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1. 发明授权

US5767330A Process for preparing alkyl chlorides 失效
标题翻译：制备烷基氯的方法
公开(公告)号：US5767330A
公开(公告)日：1998-06-16
申请号：US799035
申请日：1997-02-10
申请人： Josef Metz , Clemens Osterholt , Juergen Lange
发明人： Josef Metz , Clemens Osterholt , Juergen Lange
IPC分类号： C07C17/16 , C07C19/01
CPC分类号： C07C17/16
摘要： The preparation of long-chain alkyl chlorides from alcohols and hydrogen chloride is improved by carrying out the reaction at a temperature below the boiling point of the alkyl chloride, and distilling off the resulting alkyl chloride by feeding in additional hydrochloric acid.
摘要翻译：通过在低于烷基氯的沸点的温度下进行反应，通过加入另外的盐酸蒸馏出所得的烷基氯，可以改善从醇和氯化氢制备长链烷基氯。

2. 发明授权

US5770780A Process for preparing alkyl halides 失效
标题翻译：制备烷基卤的方法
公开(公告)号：US5770780A
公开(公告)日：1998-06-23
申请号：US799068
申请日：1997-02-10
申请人： Josef Metz , Clemens Osterholt
发明人： Josef Metz , Clemens Osterholt
IPC分类号： C07C17/08 , C07C23/08
CPC分类号： C07C17/08
摘要： In the preparation of alkyl halides from cycloaliphatic olefins and hydrohalic acids, the reaction is carried out at a temperature below the boiling point of the olefin without the addition of catalyst and without a solvent. At a high olefin conversion rate, alkyl halides are obtained with high selectivity and with very good color quality.
摘要翻译：在从脂环族烯烃和氢卤酸制备烷基卤化物时，反应在不加入催化剂的情况下在低于烯烃沸点的温度下进行，而不用溶剂。在高烯烃转化率下，以高选择性和非常好的颜色质量获得烷基卤化物。

3. 发明授权

US6121466A Process for the preparation of macrocyclic esters 失效
标题翻译：制备大环酯的方法
公开(公告)号：US6121466A
公开(公告)日：2000-09-19
申请号：US261227
申请日：1999-03-03
申请人： Clemens Osterholt , Josef Metz , Gunther Kohler , Marcel Feld
发明人： Clemens Osterholt , Josef Metz , Gunther Kohler , Marcel Feld
IPC分类号： C07D319/00 , B01J31/18 , B01J31/22 , C07B61/00 , C07D321/00
CPC分类号： C07D321/00 , Y02P20/582
摘要： The invention relates to a process for the preparation of a macrocyclic ester of the general formula: in which m is an integer from 6 to 14 and n is an integer from 2 to 12.
摘要翻译：本发明涉及制备通式如下的大环酯的方法：其中m为6至14的整数，n为2至12的整数。

4. 发明授权

US6107496A Process for the preparation of cyclic esters 失效
标题翻译：环酯的制备方法
公开(公告)号：US6107496A
公开(公告)日：2000-08-22
申请号：US261132
申请日：1999-03-03
申请人： Clemens Osterholt , Josef Metz , Guenther Koehler
发明人： Clemens Osterholt , Josef Metz , Guenther Koehler
IPC分类号： C07B61/00 , C07D321/00 , C07D323/04 , C07D407/00
CPC分类号： C07D321/00 , Y02P20/582
摘要： A process for the preparation of cyclic esters of the general formula: ##STR1## in which m is an integer from 6-14 and n is an integer from 2-6, which comprises heating a dicarboxylic acid bis(glycol) ester of the general formula:HO--(CH.sub.2).sub.n --O--CO--(CH.sub.2).sub.m --CO--O--(CH.sub.2).sub.n --OH, formula IIin which m and n are as defined above,(b) optionally, up to 100% by weight, based on the weight of ester II, of esters of the general formula:H[O--(CH.sub.2).sub.n --O--CO--(CH.sub.2).sub.m --CO--].sub.x --O--(CH.sub.2).sub.n --OH, formula IIIH[O--(CH.sub.2).sub.n --O--CO--(CH.sub.2).sub.m CO--]X--OH and/orformula IVHO--CO--(CH.sub.2).sub.m --CO--[--O--(CH.sub.2).sub.n O--CO--(CH.sub.2).sub.m --CO--].sub.x --OH, formula Vin which m and n are as defined previously and x is an integer >1, and(c) a glycol of the general formula:HO--(CH.sub.2).sub.n --OH, formula VIin which n has the same numerical value as in formula I-V,(d) an inert high-boiling reaction medium, and(e) a catalyst.
摘要翻译：一种制备通式的环酯的方法：其中m是6-14的整数，n是2-6的整数，其包括加热通式为HO的二羧酸双（二醇）酯 - （CH 2）n O-CO-（CH 2）m -CO-O-（CH 2）n -OH，其中m和n如上所定义的式IIin，（b）任选地，至多100重量％酯II的通式为H [O-（CH 2）n O-CO-（CH 2）m -CO-] x O - （CH 2）n -OH的酯，式IIIH [O-（CH 2）n O- CO-（CH 2）m CO-] X-OH和/或式IVHO-CO-（CH 2）m -CO- [-O-（CH 2）n O-CO-（CH 2）m -CO-] x-OH，式Vin 其中m和n如前定义，x是> 1的整数，和（c）通式为HO-（CH 2）n -OH的二醇，其中n具有与式IV相同的数值，（d）惰性高沸点反应介质，和（e）催化剂。

5. 发明授权

US6093286A Process for purifying n-butyl chloride 失效
标题翻译：正丁基氯纯化方法
公开(公告)号：US6093286A
公开(公告)日：2000-07-25
申请号：US084957
申请日：1998-05-28
申请人： Clemens Osterholt , Josef Metz , Udo Jegelka
发明人： Clemens Osterholt , Josef Metz , Udo Jegelka
IPC分类号： C07C17/38 , C07C17/383 , B01D11/04
CPC分类号： C07C17/38 , C07C17/383
摘要： A process for purifying at least 90% pure n-butyl chloride which is present in a mixture with other C.sub.1 to C.sub.4 alkyl chlorides, C.sub.1 to C.sub.4 alcohols, esters, ketones, nitrites, and organic sulfur compounds. In this process the mixture is first distilled, with high-boilers being separated off, and then washed in a plurality of stages with water and with dilute alkali metal hydroxide solution, and, optionally, an aqueous solution of H.sub.2 O.sub.2. In this manner, even a typical impurities may be separated off and a >99% pure product may be obtained.
摘要翻译：纯化与其它C1至C4烷基氯，C1至C4醇，酯，酮，亚硝酸盐和有机硫化合物的混合物中存在的至少90％纯正丁基氯的方法。在此过程中，首先将混合物蒸馏，分离出高锅炉，然后用水和稀碱金属氢氧化物溶液以及任选的H 2 O 2水溶液在多个阶段中洗涤。以这种方式，甚至可以分离出典型的杂质，并且可以获得> 99％的纯品。

6. 发明授权

US06262298B1 Process for the C-alkylation of malonic esters using phase-transfer agents 失效
标题翻译：使用相转移剂丙二酸酯C烷基化的方法
公开(公告)号：US06262298B1
公开(公告)日：2001-07-17
申请号：US09198581
申请日：1998-11-24
申请人： Josef Metz , Clemens Osterholt
发明人： Josef Metz , Clemens Osterholt
IPC分类号： C07C6730
CPC分类号： C07C67/343 , C07C69/34 , C07C69/74
摘要： The invention relates to a process for the C-alkylation of dialkyl malonates, in which a dialkyl malonate is reacted with an alkyl halide in the presence of potassium carbonate as a hydrogen halide acceptor in an inert solvent, and a phase-transfer catalyst is not added until from 50 to 80% of the dialkyl malonate has reacted. The phase-transfer catalyst may be, for example, a tetraalkylammonium salt or a tetraalkylammonium hydroxide, a tetraalkylphosphonium salt or a tetraalkylphosphonium hydroxide or a crown ether.
摘要翻译：本发明涉及丙二酸二烷基酯的方法，其中在惰性溶剂中，在碳酸钾作为卤化氢受体的存在下，丙二酸二烷基酯与烷基卤化物反应，相转移催化剂不是直至丙烯酸二烷基酯的50-80％反应。相转移催化剂可以是例如四烷基铵盐或四烷基氢氧化铵，四烷基鏻盐或四烷基鏻氢氧化物或冠醚。

7. 发明授权

US5831137A Process for the preparation of alkyl halides 失效
标题翻译：制备烷基卤的方法
公开(公告)号：US5831137A
公开(公告)日：1998-11-03
申请号：US799043
申请日：1997-02-10
申请人： Josef Metz , Clemens Osterholt
发明人： Josef Metz , Clemens Osterholt
IPC分类号： C07C17/08 , C07C19/01 , C07C17/02
CPC分类号： C07C17/08
摘要： In the continuous preparation of alkyl halides from branched olefins and hydrohalic acids, the reaction is carried out without the addition of catalysts and without solvents. With a high olefin conversion, alkyl halides are obtained with high selectivity and with very good color quality.
摘要翻译：在从支链烯烃和氢卤酸连续制备烷基卤化物中，反应在不加入催化剂和无溶剂的情况下进行。通过高烯烃转化率，可以获得高选择性和非常好的颜色质量的烷基卤化物。

8. 发明申请

US20050033096A1 Granular alkali metal alkoxides and alkaline earth metal alkoxides 审中-公开
标题翻译：颗粒状碱金属醇盐和碱土金属醇盐
公开(公告)号：US20050033096A1
公开(公告)日：2005-02-10
申请号：US10935595
申请日：2004-09-08
申请人： Andreas Harthun , Christoph Theis , Andre Noppe , Josef Metz
发明人： Andreas Harthun , Christoph Theis , Andre Noppe , Josef Metz
IPC分类号： C07C31/30 , C07C67/343 , C07C29/10
CPC分类号： C07C31/30 , C07C67/343 , C07C69/716
摘要： An alkali metal alkoxide or alkaline earth metal alkoxide in granular form.
摘要翻译：颗粒状碱金属醇盐或碱土金属醇盐。

9. 发明授权

US5105715A Tank turret with increased recoil mass 失效
标题翻译：具有增加回收质量的油罐
公开(公告)号：US5105715A
公开(公告)日：1992-04-21
申请号：US579632
申请日：1990-09-10
申请人： Adolf Nordmann , Wilfried Becker , Josef Metz , Erich Zielinski , Jochen Hoff , Hans Hulsewies , Friedhelm Knorich , Wolfgang Boer
发明人： Adolf Nordmann , Wilfried Becker , Josef Metz , Erich Zielinski , Jochen Hoff , Hans Hulsewies , Friedhelm Knorich , Wolfgang Boer
IPC分类号： F41A25/00 , F41H7/04
CPC分类号： F41H5/20 , F41A25/00 , F41H7/04
摘要： A tank turret including an armored turret housing having a front side provided with solid front armor, and a pivotally mounted gun including a cradle shield, cradle, recoil device and rearward breech block housing being arranged in the turret housing. The armored turret housing, or at least parts of it, are used to increase recoil mass of the gun.
摘要翻译：一个包括装甲转台壳体的坦克炮塔，其前侧设有实心的前装甲，以及一个枢轴安装的枪，其中包括支架护罩，支架，反冲装置和后枪闩壳体。装甲炮塔外壳，或其至少部分，用于增加枪的后座质量。

10. 发明授权

US4955281A Counterrecoil blocking device 失效
标题翻译：反卷取阻挡装置
公开(公告)号：US4955281A
公开(公告)日：1990-09-11
申请号：US390393
申请日：1989-08-07
申请人： Josef Metz , Hans Hulsewis
发明人： Josef Metz , Hans Hulsewis
IPC分类号： F41A25/02
CPC分类号： F41A25/02
摘要： A gun includes a barrel arranged to execute a recoil and a counterrecoil after a shot is fired; a trunnion about which the barrel is pivotal in a vertical plane to assume an index position and firing positions situated at an angle to the index position; a case ejector for ejecting a case from the barrel during counterrecoil; and a counterrecoil blocking device for interrupting the counterrecoil as long as the barrel is in a firing position other than the index position and for allowing the counterrecoil to resume when the barrel assumes the index position, whereby case ejection by the case ejector is effected in the index position.
摘要翻译：一把枪包括一个枪管，用于在射击后被执行反冲和反卷取; 耳轴，所述筒在所述耳轴处于垂直平面中枢转以呈现与所述指示位置成一定角度的折索位置和触发位置; 用于在反卷盘期间从壳体中弹出壳体的壳体喷射器; 以及用于中断反卷盘的反卷取阻挡装置，只要桶处于除索引位置以外的点火位置，并且当筒体呈现折痕位置时允许反卷盘恢复，由此通过壳体喷射器进行壳体喷射指数位置

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