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1. 发明授权

US07728180B2 Method for producing ethers 失效
标题翻译：醚的制备方法
公开(公告)号：US07728180B2
公开(公告)日：2010-06-01
申请号：US11628865
申请日：2005-06-08
申请人： Jin Tokuyasu , Taketoshi Okuno , Takashi Hori , Hideharu Iwasaki
发明人： Jin Tokuyasu , Taketoshi Okuno , Takashi Hori , Hideharu Iwasaki
IPC分类号： C07C41/06
CPC分类号： B01J31/24 , B01J31/0212 , B01J31/1805 , B01J2231/20 , B01J2531/824 , C07C41/06 , C07C43/15
摘要： A method for producing ethers comprises the following steps:initiating telomerization process of a conjugated diene compound with an hydroxyl compound represented by the following formula (I): R1OH (I) in the presence of a palladium compound, a tertiary isocyanide represented by the following formula (II): R2NC (II), and a base; and adding halfway through the telomerization process a tertiary phosphine represented by the following formula (III): PR3R4R5 (III) (the respective symbols are defined in the description).
摘要翻译：一种制备醚的方法包括以下步骤：使用下式（I）表示的羟基化合物引发共轭二烯化合物的调聚过程：R1OH（Ⅰ）在钯化合物存在下，以下列化合物表示的三异氰酸酯式（II）：R2NC（II）和碱; 并通过调聚过程中途加入由下式（III）表示的叔膦：PR3R4R5（III）（各符号在说明书中定义）。

2. 发明申请

US20080262272A1 Method For Producing Ethers 失效
标题翻译：生产醚的方法
公开(公告)号：US20080262272A1
公开(公告)日：2008-10-23
申请号：US11628865
申请日：2005-06-08
申请人： Jin Tokuyasu , Taketoshi Okuno , Takashi Hori , Hideharu Iwasaki
发明人： Jin Tokuyasu , Taketoshi Okuno , Takashi Hori , Hideharu Iwasaki
IPC分类号： C07C41/06
CPC分类号： B01J31/24 , B01J31/0212 , B01J31/1805 , B01J2231/20 , B01J2531/824 , C07C41/06 , C07C43/15
摘要： A method for producing ethers comprises the following steps:initiating telomerization process of a conjugated diene compound with an hydroxyl compound represented by the following formula (I): R1OH (I) in the presence of a palladium compound, a tertiary isocyanide represented by the following formula (II): R2NC (II) , and a base; andadding halfway through the telomerization process a tertiary phosphine represented by the following formula (III): PR3R4R5 (III) (the respective symbols are defined in the description).
摘要翻译：一种制备醚的方法包括以下步骤：使用下式（I）表示的羟基化合物引发共轭二烯化合物的调聚过程：<？在线式描述=“在线式”末端=“铅在钯化合物的存在下，“Ⅳ”表示“？”，“？”（I）通过下面的公式（II）：<？in-line-formula description =“In-line formula”end =“lead”？> R＆lt; 2＆gt; NC（II） description =“In-Line Formulas”end =“tail”？>，和base; 并且通过调聚过程中途加入由下式（III）表示的叔膦：<？in-line-formula description =“In-line Formulas”end =“lead”？> PR 3 （3）式（3）式（3）式中，“-in-line-formula”=“在线公式”end =“tail”→（各自的符号定义在说明）。

3. 发明授权

US06541575B2 Process for producing an epoxidized polymer 失效
公开(公告)号：US06541575B2
公开(公告)日：2003-04-01
申请号：US10024240
申请日：2001-12-21
申请人： Taketoshi Okuno , Hideharu Iwasaki , Takuo Tsuruta
发明人： Taketoshi Okuno , Hideharu Iwasaki , Takuo Tsuruta
IPC分类号： C08F808
CPC分类号： C08C19/06 , C08F8/08 , C08F297/046
摘要： According to the present invention, provided is an industrially advantageous process for producing an epoxidized polymer, with safety and efficiency, wherein the epoxidation of a polymer having an olefinic carbon-carbon double bond is effected under the presence of substantially no alkali metal ion by adding an aqueous solution containing (i) ammonium tungstate and/or tungstophosphoric acid and (ii) phosphoric acid, in which the amount of (ii) phosphoric acid is not less than 0.25 moles relative to 1 gram atom of tungsten atom contained in the (i) ammonium tungstate and/or tungstophosphoric acid, and an aqueous hydrogen peroxide, separately to a solution of said polymer and a quaternary ammonium salt in an organic solvent immiscible with water.

4. 发明授权

US07842843B2 Mixture containing 1,3-butadiene and process for producing the same 失效
标题翻译：含有1,3-丁二烯的混合物及其制备方法
公开(公告)号：US07842843B2
公开(公告)日：2010-11-30
申请号：US11564583
申请日：2006-11-29
申请人： Jin Tokuyasu , Hideharu Iwasaki
发明人： Jin Tokuyasu , Hideharu Iwasaki
IPC分类号： C07C41/06
CPC分类号： C10G63/04 , B01J23/78 , C07C7/163 , C07C11/08 , C07C11/167 , C07C41/06 , C10G45/00 , C07C43/15
摘要： To provide a C4 fraction that contains significantly reduced amounts of butynes and methylallene and to provide a process for low-cost and effective production of ethers in which the C4 fraction is used as the starting material for a telomerization process.A mixture containing 25 to 80 mass % 1,3-butadiene, 13 to 68 mass % butenes and 2 to 15 mass % butanes with butynes and methylallene being contained in amounts of 50 ppm or less and 5 to 800 ppm, respectively.
摘要翻译：提供含有显着降低量的丁炔和甲基亚甲基的C4级分，并提供一种低成本和有效生产醚的方法，其中C4馏分用作调聚过程的起始原料。含有25〜80质量％的1,3-丁二烯，13〜68质量％丁烯和2〜15质量％丁烷的丁酸酯和甲基铝的混合物的含量分别为50ppm以下且5〜800ppm。

5. 发明申请

US20090259073A1 METHOD FOR PRODUCING ALDEHYDE USING BISPHOSPHITE AND GROUP 8-10 METAL COMPOUND, AND SUCH BISPHOSPHITE 有权
标题翻译：使用双磷酸盐和第8-10族金属化合物生产二氢呋喃的方法和这种双磷酸盐
公开(公告)号：US20090259073A1
公开(公告)日：2009-10-15
申请号：US12295874
申请日：2007-04-03
申请人： Takashi Sugioka , Jin Tokuyasu , Takuo Tsuruta , Hideharu Iwasaki
发明人： Takashi Sugioka , Jin Tokuyasu , Takuo Tsuruta , Hideharu Iwasaki
IPC分类号： C07F9/06 , C07C45/49
CPC分类号： B01J31/185 , B01J2231/321 , B01J2531/80 , B01J2531/822 , C07C45/49 , C07C45/50 , C07F9/65746 , C07C47/277
摘要： A bisphosphite represented by the general formula (I): General Formula (I) (in the formula, A represents an alkylene group which may have a substituent, a cycloalkylene group which may have a substituent, a phenylene group which may have a substituent, or a naphthylene group which may have a substituent; and R1 represents a hydrogen atom or an alkyl group) and a method for producing an aldehyde including reacting a non-conjugated diene having a carbon-carbon double bond in a molecular end and having from 6 to 20 carbon atoms with a carbon monoxide and hydrogen in the presence of such a bisphosphite and a group 8 to 10 metal compound, are provided.
摘要翻译：由通式（I）表示的双亚磷酸酯：通式（I）（式中，A表示可以具有取代基的亚烷基，可以具有取代基的亚环烷基，可以具有取代基的亚苯基，或可以具有取代基的亚萘基; R 1表示氢原子或烷基），以及制备醛的方法，包括在分子末端使具有碳 - 碳双键的非共轭二烯与6 在这种二亚磷酸酯和8-10族金属化合物的存在下，使用一氧化碳和氢气使碳原子数为20的碳原子。

6. 发明授权

US07745666B2 Method for producing aldehyde using bisphosphite and group 8-10 metal compound, and such bisphosphite 有权
标题翻译：使用双亚磷酸酯和第8-10族金属化合物生产醛的方法和这种双亚磷酸酯
公开(公告)号：US07745666B2
公开(公告)日：2010-06-29
申请号：US12295874
申请日：2007-04-03
申请人： Takashi Sugioka , Jin Tokuyasu , Takuo Tsuruta , Hideharu Iwasaki
发明人： Takashi Sugioka , Jin Tokuyasu , Takuo Tsuruta , Hideharu Iwasaki
IPC分类号： C07C45/50 , C07F9/02
CPC分类号： B01J31/185 , B01J2231/321 , B01J2531/80 , B01J2531/822 , C07C45/49 , C07C45/50 , C07F9/65746 , C07C47/277
摘要： A bisphosphite represented by the general formula (I):General Formula (I) (in the formula, A represents an alkylene group which may have a substituent, a cycloalkylene group which may have a substituent, a phenylene group which may have a substituent, or a naphthylene group which may have a substituent; and R1 represents a hydrogen atom or an alkyl group) and a method for producing an aldehyde including reacting a non-conjugated diene having a carbon-carbon double bond in a molecular end and having from 6 to 20 carbon atoms with a carbon monoxide and hydrogen in the presence of such a bisphosphite and a group 8 to 10 metal compound, are provided.
摘要翻译：由通式（I）表示的双亚磷酸酯：通式（I）（式中，A表示可以具有取代基的亚烷基，可以具有取代基的亚环烷基，可以具有取代基的亚苯基，或可以具有取代基的亚萘基; R 1表示氢原子或烷基），以及制备醛的方法，包括在分子末端使具有碳 - 碳双键的非共轭二烯与6 在这种二亚磷酸酯和8-10族金属化合物的存在下，使用一氧化碳和氢气使碳原子数为20的碳原子。

7. 发明申请

US20070123738A1 MIXTURE CONTAINING 1,3-BUTADIENE AND PROCESS FOR PRODUCING THE SAME 失效
标题翻译：含有1,3-丁二烯的混合物及其制造方法
公开(公告)号：US20070123738A1
公开(公告)日：2007-05-31
申请号：US11564583
申请日：2006-11-29
申请人： Jin TOKUYASU , Hideharu Iwasaki
发明人： Jin TOKUYASU , Hideharu Iwasaki
IPC分类号： C07C41/06 , C07C11/00 , C07C9/00 , C07C2/00
CPC分类号： C10G63/04 , B01J23/78 , C07C7/163 , C07C11/08 , C07C11/167 , C07C41/06 , C10G45/00 , C07C43/15
摘要： To provide a C4 fraction that contains significantly reduced amounts of butynes and methylallene and to provide a process for low-cost and effective production of ethers in which the C4 fraction is used as the starting material for a telomerization process. A mixture containing 25 to 80 mass % 1,3-butadiene, 13 to 68 mass % butenes and 2 to 15 mass % butanes with butynes and methylallene being contained in amounts of 50 ppm or less and 5 to 800 ppm, respectively
摘要翻译：提供含有显着降低量的丁炔和甲基亚甲基的C4级分，并提供一种低成本和有效生产醚的方法，其中C4馏分用作调聚过程的起始原料。含有25〜80质量％的1,3-丁二烯，13〜68质量％的丁烯和2〜15质量％的丁烷和丁酸的甲烷的混合物的含量分别为50ppm以下且5〜800ppm

8. 发明授权

US08188299B2 Acrylate derivatives, alcohol derivatives, and method for producing them 有权
标题翻译：丙烯酸酯衍生物，醇衍生物及其制备方法
公开(公告)号：US08188299B2
公开(公告)日：2012-05-29
申请号：US12884677
申请日：2010-09-17
申请人： Kazuya Shimizu , Masayoshi Yamanaka , Tatsuhiko Hayashibara , Hideharu Iwasaki
发明人： Kazuya Shimizu , Masayoshi Yamanaka , Tatsuhiko Hayashibara , Hideharu Iwasaki
IPC分类号： C07D209/56
CPC分类号： C07D209/02 , C07D491/18
摘要： Provided are an acrylate derivative useful as a raw material of a polymer compound for resist compositions capable of giving resist patterns which are excellent in lithographic performance and have a good shape, an intermediate thereof (alcohol derivative) and production processes for them. To be specific, it is an acrylate derivative represented by a formula shown below: (wherein R1 represents a hydrogen atom, methyl or trifluoromethyl; R2, R3, R5, R7, R8, R9 and R10 each represent independently a hydrogen atom, an alkyl group having 1 to 6 carbon atoms, a cycloalkyl group having 3 to 6 carbon atoms or an alkoxy group having 1 to 6 carbon atoms; R4 and R6 each represent independently a hydrogen atom, an alkyl group having 1 to 6 carbon atoms, a cycloalkyl group having 3 to 6 carbon atoms or an alkoxy group having 1 to 6 carbon atoms, or both of R4 and R6 are combined to represent an alkylene group having 1 to 3 carbon atoms, —O— or —S—; and R11 represents a hydrogen atom, an alkyl group having 1 to 6 carbon atoms or a cyclic hydrocarbon group having 3 to 10 carbon atoms).
摘要翻译：提供可用作抗蚀剂组合物的聚合物化合物的原料的丙烯酸酯衍生物，其能够提供平版印刷性能优异且形状良好的抗蚀剂图案，其中间体（醇衍生物）及其制备方法。具体来说，它是由下式表示的丙烯酸酯衍生物：其中R1表示氢原子，甲基或三氟甲基; R2，R3，R5，R7，R8，R9和R10各自独立地表示氢原子，烷基具有1至6个碳原子的基团，具有3至6个碳原子的环烷基或具有1至6个碳原子的烷氧基; R 4和R 6各自独立地表示氢原子，具有1至6个碳原子的烷基，环烷基具有3至6个碳原子的烷基或具有1至6个碳原子的烷氧基，或者R 4和R 6都被结合以表示具有1至3个碳原子的亚烷基，-O-或-S-; R 11表示氢原子，碳原子数1〜6的烷基或碳原子数3〜10的环状烃基）。

9. 发明授权

US08110124B2 Method of preparing fluorescent body precursor 有权
标题翻译：制备荧光体前体的方法
公开(公告)号：US08110124B2
公开(公告)日：2012-02-07
申请号：US12373989
申请日：2007-07-26
申请人： Yoshihisa Tsuji , Hideharu Iwasaki
发明人： Yoshihisa Tsuji , Hideharu Iwasaki
IPC分类号： C09K11/56
CPC分类号： C09K11/7702 , C01G9/00 , C01G9/006 , C01G9/08 , C01G45/006 , C01G45/02 , C01P2002/52 , C01P2002/72 , C01P2006/80 , C09K11/574 , C09K11/876
摘要： To produce fluorescent bodies providing high brightness and high energy efficiency, a method of preparing a fluorescent body precursor is provided to enable an activator having a large ionic radius to be doped arbitrarily. The problems described above are solved by a method of preparing a fluorescent body precursor, which method is characterized by comprising applying a shock pressure of 0.1 GPa or higher to a mixture consisting essentially of a fluorescent body base, an activator and a co-activating particle-growth promoter to dope the activator into the fluorescent body base in the presence of the co-activating particle-growth promoter.
摘要翻译：为了产生提供高亮度和高能量效率的荧光体，提供了制备荧光体前体的方法，以使得具有大离子半径的活化剂能够被任意掺杂。上述问题是通过制备荧光体前体的方法来解决的，该方法的特征在于包括对基本上由荧光体碱，活化剂和共活化颗粒组成的混合物施加0.1GPa或更高的冲击压力生长促进剂，在共活化的颗粒生长促进剂存在下将活化剂掺入荧光体碱中。

10. 发明申请

US20110147663A1 METHOD FOR PRODUCING ZINC SULFIDE BASED PHOSPHOR 失效
标题翻译：生产基于硫化锌的磷光体的方法
公开(公告)号：US20110147663A1
公开(公告)日：2011-06-23
申请号：US13057168
申请日：2009-07-30
申请人： Yoshihisa Tsuji , Kazuma Inoue , Jun Takai , Hideharu Iwasaki
发明人： Yoshihisa Tsuji , Kazuma Inoue , Jun Takai , Hideharu Iwasaki
IPC分类号： C09K11/56
CPC分类号： C09K11/625 , C09K11/876 , H05B33/14
摘要： The present invention provides a method for producing a zinc sulfide based phosphor by firing a zinc sulfide based phosphor precursor, comprising at least: a first firing step of firing a mixture containing a zinc sulfide based phosphor precursor, sulfur, and a chlorine-containing flux; and a second firing step of further firing the fired product obtained from the first firing step, wherein the first firing step comprises: heating the mixture in an atmosphere wherein an air stream is introduced so that a temperature of the mixture is increased from normal temperature to a transformation temperature at which a crystal system of the phosphor precursor is transformed; when a temperature of the mixture is increased above the transformation temperature, switching the atmosphere to a nitrogen atmosphere and continuing the heating of the mixture; and when the temperature of the mixture reaches a temperature in a range of 1000° C. to 1200° C., inclusive, maintaining the temperature of the mixture at a constant level and thereafter rapidly quenching the mixture and washing the mixture to obtain a fired product; and wherein the second firing step comprises heating in the nitrogen atmosphere the fired product obtained from the first firing step so that the temperature of the fired product is increased from normal temperature to a temperature in a range of 650° C. to 1000° C., inclusive; and when a temperature of the fired product reaches the temperature in the range of 650° C. to 1000° C., inclusive, introducing oxygen while maintaining the temperature of the fired product and thereafter rapidly quenching the fired product and washing the fired product to obtain a zinc sulfide based phosphor. Use of the method of the present invention makes it possible to provide a zinc sulfide based phosphor material suitable for use in the production of an EL device that shows high brightness.
摘要翻译：本发明提供了一种通过焙烧硫化锌系荧光体前体来制造硫化锌系荧光体的方法，该方法至少包括：将含有硫化锌系荧光体前体，硫和含氯助熔剂的混合物进行烧成的第一烧成工序 ; 以及第二烧成工序，对从所述第一烧成工序得到的烧成品进一步进行烧成，其中，所述第一烧成工序包括：在导入空气流的气氛中加热所述混合物，使得所述混合物的温度从常温升高到改变荧光体前体的晶体体系的相变温度; 当混合物的温度升高到转化温度以上时，将气氛切换至氮气氛并继续加热混合物; 并且当混合物的温度达到1000℃至1200℃的范围内的温度时，将混合物的温度保持在恒定水平，然后快速骤冷混合物并洗涤该混合物以获得烧制产品; 并且其中所述第二烧制步骤包括在所述氮气气氛中加热从所述第一烧制步骤获得的烧制产品，使得所述烧制产品的温度从常温升高至650℃至1000℃的温度。，包括的; 并且当烧制品的温度达到650℃至1000℃的温度时，在保持烧制产品的温度的同时引入氧气，然后迅速骤冷烧制产品并将烧制产品洗涤至得到硫化锌系荧光体。通过使用本发明的方法，可以提供一种适用于制造高亮度的EL器件的硫化锌系荧光体材料。

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