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1. 发明授权

US06268444B1 3-heteroatom substituted cyclopentadienyl-containing metal complexes and olefin polymerization process 有权
标题翻译：含3-杂原子取代的环戊二烯基金属络合物和烯烃聚合方法
公开(公告)号：US06268444B1
公开(公告)日：2001-07-31
申请号：US09230185
申请日：1999-01-15
申请人： Jerzy Klosin , William J. Kruper, Jr. , Peter N. Nickias , Jasson T. Patton , David R. Wilson
发明人： Jerzy Klosin , William J. Kruper, Jr. , Peter N. Nickias , Jasson T. Patton , David R. Wilson
IPC分类号： C08F416
CPC分类号： C07F17/00 , C07F7/10 , C08F4/65908 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F10/00 , C08F210/16 , C08F2420/02 , Y10S526/943 , C08F210/14 , C08F2500/12
摘要： This invention relates to heteroatom substituted cyclopentadienyl-containing ligands, metal complexes containing these ligands, catalyst systems prepared from catalyst components comprising these metal complexes. The metal complexes contain a “a” heteroatom-Cp bond or a ring heteroatom-Cp bond in the 3-position of the Cp. In preferred metal complexes the ligand is a 3-heteroatom substituted indenyl group. The catalyst systems for olefin polymerization may be used at high temperatures, are highly active and produce high molecular weight polymer.
摘要翻译：本发明涉及含杂原子取代的含环戊二烯基的配位体，含有这些配体的金属络合物，由包含这些金属络合物的催化剂组分制备的催化剂体系金属络合物在Cp的3位上含有“a”个杂原子-Cp键或环杂原子-Cp键。在优选的金属络合物中，配体是3-杂原子取代的茚基。用于烯烃聚合的催化剂体系可以在高温下使用，高活性并且产生高分子量聚合物。

2. 发明授权

US6140521A Ansa group 4 metal bis (.mu.-substituted) aluminum complexes 失效
标题翻译： Ansa组4金属双（μ-取代）铝络合物
公开(公告)号：US6140521A
公开(公告)日：2000-10-31
申请号：US330672
申请日：1999-06-11
申请人： Eugene Y. Chen , William J. Kruper, Jr. , Peter N. Nickias , David R. Wilson
发明人： Eugene Y. Chen , William J. Kruper, Jr. , Peter N. Nickias , David R. Wilson
IPC分类号： C07F5/06 , C07F7/10 , C07F7/28 , C07F17/00 , C07F19/00 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00 , C07F7/00 , C08F4/64
CPC分类号： C08F10/00 , C07F17/00 , C07F5/066 , C08F210/16 , C08F4/65908 , C08F4/6592 , C08F4/65927 , Y10S526/943
摘要： Ansa bis(.mu.-substituted) Group 4 metal and aluminum compounds comprising a single Group 4 metal atom and two aluminum metal atoms corresponding to the formula: ##STR1## wherein: L' is a .pi.-bonded group,M is a Group 4 metal,J is nitrogen or phosphorus;Z is a divalent bridging group causing the complex to have an ansa structure,R' is an inert monovalent ligand;r is one or two;X independently each occurrence is a Lewis basic ligand group able to form a .mu.-bridging ligand group, and optionally the two X groups may be joined together, andA' independently each occurrence is an aluminum containing Lewis acid compound that forms an adduct with the metal complex by means of the .mu.-bridging groups, and optionally two A' groups may be joined together thereby forming a single difunctional Lewis acid containing compound, and a method of preparation comprising contacting a charge-neutral Group IV metal coordination complex having at least two Lewis basic groups with at least two molar equivalents of charge-neutral aluminum coordination complexes having Lewis acidic aluminum atoms such that at least two of the aluminum atoms of the aluminum coordination complexes bond to at least two of the Lewis basic groups of the Group IV coordination complex.
摘要翻译： Ansa双（μ-取代的）第4族金属和铝化合物，其包含对应于下式的单个第4族金属原子和两个铝金属原子：其中：L'是π键合基团，M是第4族金属，J是氮或磷; Z是使络合物具有ansa结构的二价桥连基团，R'是惰性单价配体; r是一两个; 独立地，X独立地是能够形成mu-桥接配体基团的路易斯碱性配体基团，并且任选地两个X基团可以连接在一起，并且A'独立地是含铝的路易斯酸化合物，其与金属络合物，并且任选地两个A'基团可以连接在一起，从而形成单一双官能路易斯酸化合物，以及制备方法，包括使具有至少一个电荷的中性IV族金属配位络合物两个路易斯碱性基团，其具有至少两摩尔当量的具有路易斯酸性铝原子的电荷 - 中性铝配位络合物，使得铝配位络合物的至少两个铝原子与至少两个第IV族的路易斯碱性基团键合协调综合体

3. 发明授权

US6136993A Integrated process for preparation of diene complexes 有权
公开(公告)号：US6136993A
公开(公告)日：2000-10-24
申请号：US420625
申请日：1999-10-20
申请人： Eugene Y. Chen , Richard E. Campbell, Jr. , David D. Devore , D. Patrick Green , Jasson T. Patton , Jorge Soto , David R. Wilson
发明人： Eugene Y. Chen , Richard E. Campbell, Jr. , David D. Devore , D. Patrick Green , Jasson T. Patton , Jorge Soto , David R. Wilson
IPC分类号： C07F7/00 , C07F7/08 , C07F9/50 , C07F17/00 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00
CPC分类号： C07F17/00 , C07F7/00 , C07F7/082 , C07F9/5045 , Y02P20/125 , Y10S526/943
摘要： Disclosed is a process for preparing bridged Group 4 metal complexes containing a neutral diene ligand starting from the corresponding novel, metal diene containing complexes by reaction thereof with the divalent derivative of a bridged bidentate ligand compound. The novel, intermediate metal diene complexes, their formation from tetravalent metal salts and an integrated process combining both process steps are claimed.

4. 发明授权

US6127563A Integrated process for preparation of diene complexes 有权
标题翻译：二烯配合物的制备方法
公开(公告)号：US6127563A
公开(公告)日：2000-10-03
申请号：US420626
申请日：1999-10-20
申请人： Eugene Y. Chen , David D. Devore , Richard E. Campbell, Jr. , D. Patrick Green , Jasson T. Patton , Jorge Soto , David R. Wilson
发明人： Eugene Y. Chen , David D. Devore , Richard E. Campbell, Jr. , D. Patrick Green , Jasson T. Patton , Jorge Soto , David R. Wilson
IPC分类号： C07F7/00 , C07F7/08 , C07F9/50 , C07F17/00 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00 , C07F9/02
CPC分类号： C07F17/00 , C07F7/00 , C07F7/082 , C07F9/5045 , Y02P20/125 , Y10S526/943
摘要： Disclosed is a process for preparing bridged Group 4 metal complexes containing a neutral diene ligand starting from the corresponding novel, metal diene containing complexes by reaction thereof with the divalent derivative of a bridged bidentate ligand compound. The novel, intermediate metal diene complexes, their formation from tetravalent metal salts and an integrated process combining both process steps are claimed.
摘要翻译：公开了一种通过与桥连二齿配位体化合物的二价衍生物反应制备含有中性二烯配体的桥连的第4族金属配合物的方法，其起始于相应的新型含金属二烯复合物。所述的新型中间体金属二烯络合物，它们由四价金属盐的形成以及组合两个工艺步骤的一体化方法。

5. 发明授权

US06284698B1 Highly activated bimetallic complexes and polymerization process 有权
标题翻译：高活性双金属络合物和聚合过程
公开(公告)号：US06284698B1
公开(公告)日：2001-09-04
申请号：US09528787
申请日：2000-03-17
申请人： Eugene Y. Chen , Shaoguang S. Feng , David D. Graf , Jasson T. Patton , David R. Wilson
发明人： Eugene Y. Chen , Shaoguang S. Feng , David D. Graf , Jasson T. Patton , David R. Wilson
IPC分类号： B01J3100
CPC分类号： C07F17/00 , C08F4/65908 , C08F4/65912 , C08F10/00 , C08F2410/03 , C08F4/6592
摘要： Catalyst compositions comprising 1) one or more bimetallic Group 3-6 or Lanthanide metal complexes corresponding to the formula: wherein: M and M′ are independently Group 3, 4, 5, 6, or Lanthanide metals; L is a divalent group (or trivalent group if bound to Q) having up to 50 nonhydrogen atoms and containing an aromatic &pgr;-system through which the group is bound to M, said L also being bound to Z; L′ is a monovalent group or a divalent group (if bound to L″ or Q), or a trivalent group (if bound to both L″ and Q) having up to 50 nonhydrogen atoms and containing an aromatic &pgr;-system through which the group is bound to M′; L″ is a monovalent group or a divalent group (if bound to L′ or Q), or a trivalent group (if bound to both L′ and Q) having up to 50 nonhydrogen atoms and containing an aromatic &pgr;-system through which the group is bound to M′, or L″ is a moiety comprising boron or a member of Group 14 of the Periodic Table of the Elements, and optionally also comprising nitrogen, phosphorus, sulfur or oxygen, said L″ having up to 20 non-hydrogen atoms; Z is a moiety comprising boron or a member of Group 14 of the Periodic Table of the Elements, and also comprising nitrogen, phosphorus, sulfur or oxygen, said Z having up to 20 non-hydrogen atoms; X, X′ and X″ are as defined in the specification; Q is a divalent anionic ligand group bound at one terminus to either Z or L and bound at the remaining terminus to either L′ or L″, said Q having up to 20 nonhydrogen atoms; and x, x′, and x″ are independently integers from 0 to 3; and 2) one or more activating cocatalysts; wherein activating cocatalyst component 2) causes both metal centers, M and M′, of the one or more bimetallic metal complexes 1) to be catalytically active for the polymerization of addition polymerizable monomers.
摘要翻译：催化剂组合物包含1）一种或多种对应于下式的双金属组3-6或镧系元素金属络合物：其中：M和M'独立地为第3,4,5,6族或镧系金属; L为二价基团（或三价基团如果结合Q）具有多达50个非氢原子并且含有基团与M结合的芳族π系统，所述L也与Z结合; L'是一价基团或二价基团（如果与 L“或Q）或三价基团（如果与L”和Q两者结合），其具有多达50个非氢原子并且含有该基团通过其与M'结合的芳族π系统; L“是一价基团或二价基团（如果与L'或Q键合）或三价基团（如果与L'和Q两者结合）具有多达50个非氢原子并含有芳族π-系统，通过该基团键合该基团 M'或L“是包含元素周期表第14族的硼或元素的部分，并且任选地也包含氮，磷所述L“具有多达20个非氢原子; Z是包含元素周期表第14族的硼或元素的部分，并且还包含氮，磷，硫或氧，所述Z具有至多20个非氢原子; X，X'和X“如说明书中所定义; Q是在一个末端与Z或L结合的二价阴离子配体基团，并在剩余的末端结合至 L'或L“，所述Q具有至多20个非氢原子; 和x，x'独立地为0至3的整数; 和2）一种或多种活化助催化剂;其中活化助催化剂组分2）使得一种或多种双金属金属络合物1）的金属中心M和M'两者对于可加聚单体的聚合具有催化活性。

6. 发明授权

US06084115A Diene complexes of group 4 metals and process of preparation 有权
标题翻译：第4族金属的二烯络合物及其制备方法
公开(公告)号：US06084115A
公开(公告)日：2000-07-04
申请号：US265641
申请日：1999-03-10
申请人： Eugene Y. Chen , Richard E. Campbell, Jr. , David D. Devore , D. Patrick Green , Jasson T. Patton , Jorge Soto , David R. Wilson
发明人： Eugene Y. Chen , Richard E. Campbell, Jr. , David D. Devore , D. Patrick Green , Jasson T. Patton , Jorge Soto , David R. Wilson
IPC分类号： C07F7/00 , C07F7/08 , C07F9/50 , C07F17/00 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00 , C07F9/02
CPC分类号： C07F17/00 , C07F7/00 , C07F7/082 , C07F9/5045 , Y02P20/125 , Y10S526/943
摘要： Disclosed is a process for preparing bridged Group 4 metal complexes containing a neutral diene ligand starting from the corresponding novel, metal diene containing complexes by reaction thereof with the divalent derivative of a bridged bidentate ligand compound. The novel, intermediate metal diene complexes, their formation from tetravalent metal salts and an integrated process combining both process steps are claimed.
摘要翻译：公开了一种通过与桥连二齿配位体化合物的二价衍生物反应制备含有中性二烯配体的桥连的第4族金属配合物的方法，其起始于相应的新型含金属二烯复合物。所述的新型中间体金属二烯络合物，它们由四价金属盐的形成以及组合两个工艺步骤的一体化方法。

7. 发明授权

US5543480A Polymerization process using diene containing catalysts 失效
标题翻译：使用含二烯催化剂的聚合方法
公开(公告)号：US5543480A
公开(公告)日：1996-08-06
申请号：US267991
申请日：1994-06-28
申请人： Jasson T. Patton , David D. Devore , Francis J. Timmers , Jorge Soto , Gregory F. Schmidt , David R. Wilson
发明人： Jasson T. Patton , David D. Devore , Francis J. Timmers , Jorge Soto , Gregory F. Schmidt , David R. Wilson
IPC分类号： C08F4/642 , C08F4/64 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F12/00
CPC分类号： C08F10/00 , C08F4/65908 , C08F4/65912 , C08F4/65916 , C08F4/6592
摘要： Compositions comprising Group 4 metal complexes containing a diene moiety and activating cocatalysts are used as catalysts for polymerizing olefins, diolefins and/or acetylenically unsaturated monomers. Vinylidene aromatic monomers, particularly styrene are polymerized to form highly syndiotactic polymers.
摘要翻译：包含含有二烯部分的第4族金属络合物和活化助催化剂的组合物用作聚合烯烃，二烯烃和/或炔属不饱和单体的催化剂。将亚乙烯基芳族单体，特别是苯乙烯聚合以形成高度间同立构聚合物。

8. 发明申请

US20090149561A1 EXTRUDED POLYMER FOAMS CONTAINING BROMINATED 2-OXO-1,3,2-DIOXAPHOSPHORINANE COMPOUNDS AS FLAME RETARDANT ADDITIVES 审中-公开
标题翻译：含有作为阻燃添加剂的2-氧代-1,3-二氧杂环己烷化合物的挤出聚合物
公开(公告)号：US20090149561A1
公开(公告)日：2009-06-11
申请号：US12331856
申请日：2008-12-10
申请人： Anteneh Z. Worku , William G. Stobby , Sheila M. Tinetti , Inken Beulich , David R. Wilson , Duane R. Romer , James P. Godschalx , Nelson G. Rondan , William J. Kruper, JR. , Ted A. Morgan
发明人： Anteneh Z. Worku , William G. Stobby , Sheila M. Tinetti , Inken Beulich , David R. Wilson , Duane R. Romer , James P. Godschalx , Nelson G. Rondan , William J. Kruper, JR. , Ted A. Morgan
IPC分类号： C08J9/35
CPC分类号： C08J9/0038 , C08J9/12 , C08J2201/03 , C08J2325/04
摘要： Extruded polymer foams are prepared using 5,5-bis(bromomethyl)-2-oxo-1,3,2-dioxaphosphorinane or brominated 2-oxo-1,3,2-dioxaphosphorinane compounds. The brominated FR additives unexpectedly are stable at the extrusion temperatures, and provide excellent flame retardancy to the foams.
摘要翻译：使用5,5-双（溴甲基）-2-氧代-1,3,2-二氧杂磷杂环己烷或溴化2-氧代-1,3,2-二氧杂磷杂环己烷化合物制备挤出的聚合物泡沫体。溴化FR添加剂在挤出温度下出人意料地稳定，并且对泡沫具有优异的阻燃性。

9. 发明授权

US08574773B2 Battery electrolyte solutions containing aromatic phosphorus compounds 有权
标题翻译：含有芳香族磷化合物的电池电解液
公开(公告)号：US08574773B2
公开(公告)日：2013-11-05
申请号：US13132374
申请日：2009-11-16
申请人： David R. Wilson , Ravi B. Shankar , Houxiang Tang , Andrew J. Pasztor, Jr. , Peter M. Margl , William J. Kruper, Jr. , Mark D. Newsham , Jing Jin , Matthew M. Yonkey , Deidre A. Strand , Thomas D. Gregory , Jamie L. Cohen , Jeremy R. Stajdl
发明人： David R. Wilson , Ravi B. Shankar , Houxiang Tang , Andrew J. Pasztor, Jr. , Peter M. Margl , William J. Kruper, Jr. , Mark D. Newsham , Jing Jin , Matthew M. Yonkey , Deidre A. Strand , Thomas D. Gregory , Jamie L. Cohen , Jeremy R. Stajdl
IPC分类号： H01M10/0567 , H01M10/052
CPC分类号： H01M10/0567 , H01M6/168 , H01M10/052 , H01M10/4235 , H01M2300/0025 , Y02T10/7011
摘要： A battery electrolyte solution contains from 0.01 to 80% by weight of an aromatic phosphorus compound. The aromatic phosphorus compound provides increased thermal stability for the electrolyte, helping to reduce thermal degradation, thermal runaway reactions and the possibility of burning. The aromatic phosphorus compound has little adverse impact on the electrical properties of the battery, and in some cases actually improves battery performance.
摘要翻译：电池电解液含有0.01〜80重量％的芳香族磷化合物。芳族磷化合物为电解质提供了增加的热稳定性，有助于减少热降解，热失控反应和燃烧的可能性。芳香族磷化合物对电池的电气性能几乎没有不利影响，在某些情况下实际上提高了电池性能。

10. 发明授权

US09147906B2 Battery electrolyte solutions containing phosphorus-sulfur compounds 有权
标题翻译：含磷硫化合物的电池电解液
公开(公告)号：US09147906B2
公开(公告)日：2015-09-29
申请号：US13503369
申请日：2009-11-16
申请人： Houxiang Tang , William J. Kruper, Jr. , Ravi B. Shankar , Deidre A. Strand , Peter M. Margl , Andrew J. Pasztor, Jr. , David R. Wilson , Jeremy R. Stajdl
发明人： Houxiang Tang , William J. Kruper, Jr. , Ravi B. Shankar , Deidre A. Strand , Peter M. Margl , Andrew J. Pasztor, Jr. , David R. Wilson , Jeremy R. Stajdl
IPC分类号： H01M10/0567 , H01M6/16 , H01M10/052
CPC分类号： H01M10/0567 , H01M6/168 , H01M10/052 , H01M2300/0025 , Y02E60/122
摘要： A battery electrolyte solution contains from 0.001 to 20% by weight of certain phosphorus-sulfur compounds. The phosphorus-sulfur compound performs effectively as a solid-electrolyte interphase (SEI) forming material. The phosphorus-sulfur compound has little adverse impact on the electrical properties of the battery, and in some cases actually improves battery performance. Batteries containing the electrolyte solution form robust and stable SEIs even when charged at high rates during initial formation cycles.
摘要翻译：电池电解液含有0.001〜20重量％的某些硫 - 硫化合物。磷硫化合物作为固体 - 电解质间相（SEI）形成材料有效地进行。磷硫化合物对电池的电气性能几乎没有不利影响，并且在某些情况下实际上提高了电池性能。含有电解质溶液的电池即使在初始形成循环期间以高速率进行充电也能形成稳健且稳定的SEI。

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