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    • 3. 发明专利
    • Apparatus for detecting atmosphere in furnace
    • 检测大气中的大气的装置
    • JP2000074753A
    • 2000-03-14
    • JP24134698
    • 1998-08-27
    • Hitachi Ltd株式会社日立製作所
    • TANAKA SHIGERUSUZUKI YASUTAKAYAMADA SEIICHICHIBA AKIOTAKAHASHI KEN
    • G01K11/00F27B14/20F27B17/00G01N27/04G01N27/12
    • PROBLEM TO BE SOLVED: To make detectable the temp./oxygen concn. by a convenient method, without using complicated electric wirings or measuring circuits by constituting a detector for detecting signals from a specified ceramic sintered compact.
      SOLUTION: E.g., 6 sheets of ceramic sintered compact 1 formed in specified dimensions, contg. zinc oxide 80 mol% or more, are adhered onto an alumina board 3 with an inorg. adhesive 2 to form the furnace atmosphere detector. The sheets of sintered compact 1 are made by sintering in the air (O concn. 20%) at temps. of 950°C, 960°C, 970°C, 980°C, 990°C, respectively. The furnace atmosphere detector is set in an electric furnace set e.g. at 970°C, the surface of each sintered compact 1 is visually seen after completion of the sintering process. In this time voids or cracks appear on the sintered compact surface at 950°C, 960°C, 970°C, and if no change appears on the sintered compact at 980°C, 990°C, the furnace temp. is lower than 980°C and higher than 970°C. When the temp. must be known at a more fine resolution, the furnace temp. can be estimated at an accuracy within about 2°C from the change of the crystal grain size.
      COPYRIGHT: (C)2000,JPO
    • 要解决的问题:使可测的温度/氧浓度 通过构成用于检测来自特定陶瓷烧结体的信号的检测器,通过方便的方法不使用复杂的电线或测量电路。 解决方案:例如,以特定尺寸形成的6片陶瓷烧结体1, 80摩尔%以上的氧化锌用氧化铝粘合到氧化铝板3上。 粘合剂2形成炉气氛检测器。 烧结体1通过在空气中烧结(O浓度20%)在温度下制造。 分别为950℃,960℃,970℃,980℃,990℃。 炉气氛检测器设置在例如电炉中。 在970℃下,烧结工序完成后,目视观察各烧结体1的表面。 此时,在950℃,960℃,970℃的烧结体表面上出现空隙或裂纹,如果烧结体在980℃,990℃没有变化,则炉 温度 低于980℃,高于970℃。 当温度 必须以更精细的分辨率知道炉温。 可以从晶粒尺寸的变化估计在约2℃以内的精度。
    • 9. 发明专利
    • DE69120250T2
    • 1996-10-10
    • DE69120250
    • 1991-03-18
    • HITACHI LTD
    • YASUTOMI YOSHIYUKIWATAHIKI SEIJISAKAI JUNJICHIBA AKIOMIYOSHI TADAHIKOSOBUE MASAHISA
    • C04B35/00C04B35/565C04B35/58C04B35/591C04B35/622C04B35/80C04B38/00C23C16/34C04B35/56C04B38/06C04B41/87
    • The present invention provides a composite ceramic structure of sintered ceramics having a porosity of 5 to 40 % by volume and, if necessary, a maximum pore size of 10 mu m or less comprising particles selected from the group consisting of grains and whiskers of at least one inorganic compound AB selected from the group consisting of carbides, nitrides, and oxides which are composed of an element A and an element B, where a difference in electronegativity between the element A and the element B is not higher than 1.7; or particles selected from the group consisting of grains and whiskers of an inorganic compound, between the components of which a difference in electronegativity is higher than 1.7, and having layers of the inorganic compound AB formed on the surfaces of said particles; where said particles are bonded one another with silicon nitride particles having an average particle size not more than 0.2 mu m. The composite ceramic structure is produced by sintering a shape composed of particles selected from the group consisting of grains and whiskers of at least one of the inorganic compound AB; or a shape composed of particles selected from the group consisting of grains and whiskers of an inorganic compound, between the components of which a difference in electronegativity is higher than 1.7, and having layers of the inorganic compound AB formed on the surfaces of said particles; in a gaseous atmosphere containing silicon and nitrogen to grow silicon nitride particles having an average particle size not higher than 0.2 mu m on the surfaces of said inorganic compound particles, thereby bonding said inorganic compound particles one another. A ceramic sintered shape highly accurate in dimension having a surface configuration which is a replica of the surface contour of a mold as a ceramic mechanical part of precision is also proveded.