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1. 发明授权

US5401712A Method of manufacture of single phase ceramic superconductors 失效
标题翻译：单相陶瓷超导体的制造方法
公开(公告)号：US5401712A
公开(公告)日：1995-03-28
申请号：US947324
申请日：1992-09-18
申请人： Jitrenda P. Singh , Roger B. Poeppel , Kenneth C. Goretta , Nan Chen
发明人： Jitrenda P. Singh , Roger B. Poeppel , Kenneth C. Goretta , Nan Chen
IPC分类号： H01L39/24 , H01B12/00 , H01L39/12
CPC分类号： H01L39/2464 , Y10S505/742 , Y10S505/782
摘要： A ceramic superconductor is produced by close control of oxygen partial pressure during sintering of the material. The resulting microstructure of YBa.sub.2 Cu.sub.3 O.sub.x indicates that sintering kinetics are enhanced at reduced p(O.sub.2) and that because of second phase precipitates, grain growth is prevented. The density of specimens sintered at 910.degree. C. increased from 79 to 94% theoretical when p(O.sub.2) was decreased from 0.1 to 0.0001 MPa. The increase in density with decrease in p(O.sub.2) derives from enhanced sintering kinetics, due to increased defect concentration and decreased activation energy of the rate-controlling species undergoing diffusion. Sintering at 910.degree. C resulted in a fine-grain microstructure, with an average grain size of about 4 .mu.m. Post sintering annealing in a region of stability for the desired phase converts the second phases and limits grain growth. The method of pinning grain boundaries by small scale decompositive products and then annealing to convert its product to the desired phase can be used for other complex asides. Such a microstructure results in reduced microcracking, strengths as high as 230 MPa and high critical current density capacity.
摘要翻译：陶瓷超导体是通过在材料烧结过程中紧密控制氧分压而产生的。所得到的YBa2Cu3Ox微观结构表明烧结动力学在降低的p（O 2）下得到提高，而由于第二相析出，可以防止晶粒生长。当p（O2）从0.1降低到0.0001 MPa时，在910℃下烧结的样品的密度从理论上从79增加到94％。由于增加的缺陷浓度和速率控制物质经历扩散的活化能降低，p（O 2）的密度增加来自增强的烧结动力学。在910℃烧结得到细晶粒微观结构，平均粒径约4μm。在所需相的稳定区域中的后烧结退火转变第二相并限制晶粒生长。通过小规模分解产物固定晶界的方法，然后退火以将其产物转化成所需相，可用于其它复合物。这种微观结构导致微裂纹减少，强度高达230MPa和高临界电流密度容量。

2. 发明授权

US5856277A Surface texturing of superconductors by controlled oxygen pressure 失效
标题翻译：通过控制氧气压力对超导体进行表面纹理化
公开(公告)号：US5856277A
公开(公告)日：1999-01-05
申请号：US657415
申请日：1996-06-03
申请人： Nan Chen , Kenneth C. Goretta , Stephen E. Dorris
发明人： Nan Chen , Kenneth C. Goretta , Stephen E. Dorris
IPC分类号： C04B35/45 , C04B35/622 , H01L39/24 , B05D5/12 , B05D3/02
CPC分类号： H01L39/2464 , C04B35/4508 , C04B35/62222 , Y10S505/733
摘要： A method of manufacture of a textured layer of a high temperature superconductor on a substrate. The method involves providing an untextured high temperature superconductor material having a characteristic ambient pressure peritectic melting point, heating the superconductor to a temperature below the peritectic temperature, establishing a reduced pO.sub.2 atmosphere below ambient pressure causing reduction of the peritectic melting point to a reduced temperature which causes melting from an exposed surface of the superconductor and raising pressure of the reduced pO.sub.2 atmosphere to cause solidification of the molten superconductor in a textured surface layer.
摘要翻译：在衬底上制造高温超导体纹理化层的方法。该方法包括提供具有特征的环境压力包晶熔点的无纹理的高温超导体材料，将超导体加热到低于包晶温度的温度，建立低于环境压力的降低的pO2气氛，从而将包晶熔点降低到降低的温度，导致从超导体的暴露表面熔化并且降低的pO2气氛的升高压力导致熔融超导体在纹理化表面层中的固化。

3. 发明授权

US5821201A (Bi, Pb).sub.2, Sr.sub.2 Ca.sub.2 Cu.sub.3 O.sub.x superconductor and method of making same utilizing sinter-forging 失效
标题翻译：（Bi，Pb）2，Sr2Ca2Cu3Ox超导体及其使用烧结锻造的方法
公开(公告)号：US5821201A
公开(公告)日：1998-10-13
申请号：US748259
申请日：1996-11-13
申请人： Nan Chen , Kenneth C. Goretta , Michael T. Lanagan
发明人： Nan Chen , Kenneth C. Goretta , Michael T. Lanagan
IPC分类号： C04B35/45 , H01L39/24 , C04B35/626 , C04B35/645
CPC分类号： C04B35/4525 , H01L39/2419 , Y10S505/739
摘要： A (BiPb).sub.2 Sr.sub.2 Ca.sub.2 Cu.sub.3 O.sub.x (Bi223) superconductor with high J.sub.c, phase purity, density and mechanical strength is formed from Bi2223 powder which is synthesized from a mixture of Bi.sub.2 O.sub.3, PbO, SrCO.sub.3, CaCo.sub.3 and CuO. The mixture is milled, then dried and calcined to synthesize the Bi2223 powder with the desired phase purity. The calcination is performed by heating the dried mixture for 50 hours at 840.degree. C. The partially synthesized powder is then milled for 1-4 hours before calcining further for another 50 hours at 855.degree. C. to complete the synthesis. After calcination, the Bi2223 powder is cold pressed to a predetermined density and sinter forged under controlled temperature and time to form a Bi2223 superconductor with the desired superconducting properties.
摘要翻译：由Bi2O3，PbO，SrCO3，CaCo3和CuO的混合物合成的Bi2223粉末形成具有高Jc，相纯度，密度和机械强度的（BiPb）2Sr2Ca2Cu3Ox（Bi223）超导体。将混合物研磨，然后干燥并煅烧以合成具有所需相纯度的Bi2223粉末。煅烧通过在840℃加热干燥的混合物50小时进行。然后将部分合成的粉末研磨1-4小时，然后在855℃下进一步煅烧另外50小时以完成合成。煅烧后，将Bi2223粉末冷压至预定的密度，并在受控的温度和时间下烧结锻造以形成具有所需超导性能的Bi2223超导体。

4. 发明授权

US06455166B1 Metallic substrates for high temperature superconductors 有权
标题翻译：用于高温超导体的金属基板
公开(公告)号：US06455166B1
公开(公告)日：2002-09-24
申请号：US09568890
申请日：2000-05-11
申请人： Thomas G. Truchan , Dean J. Miller , Kenneth C. Goretta , Uthamalingam Balachandran , Robert Foley
发明人： Thomas G. Truchan , Dean J. Miller , Kenneth C. Goretta , Uthamalingam Balachandran , Robert Foley
IPC分类号： H01L3904
CPC分类号： H01L39/2454 , C22F1/10 , Y10T428/31678
摘要： A biaxially textured face-centered cubic metal article having grain boundaries with misorientation angles greater than about 8° limited to less than about 1%. A laminate article is also disclosed having a metal substrate first rolled to at least about 95% thickness reduction followed by a first annealing at a temperature less than about 375° C. Then a second rolling operation of not greater than about 6% thickness reduction is provided, followed by a second annealing at a temperature greater than about 400° C. A method of forming the metal and laminate articles is also disclosed.
摘要翻译：具有大于约8°的取向角大于等于约1％的晶界的双轴织构的面心立方金属制品。还公开了一种层压制品，其首先被轧制至至少约95％的厚度减小，然后在小于约375℃的温度下进行第一次退火。然后不大于约6％的厚度减小的第二次轧制操作是提供，然后在大于约400℃的温度下进行第二次退火。还公开了形成金属和层压制品的方法。

5. 发明授权

US5929001A Engineered flux-pinning centers in BSCCO TBCCO and YBCO superconductors 失效
标题翻译： BSCCO TBCCO和YBCO超导体中的工程焊剂固定中心
公开(公告)号：US5929001A
公开(公告)日：1999-07-27
申请号：US541060
申请日：1995-10-11
申请人： Kenneth C. Goretta , Michael T. Lanagan , Dean J. Miller , Suvankar Sengupta , John C. Parker , Jieguang Hu , Uthamalingam Balachandran , Richard W. Siegel , Donglu Shi
发明人： Kenneth C. Goretta , Michael T. Lanagan , Dean J. Miller , Suvankar Sengupta , John C. Parker , Jieguang Hu , Uthamalingam Balachandran , Richard W. Siegel , Donglu Shi
IPC分类号： C04B35/45 , H01L39/24 , H01B12/00 , C04B35/50 , C04B35/505 , C04B35/63
CPC分类号： H01L39/2483 , C04B35/45 , Y10S505/739
摘要： A method of preparing a high temperature superconductor. A method of preparing a superconductor includes providing a powdered high temperature superconductor and a nanophase material. These components are combined to form a solid compacted mass with the material disposed in the polycrystalline high temperature superconductor. This combined mixture is rapidly heated, forming a dispersion of nanophase size particles without a eutectic reaction. These nanophase particles can have a flat plate or columnar type morphology.
摘要翻译：一种制备高温超导体的方法。制备超导体的方法包括提供粉末状高温超导体和纳米相材料。将这些组分组合以形成固体压实物质，其中材料设置在多晶高温超导体中。这种组合的混合物被快速加热，形成纳米尺寸颗粒的分散体而没有共晶反应。这些纳米相颗粒可以具有平板或柱状形态。

6. 发明授权

US5202306A Fracture toughness for copper oxide superconductors 失效
标题翻译：氧化铜超导体的断裂韧性
公开(公告)号：US5202306A
公开(公告)日：1993-04-13
申请号：US761551
申请日：1991-09-18
申请人： Kenneth C. Goretta , Marc L. Kullberg
发明人： Kenneth C. Goretta , Marc L. Kullberg
IPC分类号： C04B35/45 , C04B35/628 , H01L39/24
CPC分类号： C04B35/4508 , C04B35/4512 , C04B35/4521 , C04B35/62655 , C04B35/62805 , C04B35/62847 , C04B35/803 , H01L39/2477 , C04B2235/3206 , C04B2235/3215 , C04B2235/3217 , C04B2235/3225 , C04B2235/3246 , C04B2235/3463 , C04B2235/449 , C04B2235/522 , C04B2235/5224 , C04B2235/5228 , C04B2235/5236 , C04B2235/5276 , C04B2235/5292 , C04B2235/5436 , C04B2235/5445 , C04B2235/656 , C04B2235/6585 , C04B2235/77 , C04B2235/96 , Y10S505/78 , Y10S505/782 , Y10S505/783 , Y10S505/785
摘要： An oxide-based strengthening and toughening agent, such as tetragonal Zro.sub.2 particles, has been added to copper oxide superconductors, such as superconducting YBa.sub.2 Cu.sub.3 O.sub.x (123) to improve its fracture toughness (K.sub.IC). A sol-gel coating which is non-reactive with the superconductor, such as Y.sub.2 BaCuO.sub.5 (211) on the ZrO.sub.2 particles minimized the deleterious reactions between the superconductor and the toughening agent dispersed therethrough. Addition of 20 mole percent ZrO.sub.2 coated with 211 yielded a 123 composite with a K.sub.IC of 4.5 MPa(m).sup.0.5.
摘要翻译：氧化物强化和增韧剂如四方Zro2颗粒已被添加到氧化铜超导体，如超导YBa2Cu3Ox（123）以提高其断裂韧性（KIC）。与超导体无反应性的溶胶 - 凝胶涂层如ZrO 2颗粒上的Y2BaCuO5（211）使超导体和通过其分散的增韧剂之间的有害反应最小化。用211涂覆的20摩尔％ZrO 2的添加产生了KIC为4.5MPa（m）0.5的123复合物。

7. 发明授权

US07413109B2 Joining of advanced materials by superplastic deformation 有权
标题翻译：通过超塑性变形连接先进材料
公开(公告)号：US07413109B2
公开(公告)日：2008-08-19
申请号：US11302419
申请日：2005-12-12
申请人： Kenneth C. Goretta , Jules L. Routbort , Felipe Gutierrez-Mora
发明人： Kenneth C. Goretta , Jules L. Routbort , Felipe Gutierrez-Mora
IPC分类号： B23K20/00
CPC分类号： C09J5/06 , B23K35/001 , B23K35/3046 , B23K2103/16 , B32B2309/12 , B32B2315/02 , C03C27/06 , C04B35/10 , C04B35/119 , C04B35/4885 , C04B35/5626 , C04B35/6268 , C04B37/001 , C04B37/003 , C04B37/005 , C04B37/006 , C04B2235/3206 , C04B2235/3217 , C04B2235/3222 , C04B2235/3246 , C04B2235/3279 , C04B2235/3826 , C04B2235/3839 , C04B2235/3843 , C04B2235/5276 , C04B2235/5292 , C04B2235/80 , C04B2237/064 , C04B2237/068 , C04B2237/123 , C04B2237/343 , C04B2237/348 , C04B2237/36
摘要： A method for utilizing superplastic deformation with or without a novel joint compound that leads to the joining of advanced ceramic materials, intermetallics, and cermets. A joint formed by this approach is as strong as or stronger than the materials joined. The method does not require elaborate surface preparation or application techniques.
摘要翻译：一种利用具有或不具有导致先进陶瓷材料，金属间化合物和金属陶瓷的接合的新型接合化合物的超塑性变形的方法。通过这种方法形成的接头与所连接的材料一样强或者强。该方法不需要精细的表面处理或应用技术。

8. 发明授权

US07722731B2 Joining of advanced materials by plastic deformation 有权
标题翻译：通过塑性变形连接先进材料
公开(公告)号：US07722731B2
公开(公告)日：2010-05-25
申请号：US11637635
申请日：2006-12-12
申请人： Jules L. Routbort , Dileep Singh , Kenneth C. Goretta , Felipe Gutierrez-Mora
发明人： Jules L. Routbort , Dileep Singh , Kenneth C. Goretta , Felipe Gutierrez-Mora
IPC分类号： C03B29/00 , B29C65/00 , B31B1/60 , B32B37/00
CPC分类号： C04B37/001 , C04B35/645 , C04B37/005 , C04B37/026 , C04B2237/064 , C04B2237/068 , C04B2237/121 , C04B2237/122 , C04B2237/123 , C04B2237/34 , C04B2237/343 , C04B2237/348 , C04B2237/36 , C04B2237/402 , C04B2237/405 , C04B2237/58 , Y10T156/10
摘要： A method for utilizing plastic deformation resulting from grain boundary sliding with or without a novel joint compound that leads to the joining of advanced ceramic materials, intermetallics, and cermets. A joint formed by this approach is as strong as or stronger than the materials joined. The method does not require elaborate surface preparation or application techniques. The method also allows for the formation of transparent joints between two subunits of a construct joined via plastic deformation. The method can be used to tailor residual stresses and maintain native porosity.
摘要翻译：利用具有或不具有导致先进陶瓷材料，金属间化合物和金属陶瓷的接合的新型接合化合物的晶界滑动产生的塑性变形的方法。通过这种方法形成的接头与所连接的材料一样强或者强。该方法不需要精细的表面处理或应用技术。该方法还允许在通过塑性变形连接的构造的两个亚基之间形成透明接头。该方法可用于定制残余应力并保持原生孔隙度。

9. 发明授权

US07452837B2 Fibrous ceramic monoliths made from multi-phase ceramic filaments 失效
标题翻译：由多相陶瓷丝制成的纤维整体料
公开(公告)号：US07452837B2
公开(公告)日：2008-11-18
申请号：US10275537
申请日：2001-01-22
申请人： Kenneth C. Goretta , Dileep Singh , Bryant J. Polzin , Terry Cruse , John J. Picciolo
发明人： Kenneth C. Goretta , Dileep Singh , Bryant J. Polzin , Terry Cruse , John J. Picciolo
IPC分类号： C04B35/00
CPC分类号： C04B35/632 , B28B3/2636 , B29C47/0014 , B29C47/003 , B29C47/0066 , B29C47/02 , B29C47/065 , B29C47/128 , B29K2309/02 , B29L2031/731 , C04B35/10 , C04B35/16 , C04B35/185 , C04B35/6264 , C04B35/62849 , C04B35/62852 , C04B35/63 , C04B35/634 , C04B35/638 , C04B35/80 , C04B35/803 , C04B2235/3217 , C04B2235/3246 , C04B2235/3463 , C04B2235/5224 , C04B2235/5228 , C04B2235/5232 , C04B2235/5236 , C04B2235/5268 , C04B2235/6021 , C04B2235/80 , C04B2235/96 , C04B2235/9607 , Y10S264/19 , Y10S264/26 , Y10T428/249929
摘要： A method for producing composite ceramic material is provided wherein a core ceramic structure is produced and simultaneously enveloped with a sleeve of similar material.
摘要翻译：提供一种制造复合陶瓷材料的方法，其中制造核心陶瓷结构并且同时被类似材料的套管包围。

10. 发明授权

US06974070B2 Joining of advanced materials by superplastic deformation 失效
标题翻译：通过超塑性变形连接先进材料
公开(公告)号：US06974070B2
公开(公告)日：2005-12-13
申请号：US09924571
申请日：2001-08-07
申请人： Kenneth C. Goretta , Jules L. Routbort , Felipe Gutierrez-Mora
发明人： Kenneth C. Goretta , Jules L. Routbort , Felipe Gutierrez-Mora
IPC分类号： B23K35/00 , B23K35/30 , C03C27/06 , C04B35/119 , C04B35/488 , C04B37/00 , C09J5/06 , B23K31/02
CPC分类号： C09J5/06 , B23K35/001 , B23K35/3046 , B23K2103/16 , B32B2309/12 , B32B2315/02 , C03C27/06 , C04B35/10 , C04B35/119 , C04B35/4885 , C04B35/5626 , C04B35/6268 , C04B37/001 , C04B37/003 , C04B37/005 , C04B37/006 , C04B2235/3206 , C04B2235/3217 , C04B2235/3222 , C04B2235/3246 , C04B2235/3279 , C04B2235/3826 , C04B2235/3839 , C04B2235/3843 , C04B2235/5276 , C04B2235/5292 , C04B2235/80 , C04B2237/064 , C04B2237/068 , C04B2237/123 , C04B2237/343 , C04B2237/348 , C04B2237/36
摘要： A method for utilizing superplastic deformation with or without a novel joint compound that leads to the joining of advanced ceramic materials, intermetallics, and cermets. A joint formed by this approach is as strong as or stronger than the materials joined. The method does not require elaborate surface preparation or application techniques.
摘要翻译：一种利用具有或不具有导致先进陶瓷材料，金属间化合物和金属陶瓷的接合的新型接合化合物的超塑性变形的方法。通过这种方法形成的接头与所连接的材料一样强或者强。该方法不需要精细的表面处理或应用技术。

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