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1. 发明申请

US20110166257A1 Low odor compositions and methods to attain low odor compositions 有权
标题翻译：低气味组合物和获得低气味组合物的方法
公开(公告)号：US20110166257A1
公开(公告)日：2011-07-07
申请号：US12928408
申请日：2010-12-10
申请人： James Bohling , Paul F. Doll , David E. Frattarelli , Kathleen R. Manna , Alvin M. Maurice
发明人： James Bohling , Paul F. Doll , David E. Frattarelli , Kathleen R. Manna , Alvin M. Maurice
IPC分类号： C09D131/04 , C09D189/00 , C08J3/00 , C09D133/06
CPC分类号： C08F6/006 , C09D131/04 , C08L33/06 , C08L31/02
摘要： This invention provides stable aqueous compositions including stable coating compositions, and methods of their production. The stable aqueous compositions and stable aqueous coating compositions comprise i) an aqueous dispersion of one or more emulsion-polymerized addition polymer comprising polymerized units of one or more carboxylester monomer, wherein at least one carboxylester monomer is a vinyl ester monomer; ii) one or more carboxylesterase enzyme; iii) one or more mono-alcohol with a formula molecular weight of less than 76; iv) optionally, acetaldehyde; and v) optionally, one or more organic carboxylester with a normal boiling point of less than 150° C.; and wherein the aqueous composition has a headspace volatile organic compound(VOC) content, as measured by headspace gas chromatography-mass spectrometry (GC-MS) at 33° C., characterized by a content of less than 10 ppm of acetaldehyde, and less than 10 ppm of the one or more organic carboxylester, and more than 50 ppm of the one or more mono-alcohol. Preferably, the ester hydrolysis activity in the composition is less than 0.010 micromole/minute.
摘要翻译：本发明提供稳定的含水组合物，包括稳定的涂料组合物及其生产方法。稳定的含水组合物和稳定的水性涂料组合物包含i）一种或多种乳液聚合的加成聚合物的水分散体，其包含一个或多个羧酸酯单体的聚合单元，其中至少一个羧酸酯单体是乙烯基酯单体; ii）一种或多种羧酸酯酶; iii）一种或多种具有式分子量小于76的单醇; iv）任选的乙醛; 和v）任选的一种或多种正常沸点低于150℃的有机羧酸酯; 并且其中所述含水组合物具有顶空挥发性有机化合物（VOC）含量，其通过顶空气相色谱 - 质谱（GC-MS）在33℃下测量，其特征在于小于10ppm的乙醛含量和较少超过10ppm的一种或多种有机羧酸酯，以及大于50ppm的一种或多种单醇。优选地，组合物中的酯水解活性小于0.010微摩尔/分钟。

2. 发明授权

US08546482B2 Low odor compositions and low odor coating compositions 有权
标题翻译：低气味组合物和低气味涂料组合物
公开(公告)号：US08546482B2
公开(公告)日：2013-10-01
申请号：US12928409
申请日：2010-12-10
申请人： James Bohling , Paul F. Doll , David L. Frattarelli , Kathleen R. Manna , Alvin M. Maurice
发明人： James Bohling , Paul F. Doll , David L. Frattarelli , Kathleen R. Manna , Alvin M. Maurice
IPC分类号： C08G18/62 , C12N9/18 , C08L89/00
CPC分类号： C08L33/04 , C08F6/006 , C08L2201/52 , C09D131/04 , C09D133/04 , C09D133/08 , C09D135/06 , C08L33/00
摘要： This invention provides stable aqueous compositions including stable coating compositions, and methods of their production. The stable aqueous compositions and stable aqueous coating compositions comprise one or more emulsion-polymerized addition polymer, one or more carboxylesterase enzyme, and one or more carboxylesterase deactivating agent, such that the ester hydrolysis activity in the composition is less than 0.010 micromole/minute, and wherein the aqueous composition has a headspace volatile organic compound (VOC) content, as measured by headspace gas chromatography-mass spectrometry (GC-MS) at 33° C., of less than 10 ppm of organic carboxylester with a normal boiling point of less than 150° C. and more than 50 ppm of mono-alcohol with a formula molecular weight of less than 76. The carboxylesterase enzyme is employed to minimize the free carboxylester content in the composition, thereby providing a low odor composition, and the carboxylesterase is deactivated in situ in order to minimize the residual carboxylesterase enzyme activity.
摘要翻译：本发明提供稳定的含水组合物，包括稳定的涂料组合物及其生产方法。稳定的水性组合物和稳定的水性涂料组合物包含一种或多种乳液聚合的加成聚合物，一种或多种羧酸酯酶和一种或多种羧酸酯酶失活剂，使得组合物中的酯水解活性小于0.010微摩尔/分钟，并且其中所述含水组合物具有顶空挥发性有机化合物（VOC）含量，如通过顶空气相色谱 - 质谱（GC-MS）在33℃下测得的，小于10ppm的有机羧酸酯的正常沸点为低于150℃和超过50ppm的具有式分子量小于76的单醇。羧酸酯酶用于使组合物中游离羧酸酯含量最小化，从而提供低气味组合物，并且羧酸酯酶在原位失活，以使残留的羧酸酯酶活性最小化。

3. 发明申请

US20110152406A1 Low odor compositions and low odor coating compositions 有权
标题翻译：低气味组合物和低气味涂料组合物
公开(公告)号：US20110152406A1
公开(公告)日：2011-06-23
申请号：US12928409
申请日：2010-12-10
申请人： James Bohling , Paul F. Doll , David L. Frattarelli , Kathleen R. Manna , Alvin M. Maurice
发明人： James Bohling , Paul F. Doll , David L. Frattarelli , Kathleen R. Manna , Alvin M. Maurice
IPC分类号： C09D133/12 , C09D189/00 , C08J3/00
CPC分类号： C08L33/04 , C08F6/006 , C08L2201/52 , C09D131/04 , C09D133/04 , C09D133/08 , C09D135/06 , C08L33/00
摘要： This invention provides stable aqueous compositions including stable coating compositions, and methods of their production. The stable aqueous compositions and stable aqueous coating compositions comprise one or more emulsion-polymerized addition polymer, one or more carboxylesterase enzyme, and one or more carboxylesterase deactivating agent, such that the ester hydrolysis activity in the composition is less than 0.010 micromole/minute, and wherein the aqueous composition has a headspace volatile organic compound (VOC) content, as measured by headspace gas chromatography-mass spectrometry (GC-MS) at 33° C., of less than 10 ppm of organic carboxylester with a normal boiling point of less than 150° C. and more than 50 ppm of mono-alcohol with a formula molecular weight of less than 76. The carboxylesterase enzyme is employed to minimize the free carboxylester content in the composition, thereby providing a low odor composition, and the carboxylesterase is deactivated in situ in order to minimize the residual carboxylesterase enzyme activity.
摘要翻译：本发明提供稳定的含水组合物，包括稳定的涂料组合物及其生产方法。稳定的水性组合物和稳定的水性涂料组合物包含一种或多种乳液聚合的加成聚合物，一种或多种羧酸酯酶和一种或多种羧酸酯酶失活剂，使得组合物中的酯水解活性小于0.010微摩尔/分钟，并且其中所述含水组合物具有顶空挥发性有机化合物（VOC）含量，如通过顶空气相色谱 - 质谱（GC-MS）在33℃下测得的，小于10ppm的有机羧酸酯的正常沸点为低于150℃和超过50ppm的具有式分子量小于76的单醇。羧酸酯酶用于使组合物中游离羧酸酯含量最小化，从而提供低气味组合物，并且羧酸酯酶在原位失活，以使残留的羧酸酯酶活性最小化。

4. 发明授权

US08524809B2 Low odor compositions and methods to attain low odor compositions 有权
标题翻译：低气味组合物和获得低气味组合物的方法
公开(公告)号：US08524809B2
公开(公告)日：2013-09-03
申请号：US12928408
申请日：2010-12-10
申请人： James Bohling , Paul F. Doll , David L. Frattarelli , Kathleen R. Manna , Alvin M. Maurice
发明人： James Bohling , Paul F. Doll , David L. Frattarelli , Kathleen R. Manna , Alvin M. Maurice
IPC分类号： C08L89/00 , C08K5/10 , C12P7/62
CPC分类号： C08F6/006 , C09D131/04 , C08L33/06 , C08L31/02
摘要： This invention provides stable aqueous compositions including stable coating compositions, and methods of their production. The stable aqueous compositions and stable aqueous coating compositions comprise i) an aqueous dispersion of one or more emulsion-polymerized addition polymer comprising polymerized units of one or more carboxylester monomer, wherein at least one carboxylester monomer is a vinyl ester monomer; ii) one or more carboxylesterase enzyme; iii) one or more mono-alcohol with a formula molecular weight of less than 76; iv) optionally, acetaldehyde; and v) optionally, one or more organic carboxylester with a normal boiling point of less than 150° C.; and wherein the aqueous composition has a headspace volatile organic compound (VOC) content, as measured by headspace gas chromatography-mass spectrometry (GC-MS) at 33° C., characterized by a content of less than 10 ppm of acetaldehyde, and less than 10 ppm of the one or more organic carboxylester, and more than 50 ppm of the one or more mono-alcohol. Preferably, the ester hydrolysis activity in the composition is less than 0.010 micromole/minute.
摘要翻译：本发明提供稳定的含水组合物，包括稳定的涂料组合物及其生产方法。稳定的含水组合物和稳定的水性涂料组合物包含i）一种或多种乳液聚合的加成聚合物的水分散体，其包含一个或多个羧酸酯单体的聚合单元，其中至少一个羧酸酯单体是乙烯基酯单体; ii）一种或多种羧酸酯酶; iii）一种或多种具有式分子量小于76的单醇; iv）任选的乙醛; 和v）任选的一种或多种正常沸点低于150℃的有机羧酸酯; 并且其中所述含水组合物具有顶空挥发性有机化合物（VOC）含量，其通过顶空气相色谱 - 质谱（GC-MS）在33℃下测量，其特征在于小于10ppm的乙醛含量和较少超过10ppm的一种或多种有机羧酸酯，以及大于50ppm的一种或多种单醇。优选地，组合物中的酯水解活性小于0.010微摩尔/分钟。

5. 发明授权

US06814426B2 Color ink-jet printer with dye-based black and pigment-based color ink 失效
标题翻译：彩色喷墨打印机，配有染料黑色和颜料色墨
公开(公告)号：US06814426B2
公开(公告)日：2004-11-09
申请号：US10184204
申请日：2002-06-28
申请人： Paul F. Doll , Donald Dressler , Sean Kelly
发明人： Paul F. Doll , Donald Dressler , Sean Kelly
IPC分类号： B41J221
CPC分类号： C09D11/40 , B41J2/2056 , B41J2/2107
摘要： A color ink-jet printer is provided, with one pen for dispensing black ink onto a print medium and at least one pen for dispensing color ink onto a print medium. The pen for dispensing black ink contains a fade resistant dye-based ink and the pen(s) for dispensing color ink(s) contain a pigment-based ink(s). Such a color ink-jet printer provides both superior color gamut with contrast and excellent fade resistance. Since the black ink does not need to be chromatic one can employ fade resistant dyes that do not decrease the lightfastness of the whole ink set. In addition, very soluble fade resistant dyes can be used reliably in high concentrations allowing the black ink to provide more optical density than current pigment-based black inks.

6. 发明授权

US5802818A Refilling ink jet cartridges 失效
标题翻译：加墨喷墨盒
公开(公告)号：US5802818A
公开(公告)日：1998-09-08
申请号：US821068
申请日：1997-03-20
申请人： Paul F. Doll , Michael A. Andreottola , Shaun Flanagan
发明人： Paul F. Doll , Michael A. Andreottola , Shaun Flanagan
IPC分类号： B41J2/175 , B65B3/04 , B65B3/18
CPC分类号： B41J2/17506
摘要： An ink jet cartridge is refilled by establishing a fill opening extending from an outer portion of the cartridge into an interior ink bladder of the cartridge, applying pressure to sides of the cartridge to provide a decreased volume of the interior ink bladder, transferring ink into the interior ink bladder through the fill opening while maintaining the decreased volume, sealing the fill opening, and relieving pressure on the sides of the cartridge to provide an increased volume of the interior ink bladder. The fill opening can be established using a poker. Transferring ink can include using a squeeze bottle filled with ink. Pressure can be applied to the sides of the cartridge with a clamp similar to a #100 binder clip manufactured by Office Mate International Corporation of Edison, N.J. The fill opening can be sealed with a set screw or a ball cork along with pressure-sensitive tape.
摘要翻译：通过建立从盒的外部部分延伸到盒的内部墨囊中的填充开口来重新填充喷墨墨盒，向墨盒的侧面施加压力，以提供内部墨囊的减小的体积，将墨转移到内部墨囊通过填充开口，同时保持减小的体积，密封填充开口，并释放墨盒两侧的压力，以提供内部墨囊的增加的体积。填充开口可以使用扑克来建立。转印墨水可以包括使用填充有墨水的挤压瓶。压力可以用类似于美国新泽西州爱迪生办公室的Mate International Corporation制造的＃100粘合夹的夹子施加到墨盒的侧面。填充开口可以用固定螺钉或球软塞与压敏胶带一起密封。

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