-04-30
申请号：US09053690
申请日：1998-04-02
申请人： Tadasu Kawashima
发明人： Tadasu Kawashima
IPC分类号： B32B1504
CPC分类号： G03C1/685 , B32B27/32 , Y10S428/913 , Y10T428/31678 , Y10T428/31743 , Y10T428/31746 , Y10T428/31797 , Y10T428/31855 , Y10T428/31913 , Y10T428/31917 , Y10T428/31931
摘要： It is an object of the present invention to provide a highly durable photochromic film retaining a photochromic activity for a long time even when used under high temperture and high humidity conditions. A durable photochromic film comprising a coloring material layer containing a photochromic material and a phototransmissive deposition film laminated to said coloring material layer is disclosed.
摘要翻译：本发明的目的是提供即使在高温高湿条件下使用时也能长时间保持光致变色活性的高度耐用的光致变色膜。公开了一种耐久的光致变色膜，其包含含有光致变色材料的着色材料层和层压到所述着色材料层上的光致透过沉积膜。

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