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1. 发明专利

JP2014049352A Anion conductive electrolyte membrane and method for producing the same 有权
标题翻译：阴极导电电解质膜及其制造方法
公开(公告)号：JP2014049352A
公开(公告)日：2014-03-17
申请号：JP2012192620
申请日：2012-08-31
申请人： Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構 , Daihatsu Motor Co Ltd , ダイハツ工業株式会社
发明人： YOSHIMURA KIMIO , KOSHIKAWA HIROSHI , YAMAKI TETSUYA , ASANO MASAHARU , MAEKAWA YASUNARI , ITANI HIDEYUKI , ASAZAWA KOICHIRO , YAMAGUCHI SUSUMU , TANAKA HIROHISA
IPC分类号： H01M8/02 , C08F8/02 , C08F291/18 , C08J5/22 , H01B1/06 , H01B13/00 , H01M8/10
CPC分类号： C08F26/06 , B01D69/02 , B01D71/32 , B01D71/36 , B01D71/62 , B01D2323/385 , B01D2325/16 , B01D2325/42 , C08J5/2243 , H01M8/1023 , H01M2300/0082
摘要： PROBLEM TO BE SOLVED: To provide an anion conductive electrolyte membrane good in conductivity, water-containing properties and alkali resistance, and a method for producing the anion conductive electrolyte membrane.SOLUTION: A graft chain including an N-vinyl imidazole derivative is introduced in a polymer base material by radiation graft polymerization to produce an alkyl-substituted imidazolium salt through a reaction with alkyl halide. Accordingly, an anion conductive electrolyte membrane suppressed in a nucleophilic substitution reaction and an elimination reaction and having high alkali resistance can be obtained.
摘要翻译：要解决的问题：提供导电性，含水性和耐碱性良好的阴离子导电性电解质膜，以及阴离子导电性电解质膜的制造方法。解决方案：将包含N-乙烯基咪唑衍生物的接枝链引入聚合物基材通过辐射接枝聚合以通过与烷基卤反应产生烷基取代的咪唑鎓盐。因此，可以获得抑制亲核取代反应和消除反应并具有高耐碱性的阴离子导电电解质膜。

2. 发明专利

JP2012120991A Anion exchange membrane 有权
标题翻译：阴离子交换膜
公开(公告)号：JP2012120991A
公开(公告)日：2012-06-28
申请号：JP2010274554
申请日：2010-12-09
申请人： Daihatsu Motor Co Ltd , Japan Atomic Energy Agency , ダイハツ工業株式会社 , 独立行政法人日本原子力研究開発機構
发明人： YAMAMOTO KAZUYA , YAMADA KOJI , YAMAGUCHI SUSUMU , TANAKA HIROHISA , ASANO MASAHARU , YAMAKI TETSUYA , KOSHIKAWA HIROSHI , MAEKAWA YASUNARI , SINANANWANICH WARAPON
IPC分类号： B01J47/12 , C08F259/08 , H01M8/02 , H01M8/10
CPC分类号： H01M8/1041 , H01M8/0289 , H01M8/103 , H01M8/1039
摘要： PROBLEM TO BE SOLVED: To provide an anion exchange membrane that can achieve improvement in the durability while maintaining the membrane performance.SOLUTION: The anion exchange membrane includes a quaternary ammonium salt group in which two methyl groups, and one alkyl group having 3 to 8 carbon atoms are bonded to a nitrogen atom.
摘要翻译：要解决的问题：提供能够在保持膜性能的同时实现耐久性提高的阴离子交换膜。解决方案：阴离子交换膜包括其中两个甲基和一个具有3-8个碳原子的烷基与氮原子结合的季铵盐基团。版权所有（C）2012，JPO＆INPIT

3. 发明专利

JP2013186989A Anion conducting electrolyte membrane and method for producing the same 有权
标题翻译：阴极导电电解质膜及其制造方法
公开(公告)号：JP2013186989A
公开(公告)日：2013-09-19
申请号：JP2012049960
申请日：2012-03-07
申请人： Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構 , Daihatsu Motor Co Ltd , ダイハツ工業株式会社
发明人： YOSHIMURA KIMIO , KOSHIKAWA HIROSHI , YAMAKI TETSUYA , ASANO MASAHARU , MAEKAWA YASUNARI , ITANI HIDEYUKI , TANAKA HIROHISA , YAMAGUCHI SUSUMU , ASAZAWA KOICHIRO , YAMAMOTO KAZUYA , SANPEI FUMIHIRO
IPC分类号： H01M8/02 , C08J5/22 , C08J7/12 , C08J7/18 , H01B1/06 , H01B13/00 , H01M8/10
CPC分类号： H01M8/1018 , H01M8/1088 , Y02E60/521 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide: an anion conducting electrolyte membrane well-balanced in between electric conductivity and moisture content, and high in electric conductivity; and a method for producing the anion conducting electrolyte membrane.SOLUTION: A graft chain 2 including an alkyl halide group is introduced into a polymer base material 1 by radiation graft polymerization, the polymer base material comprising a fluorine polymer, an olefin polymer or an aromatic polymer which are excellent in mechanical characteristics and chemical stability at high temperatures, and a weakly basic quaternary ammonium salt 3 is introduced by a reaction between various amines with high basic strength (organic strong bases) and an alkyl halide section. Accordingly, an anion conducting electrolyte membrane having high electric conductivity and low moisture content can be obtained by the combination of a hydroxide ion that is the most weak acid and a stable weak acid-weak base group.
摘要翻译：要解决的问题：提供：在导电性和含水量之间良好平衡的阴离子导电电解质膜，并且导电性高; 和阴离子导电电解质膜的制造方法。解决方案：通过辐射接枝聚合将包含烷基卤基团的接枝链2引入聚合物基材1中，聚合物基材包含氟聚合物，烯烃聚合物或芳族在高温下机械特性和化学稳定性优异的聚合物和弱碱性季铵盐3通过具有高碱性强度的各种胺（有机强碱）和烷基卤化物部分之间的反应引入。因此，通过组合最弱弱酸的氢氧根离子和稳定的弱酸弱碱可以获得具有高导电性和低含水量的阴离子导电电解质膜。

4. 发明专利

JP2013235668A Proton-conductive polymer electrolyte membrane, method for producing the same, membrane/electrode assembly using the same, and fuel cell 审中-公开
标题翻译：导电聚合物电解质膜，其制造方法，使用其的膜/电极组件和燃料电池
公开(公告)号：JP2013235668A
公开(公告)日：2013-11-21
申请号：JP2012105856
申请日：2012-05-07
申请人： Nitto Denko Corp , 日東電工株式会社 , Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： KISHII YUTAKA , NISHII HIROYUKI , EMORI HIDEYUKI , HIGUCHI HIROYUKI , ASANO MASAHARU , MAEKAWA YASUNARI
IPC分类号： H01M8/02 , C08F259/08 , H01B1/06 , H01M8/10
CPC分类号： Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide a polymer electrolyte membrane which exhibits excellent proton conductivity even under low humidity, and a method for producing the same.SOLUTION: The polymer electrolyte membrane of the present invention is a proton-conductive polymer electrolyte membrane containing a first polymer and a second polymer. The first polymer is composed of a hydrophobic first main chain and a first side chain bonded to the first main chain. The second polymer is composed of a hydrophobic second main chain and a hydrophobic second side chain bonded to the second main chain. The first side chain has a proton-conductive moiety.
摘要翻译：要解决的问题：提供即使在低湿度下也显示出优异的质子传导性的聚合物电解质膜及其制造方法。本发明的高分子电解质膜是质子传导性高分子电解质膜，其含有第一聚合物和第二聚合物。第一聚合物由疏水性第一主链和与第一主链结合的第一侧链构成。第二聚合物由与第二主链结合的疏水性第二主链和疏水性第二侧链构成。第一侧链具有质子传导性部分。

5. 发明专利

JP2010182436A Polymer electrolyte membrane comprising alkylether graft chain, and method of producing the same 有权
标题翻译：包含碱金属链的聚合物电解质膜及其制造方法
公开(公告)号：JP2010182436A
公开(公告)日：2010-08-19
申请号：JP2009022352
申请日：2009-02-03
申请人： Japan Atomic Energy Agency , Kanagawa Univ , 学校法人神奈川大学 , 独立行政法人日本原子力研究開発機構
发明人： MAEKAWA YASUNARI , ENOMOTO KAZUYUKI , KIHARA NOBUHIRO
IPC分类号： H01M8/02 , C08J7/18 , H01B1/06 , H01B13/00 , H01M8/10
CPC分类号： H01M8/1039 , C08J7/18 , C08J2323/00 , C08J2327/12 , H01M8/1018 , H01M8/1023 , H01M8/1088 , Y02E60/521 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide an electrolyte membrane for use in a fuel cell having excellent proton conductivity, low water content, resistance to hot water, and fuel impermeability, which is more excellent than a conventional polymer electrolyte membrane, in particulr, an electrolyte membrane prepared by radiation-induced graft polymerization of a styrene monomer onto a polymer substrate, and a method of producing the same. SOLUTION: The method for producing the electrolyte membrane for use in a fuel cell includes processes of: performing radiation-induced graft polymerization of a vinyl monomer having a nucleophilic functional group selected from an acylvinyl ether derivative, a styrene derivative, and a methacrylic acid derivative, with a polymer substrate having a fluorine-containing polymer, an olefin-containing polymer, or an aromatic polymer; deprotecting an ester bond of a graft chain on the polymer substrate introduced by the radiation-induced graft polymerization; and introducing an alkylethersulfonic acid structure into the nucleophilic functional group of the graft chain thus deprotected, by use of an electrophilic reagent selected from cyclic sulfonic acid ester and alkylhalide sulfonate. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种用于燃料电池的电解质膜，其具有优异的质子传导性，低含水量，耐热水性和燃料不渗透性，其比常规聚合物电解质膜更优异，特别是，通过苯乙烯单体的辐射诱导接枝聚合制备在聚合物基材上的电解质膜及其制备方法。解决方案：用于生产用于燃料电池的电解质膜的方法包括以下步骤：对具有选自酰基乙烯基醚衍生物，苯乙烯衍生物和苯乙烯衍生物的亲核官能团的乙烯基单体进行辐射诱导的接枝聚合甲基丙烯酸衍生物，具有含氟聚合物的聚合物基材，含烯烃的聚合物或芳族聚合物; 通过辐射诱导的接枝聚合引入的聚合物基材上的接枝链的酯键脱保护; 并通过使用选自环状磺酸酯和烷基卤化物磺酸盐的亲电试剂将烷基醚磺酸结构引入接枝链的亲核官能团，从而脱保护。版权所有（C）2010，JPO＆INPIT

6. 发明专利

JP2008195748A Crosslinked aromatic polymer electrolyte membrane and its manufacturing method 审中-公开
标题翻译：交联芳香族聚合物电解质膜及其制造方法
公开(公告)号：JP2008195748A
公开(公告)日：2008-08-28
申请号：JP2007029223
申请日：2007-02-08
申请人： Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： CHIN SHINKA , MAEKAWA YASUNARI , ASANO MASAHARU , YOSHIDA MASARU
IPC分类号： C08J5/22 , C08J7/12 , H01B1/06 , H01B13/00 , H01M8/02 , H01M8/10
CPC分类号： H01M8/1018 , H01M8/0289 , H01M8/04197 , H01M8/1011 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1088 , Y02E60/523 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide a crosslinked aromatic polymer electrolyte membrane that has a low water content and exhibits high proton conductivity, low methanol permeability, a high antioxidative property and excellent mechanical properties, and its manufacturing method. SOLUTION: An aromatic polymer film substrate or a grafted aromatic polymer film substrate having a monomer introduced thereinto as a graft chain is given a crosslinked structure by ionizing radiation irradiation. As the aromatic polymer film substrate and the grafted aromatic polymer film substrate endowed with the crosslinked structure are insoluble in a sulfonating solution, these film substrates are directly sulfonated to give the crosslinked aromatic polymer electrolyte membrane. As introduction of the monomer as the graft chain permits control of the crosslinked structure of the electrolyte membrane and of the microphase separation structure in a proton conductive domain, the crosslinked aromatic polymer electrolyte membrane, which has a low water content and exhibits high proton conductivity, low methanol permeability, a high antioxidative property and excellent mechanical properties, can be prepared. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供具有低含水量并且显示出高质子传导性，低甲醇渗透性，高抗氧化性和优异机械性能的交联芳族聚合物电解质膜及其制造方法。解决方案：通过电离辐射照射将具有引入其中的单体作为接枝链的芳族聚合物膜基材或接枝的芳族聚合物膜基材赋予交联结构。由于芳族聚合物膜基材和具有交联结构的接枝芳族聚合物膜基材不溶于磺化溶液，所以这些膜基材直接磺化，得到交联的芳族聚合物电解质膜。由于作为接枝链的单体的引入允许控制质子传导区域中的电解质膜和微相分离结构的交联结构，所以具有低含水量并且显示出高质子传导性的交联芳族聚合物电解质膜，可以制备低甲醇渗透性，高抗氧化性和优异的机械性能。版权所有（C）2008，JPO＆INPIT

7. 发明专利

JP2007031650A Resin composition colored by quantum beam and nano imaging formation method 审中-公开
标题翻译：通过量子束和纳米成像方法着色的树脂组合物
公开(公告)号：JP2007031650A
公开(公告)日：2007-02-08
申请号：JP2005220517
申请日：2005-07-29
申请人： Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： MAEKAWA YASUNARI , YOSHIDA MASARU
IPC分类号： C08L101/00 , C08K5/18 , C08K5/34 , C09K3/00
摘要： PROBLEM TO BE SOLVED: To solve the problem that almost no reaction mechanisms of highly practicable organic molecules such as photochromic molecules with quantum beams have been made clear and that no promising proposals have been made concerning next-generation recording systems that enhance recording density by leaps and bounds though utilization of quantum beams having a wavelength of a pattern size or less is inevitable as light used for densification.
SOLUTION: A resin film, comprised of a compound generating an acid by quantum beams (acid-generating agent) and an environmentally chromic molecule chemically convertible from a colorless substance to a colored substance by the acid with good efficiency, is irradiated with quantum nano beams operable at a high speed thereby to realize writing technology of colored patterns having nano scale resolution that attains a recording density several figures higher than that of conventional recording media utilizing light.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：为了解决几乎没有高度实用的有机分子如光致变色分子与量子束的反应机理已经清楚的问题，并且对于增强记录的下一代记录系统没有提出有希望的建议尽管利用具有图案尺寸或更小的波长的量子束，但是由于用于致密化的光是不可避免的，所以通过跨越式的密度来实现。
解决方案：通过量子光（酸产生剂）产生酸的化合物和通过酸从无色物质化学转化成有色物质的环境色度分子的树脂膜被照射到具有良好效率的酸中能够以高速操作的量子纳米光束，从而实现具有纳米级分辨率的彩色图案的写入技术，其具有比利用光的常规记录介质高几十倍的记录密度。版权所有（C）2007，JPO＆INPIT

8. 发明专利

JP2014086205A Method for producing ion exchange membrane 审中-公开
标题翻译：生产离子交换膜的方法
公开(公告)号：JP2014086205A
公开(公告)日：2014-05-12
申请号：JP2012232670
申请日：2012-10-22
申请人： Nitto Denko Corp , 日東電工株式会社 , Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： SUZUKI HIROSE , HIGUCHI HIROYUKI , EMORI HIDEYUKI , MATSUDA YASUTAKE , INOUE TAKEO , MATSUSHIMA RYOICHI , ASANO MASAHARU , MAEKAWA YASUNARI
IPC分类号： H01M8/02 , C08J5/22 , H01B13/00 , H01M8/10
CPC分类号： Y02E60/521
摘要： PROBLEM TO BE SOLVED: To provide an ion exchange membrane small in an area change ratio even when changed from a dry state to a heated and swollen state.SOLUTION: A method of the present invention for producing an ion exchange membrane includes the steps of: (i) forming a membrane using a liquid including a polymer containing an acidic group by means of a cast film formation method; (ii) causing the membrane to hold water; and (iii) drying the membrane that holds water while the shape is fixed. The method does not include a step of substantially drawing the membrane obtained through the step (ii), after the step (ii).
摘要翻译：要解决的问题：即使从干燥状态变为加热和膨胀状态，也提供面积变化率小的离子交换膜。解决方案：本发明的用于制造离子交换膜的方法包括以下步骤：（i）通过流延膜形成法使用包含含有酸性基团的聚合物的液体形成膜; （ii）使膜保持水分; 和（iii）在固定形状的同时干燥保持水的膜。该方法不包括在步骤（ii）之后基本上拉出通过步骤（ii）获得的膜的步骤。

9. 发明专利

JP2014084350A Ion exchange resin-containing liquid and ion exchange membrane, and methods for producing them 审中-公开
标题翻译：离子交换树脂含液和离子交换膜及其生产方法
公开(公告)号：JP2014084350A
公开(公告)日：2014-05-12
申请号：JP2012232666
申请日：2012-10-22
申请人： Nitto Denko Corp , 日東電工株式会社 , Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： SUZUKI HIROSE , HIGUCHI HIROYUKI , EMORI HIDEYUKI , MATSUDA YASUTAKE , INOUE TAKEO , MATSUSHIMA RYOICHI , ASANO MASAHARU , MAEKAWA YASUNARI
IPC分类号： C08L51/00 , C08F291/00 , C08J5/22 , H01B1/06 , H01B13/00 , H01M8/02 , H01M8/10
CPC分类号： Y02E60/521
摘要： PROBLEM TO BE SOLVED: To provide novel methods for producing an ion exchange resin-containing liquid and ion exchange membrane.SOLUTION: The disclosed method for producing an ion exchange resin-containing liquid includes steps of: irradiating a first polymer with radiation ray at a temperature of 10°C or less; synthesizing a second polymer containing precursor of sulfonic acid group by contacting a solution containing a monomer that contains precursor of sulfonic acid group, with the first polymer in solid state to graft polymerize the monomer to the first polymer; obtaining a third polymer containing sulfonic acid group by converting the precursor of sulfonic acid of second polymer into sulfonic acid group; and dispersing or dissolving the third polymer into an organic solvent.
摘要翻译：要解决的问题：提供用于制备含离子交换树脂的液体和离子交换膜的新方法。解决方案：所公开的含离子交换树脂的液体的制造方法包括以下步骤：在第一聚合物的辐射线温度为10℃以下; 通过使包含含有磺酸前体的单体的溶液与固体状态的第一聚合物接触聚合单体至第一聚合物，合成含有磺酸基前体的第二聚合物; 通过将第二聚合物的磺酸的前体转化为磺酸基，得到含有磺酸基团的第三聚合物; 并将第三聚合物分散或溶解到有机溶剂中。

10. 发明专利

JP2013235667A Proton-conductive polymer electrolyte membrane, method for producing the same, membrane/electrode assembly using the same, and fuel cell 审中-公开
标题翻译：导电聚合物电解质膜，其制造方法，使用其的膜/电极组件和燃料电池
公开(公告)号：JP2013235667A
公开(公告)日：2013-11-21
申请号：JP2012105855
申请日：2012-05-07
申请人： Nitto Denko Corp , 日東電工株式会社 , Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： KISHII YUTAKA , EMORI HIDEYUKI , NISHII HIROYUKI , HIGUCHI HIROYUKI , ASANO MASAHARU , MAEKAWA YASUNARI
IPC分类号： H01M8/02 , C08J3/24 , C08J5/22 , H01B1/06 , H01B13/00 , H01M8/10
CPC分类号： Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide a polymer electrolyte membrane which exhibits sufficient proton conductivity even under low humidity, and a method for producing the same.SOLUTION: The polymer electrolyte membrane of the present invention is a proton-conductive polymer electrolyte membrane containing a polymer which contains a main chain and side chains bonded to the main chain. The side chains contain a plurality of sulfonic acid groups. At least some of the side chains are crosslinked by a crosslinking structure formed by reaction of at least one group selected from the group consisting of sulfonic acid groups and sulfonic acid group derivatives with a compound containing a plurality of isocyanate groups.
摘要翻译：要解决的问题：提供即使在低湿度下也显示出足够的质子传导性的聚合物电解质膜及其制造方法。本发明的高分子电解质膜是含有聚合物的质子传导性高分子电解质膜其包含主链和侧链键合到主链上。侧链含有多个磺酸基团。至少一些侧链通过由选自磺酸基和磺酸基衍生物的至少一个基团与含有多个异氰酸酯基团的化合物反应而形成的交联结构交联。

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