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1. 发明授权

US5783735A Process for preparing polymeric amides useful as additives in fuels and lubricating oils 失效
标题翻译：制备用作燃料和润滑油中添加剂的聚合酰胺的方法
公开(公告)号：US5783735A
公开(公告)日：1998-07-21
申请号：US441029
申请日：1995-05-25
申请人： Jacob I. Emert , Joseph V. Cusumano , David C. Dankworth , William D. Diana , William B. Eckstrom , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
发明人： Jacob I. Emert , Joseph V. Cusumano , David C. Dankworth , William D. Diana , William B. Eckstrom , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
IPC分类号： C10M159/12 , C08F8/00 , C08F8/32 , C10L1/2383 , C10L1/30 , C10L10/00 , C10M129/93 , C10M129/95 , C10M133/56 , C07C231/02 , C10M149/00 , C10M149/18
CPC分类号： C10M133/56 , C08F8/14 , C08F8/32 , C10L1/2383 , C10L1/303 , C10L10/04 , C10M129/93 , C10M129/95 , C10M2207/125 , C10M2207/129 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2215/04 , C10M2215/26 , C10M2217/046 , C10M2217/06
摘要： A process for preparing polymeric amides is disclosed. The process comprises sequentially reacting a hydrocarbon polymer functionalized (e.g., via the Koch reaction) to contain acid, ester, thioacid and/or thioester groups with a heavy polyamine to form a partially derivatized product in which at least about 85% of the functional groups are converted to heavy (thio)amide groups, and then reacting the partially derivatized product with an excess of light amine to complete the derivatization by converting substantially all of the remaining functional groups to light (thio)amide groups. Products of the foregoing process are also disclosed, which products are useful as additives in fuels and in lubricants.
摘要翻译：公开了一种制备聚合酰胺的方法。该方法包括使官能化（例如通过Koch反应）的烃聚合物顺序地反应以将酸，酯，硫代酸和/或硫酯基团与重多胺反应以形成部分衍生化的产物，其中至少约85％的官能团转化为重（硫）酰胺基团，然后使部分衍生化的产物与过量的轻胺反应，通过将基本上所有剩余的官能团转化为轻（硫）酰胺基来完成衍生化。还公开了上述方法的产物，哪些产品可用作燃料和润滑剂中的添加剂。

2. 发明授权

US5872084A Dispersants derived from heavy polyamine and second amine 失效
标题翻译：衍生自重多胺和二胺的分散剂
公开(公告)号：US5872084A
公开(公告)日：1999-02-16
申请号：US7477
申请日：1998-01-15
申请人： Jacob I. Emert , Joseph V. Cusumano , David C. Dankworth , William D. Diana , William B. Eckstrom , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
发明人： Jacob I. Emert , Joseph V. Cusumano , David C. Dankworth , William D. Diana , William B. Eckstrom , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
IPC分类号： C10M159/12 , C08F8/00 , C08F8/32 , C10L1/2383 , C10L1/30 , C10L10/00 , C10M129/93 , C10M129/95 , C10M133/56
CPC分类号： C10M133/56 , C08F8/14 , C08F8/32 , C10L1/2383 , C10L1/303 , C10L10/04 , C10M129/93 , C10M129/95 , C10M2207/125 , C10M2207/129 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2215/04 , C10M2215/26 , C10M2217/046 , C10M2217/06
摘要： A Koch functionalized product, which is the reaction product of at least one hydrocarbon with carbon monoxide and a nucleophilic trapping agent, is derivatized with a heavy polyamine and a second amine. The hydrocarbon is a hydrocarbon compound or a hydrocarbon polymer. A heavy polyamine is a mixture of polyamines containing small amounts of lower polyamine oligomers such as tetraethylene pentamine and pentaethylenehexamine and containing primarily oligomers with more than 6 nitrogens and more extensive branching. Rubber seals embrittlement is reduced or minimized.
摘要翻译：作为至少一种烃与一氧化碳和亲核捕集剂的反应产物的Koch官能化产物用重多胺和第二胺衍生化。烃是烃化合物或烃聚合物。重多胺是含有少量下述多胺低聚物如四亚乙基五胺和五亚乙基六胺的多胺的混合物，并且主要含有具有超过6个氮和更广泛支化的低聚物。橡胶密封件脆化减少或最小化。

3. 发明授权

US5854186A Lubricating oil dispersants derived from heavy polyamine 失效
标题翻译：来自重多胺的润滑油分散剂
公开(公告)号：US5854186A
公开(公告)日：1998-12-29
申请号：US820250
申请日：1997-03-18
申请人： Joseph V. Cusumano , David C. Dankworth , William D. Diana , William B. Eckstrom , Jacob I. Emert , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
发明人： Joseph V. Cusumano , David C. Dankworth , William D. Diana , William B. Eckstrom , Jacob I. Emert , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
IPC分类号： C10M159/12 , C08F8/00 , C08F8/32 , C10L1/2383 , C10L1/30 , C10L10/00 , C10M129/93 , C10M129/95 , C10M133/56 , C10M133/52 , C10M149/14
CPC分类号： C10M133/56 , C08F8/14 , C08F8/32 , C10L1/2383 , C10L1/303 , C10L10/04 , C10M129/93 , C10M129/95 , C10M2207/125 , C10M2207/129 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2215/04 , C10M2215/26 , C10M2217/046 , C10M2217/06
摘要： A Koch functionalized product, which is the reaction product of at least one hydrocarbon with carbon monoxide and a nucleophilic trapping agent is derivatized with a heavy polyamine. A heavy polyamine is a mixture of polyamines comprising small amounts of lower polyamine oligomers such as tetraethylene pentamine and pentahexamine but primarily oligomers with more than 6 nitrogens and more extensive branching.
摘要翻译：作为至少一种烃与一氧化碳和亲核捕集剂的反应产物的Koch官能化产物用重多胺衍生化。重多胺是包含少量低级多胺低聚物如四亚乙基五胺和五胺的多胺的混合物，但主要是具有超过6个氮和更广泛分支的低聚物。

4. 发明授权

US5756431A Dispersants derived from heavy polyamine and second amine 失效
公开(公告)号：US5756431A
公开(公告)日：1998-05-26
申请号：US441030
申请日：1995-05-25
申请人： Jacob I. Emert , Joseph V. Cusumano , David C.. Dankworth , William D. Diana , William B. Eckstrom , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
发明人： Jacob I. Emert , Joseph V. Cusumano , David C.. Dankworth , William D. Diana , William B. Eckstrom , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
IPC分类号： C10M159/12 , C08F8/00 , C08F8/32 , C10L1/2383 , C10L1/30 , C10L10/00 , C10M129/93 , C10M129/95 , C10M133/56
CPC分类号： C10M133/56 , C08F8/14 , C08F8/32 , C10L1/2383 , C10L1/303 , C10L10/04 , C10M129/93 , C10M129/95 , C10M2207/125 , C10M2207/129 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2215/04 , C10M2215/26 , C10M2217/046 , C10M2217/06
摘要： A Koch functionalized product, which is the reaction product of at least one hydrocarbon with carbon monoxide and a nucleophilic trapping agent, is derivatized with a heavy polyamine and a second amine. The hydrocarbon is a hydrocarbon compound or a hydrocarbon polymer. A heavy polyamine is a mixture of polyamines containing small amounts of lower polyamine oligomers such as tetraethylene pentamine and pentaethylenehexamine and containing primarily oligomers with more than 6 nitrogens and more extensive branching. Rubber seals embrittlement is reduced or minimized.

5. 发明授权

US5650536A Continuous process for production of functionalized olefins 失效
标题翻译：连续生产官能化烯烃的方法
公开(公告)号：US5650536A
公开(公告)日：1997-07-22
申请号：US261560
申请日：1994-06-17
申请人： David C. Dankworth , William H. Cross , Joseph V. Cusumano , William D. Diana , William B. Eckstrom , Jacob I. Emert , Keith R. Gorda , Robert M. Koros , Harold W. Margo , Jon E. Stanat
发明人： David C. Dankworth , William H. Cross , Joseph V. Cusumano , William D. Diana , William B. Eckstrom , Jacob I. Emert , Keith R. Gorda , Robert M. Koros , Harold W. Margo , Jon E. Stanat
IPC分类号： C10M159/12 , B01J10/00 , B01J19/24 , C07C51/14 , C07C67/38 , C08F8/00 , C08F8/10 , C08F8/14 , C08F8/32 , C08F8/34 , C08L23/26 , C08L101/00 , C08L101/06 , C10L1/14 , C10L1/18 , C10L1/195 , C10L1/198 , C10L1/20 , C10L1/22 , C10L1/236 , C10L1/238 , C10L1/2383 , C10L1/24 , C10L1/26 , C10L1/28 , C10L1/30 , C10L10/00 , C10M129/95 , C10M133/06 , C10M133/52 , C10M133/54 , C10M133/56 , C10M143/00 , C10M145/12 , C10M149/06 , C10M159/18 , C10N20/04 , C10N30/04 , C07C67/00
CPC分类号： C10M149/06 , B01J19/0066 , B01J19/2415 , B01J19/242 , C07C51/14 , C07C67/38 , C08F8/00 , C08F8/14 , C08F8/32 , C08F8/42 , C10L1/143 , C10L1/1817 , C10L1/195 , C10L1/198 , C10L1/206 , C10L1/221 , C10L1/236 , C10L1/238 , C10L1/2383 , C10L1/2475 , C10L1/2493 , C10L1/2691 , C10L1/285 , C10L1/303 , C10L10/00 , C10L10/18 , C10M129/95 , C10M133/06 , C10M133/52 , C10M133/54 , C10M133/56 , C10M143/00 , C10M145/12 , C10M159/18 , B01J2219/00094 , C08F2800/20 , C10L1/208 , C10L1/2387 , C10L1/2683 , C10L1/30 , C10M2207/023 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2207/289 , C10M2209/00 , C10M2209/02 , C10M2209/082 , C10M2209/10 , C10M2215/04 , C10M2215/042 , C10M2215/08 , C10M2215/082 , C10M2215/22 , C10M2215/221 , C10M2215/224 , C10M2215/225 , C10M2215/226 , C10M2215/26 , C10M2215/28 , C10M2215/30 , C10M2217/024 , C10M2217/046 , C10M2217/06 , C10M2219/062 , C10M2227/061 , C10M2227/09 , C10N2210/01 , C10N2210/02 , C10N2210/03 , C10N2210/04 , C10N2210/05 , C10N2210/06 , C10N2210/07 , C10N2210/08 , C10N2240/00 , C10N2240/02 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/10 , C10N2240/101 , C10N2240/102 , C10N2240/103 , C10N2240/104 , C10N2240/105 , C10N2240/106 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66 , C10N2270/02 , Y02P20/582
摘要： A continuous process for functionalizing olefins, especially polymer olefins in a CSTR or pipe reactor. Esters are preferably produced by continuous reaction of the olefin with carbon monoxide and a nucleophilic trapping agent. The liquid-filled pipe reactor operates in plug flow with static mixers and the CSTR is operated in the substantial absence of air at constant liquid level.
摘要翻译：在CSTR或管式反应器中官能化烯烃，特别是聚合物烯烃的连续方法。酯优选通过烯烃与一氧化碳和亲核捕集剂的连续反应来制备。液体填充的管式反应器在具有静态混合器的活塞流中运行，并且CSTR在基本上不存在恒定液位的空气下操作。

6. 发明授权

US5804667A Dispersant additives and process 失效
公开(公告)号：US5804667A
公开(公告)日：1998-09-08
申请号：US968230
申请日：1997-11-12
申请人： William B. Diana , Joseph V. Cusumano , Keith R. Gorda , Jacob Emert , William B. Eckstrom , David C. Dankworth , Jon E. Stanat , James P. Stokes
发明人： William B. Diana , Joseph V. Cusumano , Keith R. Gorda , Jacob Emert , William B. Eckstrom , David C. Dankworth , Jon E. Stanat , James P. Stokes
IPC分类号： C10M159/12 , C08F6/04 , C08F6/10 , C08F8/00 , C08F8/10 , C10L1/198 , C10L1/238 , C10L1/24 , C10L1/30 , C10M133/52 , C10M159/16
CPC分类号： C10M159/16 , C08F6/04 , C08F8/00 , C10L1/198 , C10L1/238 , C10L1/2475 , C10L1/303 , C10L1/305 , C10M133/52 , Y02P20/584
摘要： The invention pertains to improved lubricating oil dispersants wherein a fractionating polymer is prepared prior to functionalization (e.g., in the Koch reaction) for making dispersant additives. In one aspect, it was discovered that by fractionating a polymer to remove light hydrocarbon and unreacted monomer from the polymer before the carbonylation step of the Koch reaction, the amount of light ester impurities generated was minimized. Light ester is an undesirable byproduct that adversely affects the recycle of the catalyst from the functionalization step of the Koch reaction. The invention also pertains to improved lubricating oil nitrogen-containing dispersant additives derived from fractionated polymer.

7. 发明授权

US5936041A Dispersant additives and process 失效
标题翻译：分散添加剂和工艺
公开(公告)号：US5936041A
公开(公告)日：1999-08-10
申请号：US579317
申请日：1995-12-27
申请人： William B. Diana , Joseph V. Cusumano , Keith R. Gorda , Jacob Emert , William B. Eckstrom , David C. Dankworth , Jon E. Stanat , James P. Stokes
发明人： William B. Diana , Joseph V. Cusumano , Keith R. Gorda , Jacob Emert , William B. Eckstrom , David C. Dankworth , Jon E. Stanat , James P. Stokes
IPC分类号： C10M159/12 , C08F6/04 , C08F6/10 , C08F8/00 , C08F8/10 , C10L1/198 , C10L1/238 , C10L1/24 , C10L1/30 , C10M133/52 , C10M159/16 , C08F8/32
CPC分类号： C10M159/16 , C08F6/04 , C08F8/00 , C10L1/198 , C10L1/238 , C10L1/2475 , C10L1/303 , C10L1/305 , C10M133/52 , Y02P20/584
摘要： The invention pertains to improved lubricating oil dispersants wherein a fractionating polymer is prepared prior to functionalization (e.g., in the Koch reaction) for making dispersant additives. In one aspect, it was discovered that by fractionating a polymer to remove light hydrocarbon and unreacted monomer from the polymer before the carbonylation step of the Koch reaction, the amount of light ester impurities generated was minimized. Light ester is an undesirable byproduct that adversely affects the recycle of the catalyst from the functionalization step of the Koch reaction. The invention also pertains to improved lubricating oil nitrogen-containing dispersant additives derived from fractionated polymer.
摘要翻译：本发明涉及改进的润滑油分散剂，其中在功能化之前（例如在Koch反应中）制备分馏聚合物以制备分散剂添加剂。在一方面，发现通过在Koch反应的羰基化步骤之前从聚合物中分离聚合物以除去轻烃和未反应的单体，所产生的轻质酯杂质的量被最小化。轻质酯是不利的副产物，其不利地影响了来自Koch反应的官能化步骤的催化剂的再循环。本发明还涉及来自分馏聚合物的改进的润滑油含氮分散剂添加剂。

8. 发明授权

US6037445A Process for the continuous production of functionalized polymers 失效
标题翻译：用于连续生产官能化聚合物的方法
公开(公告)号：US6037445A
公开(公告)日：2000-03-14
申请号：US996
申请日：1997-12-30
申请人： David C. Dankworth , Chris F. Meyer , William B. Eckstrom , Ramesh R. Hemrajani , Salvatore Rea , Jon E. Stanat
发明人： David C. Dankworth , Chris F. Meyer , William B. Eckstrom , Ramesh R. Hemrajani , Salvatore Rea , Jon E. Stanat
IPC分类号： B01J10/00 , B01J19/24 , C08F8/00 , C07C67/00 , C08F6/00 , C08G67/00 , C08J3/00
CPC分类号： B01J19/242 , C08F8/18 , B01J2219/00094 , B01J2219/00103 , B01J2219/00159 , B01J2219/00162 , B01J2219/00166
摘要： A continuous process for functionalizing polymers is disclosed, wherein (A) a liquid comprising the polymer and a gas comprising a functionalizing agent are continuously introduced into a dispersing zone operated in laminar flow with high intensity mixing of the liquid and the gas under functionalization conditions, wherein the mixing is conducted for a period of the dispersing zone residence time at a shear rate effective to form a stable gas-liquid dispersion in which the gas is substantially dissolved or dispersed in the liquid for functionalization, and wherein the shear rate is less than about 5 s.sup.-1 for no more than about 30% of the residence time; (B) the gas-liquid dispersion is continuously passed to a blending zone operated in laminar flow with low intensity mixing under functionalization conditions, wherein the mixing is conducted at a shear rate effective to further dissolve the gas into the liquid for further functionalization; and (C) continuously recovering functionalized polymer. The process can be used to carbonylate unsaturated polymers, and is particularly useful in reacting unsaturated polymers with carbon monoxide in the presence of a catalyst and a co-reactant selected from water, H.sub.2 S, alcohols, and thiols to produce functionalized polymer containing carboxylic (thio)acid or carboxylic (thio)ester functional groups.
摘要翻译：公开了一种用于官能化聚合物的连续方法，其中（A）包含聚合物的液体和包含官能化试剂的气体在功能化条件下以液体和气体的高强度混合连续引入层流操作的分散区中，其中混合在有效形成稳定的气液分散体的剪切速率下进行分散区停留时间，其中气体基本上溶解或分散在用于官能化的液体中，并且其中剪切速率小于约5 s-1不超过约30％的停留时间; （B）在功能化条件下，将气液分散体连续地通过低强度混合层流运行的混合区，其中以有效进一步将气体溶解到液体中以进一步官能化的剪切速率进行混合; 和（C）连续回收官能化聚合物。该方法可用于羰基化不饱和聚合物，并且在催化剂和选自水，H 2 S，醇和硫醇的共反应物存在下使不饱和聚合物与一氧化碳反应以产生含羧酸（硫代）的官能化聚合物）酸或羧基（硫代）酯官能团。

9. 发明申请

US20120108726A1 Polyketone Plasticizers 有权
标题翻译：聚酮增塑剂
公开(公告)号：US20120108726A1
公开(公告)日：2012-05-03
申请号：US13345014
申请日：2012-01-06
申请人： Allen D Godwin , Kenneth J. Buturla , Karla S. Colle , Gabor Kiss , Kirk C. Nadler , Abhimanyu O. Patil , Edris Eileen Pike , Ramzi Y. Saleh , Jon E. Stanat , Manika Varma-Nair , Stephen Zushma
发明人： Allen D Godwin , Kenneth J. Buturla , Karla S. Colle , Gabor Kiss , Kirk C. Nadler , Abhimanyu O. Patil , Edris Eileen Pike , Ramzi Y. Saleh , Jon E. Stanat , Manika Varma-Nair , Stephen Zushma
IPC分类号： C07C49/12 , C07C45/49 , C08K5/07 , C07C49/17 , C09K3/00
CPC分类号： C08G67/02 , C08L73/00 , C08L101/00 , C08L2666/14
摘要： The invention relates to polyketone compounds and the at least partially hydrogenated products thereof, the use of said polyketone compounds and/or the at least partially hydrogenated products thereof as plasticizers, processes of making polyketone compounds and the at least partially hydrogenated products thereof, compositions comprising the polyketone compounds and/or the at least partially hydrogenated products thereof, and to articles formed from products of the invention.
摘要翻译：本发明涉及聚酮化合物及其至少部分氢化的产物，所述聚酮化合物和/或其至少部分氢化产物作为增塑剂的用途，制备聚酮化合物的方法及其至少部分氢化的产物，包含聚酮化合物和/或其至少部分氢化的产物，以及由本发明的产物形成的制品。

10. 发明授权

US08115034B2 Polyketone plasticizers 失效
标题翻译：聚酮增塑剂
公开(公告)号：US08115034B2
公开(公告)日：2012-02-14
申请号：US12058397
申请日：2008-03-28
申请人： Allen D. Godwin , Kenneth J. Buturla , Karla S. Colle , Gabor Kiss , Kirk C. Nadler , Abhimanyu O. Patil , Edris Eileen Pike , Ramzi Y. Saleh , Jon E. Stanat , Manika Varma-Nair , Stephen Zushma
发明人： Allen D. Godwin , Kenneth J. Buturla , Karla S. Colle , Gabor Kiss , Kirk C. Nadler , Abhimanyu O. Patil , Edris Eileen Pike , Ramzi Y. Saleh , Jon E. Stanat , Manika Varma-Nair , Stephen Zushma
IPC分类号： C07C45/00 , C07C45/27 , C08G67/00 , C08G67/02
CPC分类号： C08G67/02 , C08L73/00 , C08L101/00 , C08L2666/14
摘要： The invention relates to polyketone compounds and the at least partially hydrogenated products thereof, the use of said polyketone compounds and/or the at least partially hydrogenated products thereof as plasticizers, processes of making polyketone compounds and the at least partially hydrogenated products thereof, compositions comprising the polyketone compounds and/or the at least partially hydrogenated products thereof, and to articles formed from products of the invention.
摘要翻译：本发明涉及聚酮化合物及其至少部分氢化的产物，所述聚酮化合物和/或其至少部分氢化产物作为增塑剂的用途，制备聚酮化合物的方法及其至少部分氢化的产物，包含聚酮化合物和/或其至少部分氢化的产物，以及由本发明的产物形成的制品。

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