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1. 发明授权

US07270586B2 Organic electroluminescence element and production method thereof 失效
标题翻译：有机电致发光元件及其制造方法
公开(公告)号：US07270586B2
公开(公告)日：2007-09-18
申请号：US10972509
申请日：2004-10-26
申请人： Hiroshi Tokailin , Yoshikazu Nagasaki , Tadao Shibuya , Kazuyoshi Inoue
发明人： Hiroshi Tokailin , Yoshikazu Nagasaki , Tadao Shibuya , Kazuyoshi Inoue
IPC分类号： C23C14/00 , H01J1/62 , H01J9/00
CPC分类号： H01L51/5088 , H01L51/442 , H01L51/5206 , Y02E10/549 , Y10S428/917 , Y10T428/26
摘要： An organic EL element comprising; an anode, a cathode, and an organic layer sandwiched therebetween containing at least an emitting layer, wherein a ratio, [In3d5/2]h/[In3d5/2]n, is from 0.9 to 1.2 wherein [In3d5/2]h is the half band width of a spectral peak derived from a 3d5/2 orbit of an In atom in the surface of the anode, and [In3d5/2]n is the half band width of a spectral peak derived from a 3d5/2 orbit of an In atom in the interior of the anode, the spectral peaks being measured by X-ray photoelectron spectroscopy (XPS): and the method for the production thereof.
摘要翻译：一种有机EL元件，包括：阳极，阴极和夹在其间的至少一个发光层的有机层，其中比例为[In 3/2 5/2 N] / [In 3 d＆ 5/2 N n为0.9至1.2，其中[In 3 d 5/2/2] h H是半波长宽度衍射自阳极表面中的In原子的3d 5/2 /轨道的光谱峰和[In3d5 / 2] N

2. 发明申请

US20050085152A1 Organic electroluminescence element and production method thereof 失效
标题翻译：有机电致发光元件及其制造方法
公开(公告)号：US20050085152A1
公开(公告)日：2005-04-21
申请号：US10972509
申请日：2004-10-26
申请人： Hiroshi Tokailin , Yoshikazu Nagasaki , Tadao Shibuya , Kazuyoshi Inoue
发明人： Hiroshi Tokailin , Yoshikazu Nagasaki , Tadao Shibuya , Kazuyoshi Inoue
IPC分类号： B05D5/12 , C23C14/32 , H01J9/00 , H01J9/24 , H01L51/44 , H01L51/50 , H01L51/52 , H05B33/12 , H05B33/26
CPC分类号： H01L51/5088 , H01L51/442 , H01L51/5206 , Y02E10/549 , Y10S428/917 , Y10T428/26
摘要： An organic EL element comprising; an anode, a cathode, and an organic layer sandwiched therebetween containing at least an emitting layer, wherein a ratio, [In3d5/2]h/[In3d5/2]n, is from 0.9 to 1.2 wherein [In3d5/2]h is the half band width of a spectral peak derived from a 3d5/2 orbit of an In atom in the surface of the anode, and [In3d5/2]n is the half band width of a spectral peak derived from a 3d5/2 orbit of an In atom in the interior of the anode, the spectral peaks being measured by X-ray photoelectron spectroscopy (XPS): and the method for the production thereof.
摘要翻译：一种有机EL元件，包括：阳极，阴极和夹在其间的至少一个发光层的有机层，其中比例为[In 3/2 5/2 N] / [In 3 d＆ 5/2 N n为0.9至1.2，其中[In 3 d 5/2/2] h H是半波长宽度衍射自阳极表面中的In原子的3d 5/2 /轨道的光谱峰和[In3d5 / 2] N

3. 发明授权

US06963383B2 Electrode substrate and production method thereof 失效
标题翻译：电极基板及其制造方法
公开(公告)号：US06963383B2
公开(公告)日：2005-11-08
申请号：US10460677
申请日：2003-06-13
申请人： Hiroshi Tokailin , Yoshikazu Nagasaki , Tadao Shibuya , Kazuyoshi Inoue
发明人： Hiroshi Tokailin , Yoshikazu Nagasaki , Tadao Shibuya , Kazuyoshi Inoue
IPC分类号： B32B7/02 , B32B9/00 , G02F1/1343 , G09F9/30 , H01B5/14 , H01B13/00 , H01L51/50 , H05B33/02 , H05B33/10 , H05B33/26
CPC分类号： G02F1/13439 , Y10S428/917
摘要： An electrode substrate comprising; an electrode comprising a compound containing an In atom and a substrate body, wherein a half band width ratio [In3d5/2]h/[In3d5/2]n is from 0.9 to 1.2 wherein [In3d5/2]h is a half band width of a 3d5/2 orbit spectral peak of an In atom in the surface of the electrode, and [In3d5/2]n is a half band width of a 3d5/2 orbit spectral peak of an In atom in the interior of the electrode, the spectral peaks being measured by X-ray photoelectron spectroscopy: and the method for the production thereof.
摘要翻译：一种电极基板，包括：包含含有In原子和底物的化合物的电极，其中半带宽比[In 3 d 5/2/2] / [In 3 d 5/2 其中[In 3 d 5/2/2] h是3d的一半带宽（SUB）在电极表面中的In原子的5/2 / 2的轨道光谱峰，并且[In 3 d 5/2 N] N N是半波段宽度在电极内部的In原子的3d5 / 2/2轨道光谱峰，通过X射线光电子能谱测量的光谱峰及其制造方法。

4. 发明授权

US06828045B1 Organic electroluminescence element and production method thereof 失效
标题翻译：有机电致发光元件及其制造方法
公开(公告)号：US06828045B1
公开(公告)日：2004-12-07
申请号：US10460678
申请日：2003-06-13
申请人： Hiroshi Tokailin , Yoshikazu Nagasaki , Tadao Shibuya
发明人： Hiroshi Tokailin , Yoshikazu Nagasaki , Tadao Shibuya
IPC分类号： H05B3326
CPC分类号： H01L51/5088 , H01L51/442 , H01L51/5206 , Y02E10/549 , Y10S428/917 , Y10T428/26
摘要： An organic EL element comprising: an anode, a cathode, and an organic layer sandwiched therebetween containing at least an emitting layer, wherein a ratio, [In3d5/2]h/[In3d5/2]n, is from 0.9 to 1.2 wherein [In3d5/2]h is the half band width of a spectral peak derived from a 3d5/2 orbit of an In atom in the surface of the anode, and [In3d5/2]n is the half band width of a spectral peak derived from a 3d5/2 orbit of an In atom in the interior of the anode, the spectral peaks being measured by X-ray photoelectron spectroscopy (XPS): and the method for the production thereof.
摘要翻译：一种有机EL元件，包括：阳极，阴极和夹在其间的至少一个发光层的有机层，其中[In3d5 / 2] h / [In3d5 / 2] n的比例为0.9〜1.2，其中[ In3d5 / 2] h是从阳极表面的In原子的3d5 / 2轨道衍生的光谱峰的半带宽，[In3d5 / 2] n是衍生自在阳极内部的In原子的3d5 / 2轨道，通过X射线光电子能谱（XPS）测量的光谱峰及其制造方法。

5. 发明授权

US06633121B2 Organic electroluminescence display device and method of manufacturing same 有权
标题翻译：有机电致发光显示装置及其制造方法
公开(公告)号：US06633121B2
公开(公告)日：2003-10-14
申请号：US09767018
申请日：2001-01-23
申请人： Mitsuru Eida , Hiroshi Tokailin , Yoshikazu Nagasaki , Toshio Sakai
发明人： Mitsuru Eida , Hiroshi Tokailin , Yoshikazu Nagasaki , Toshio Sakai
IPC分类号： H05B3304
CPC分类号： H05B33/10 , H01L27/322 , H01L27/3244 , H01L27/3295 , H01L51/5088 , H01L51/5092 , H01L51/5237 , H01L51/5284 , H01L51/56 , H05B33/04
摘要： An organic electroluminescent device including a lower electrode, an organic light-emission medium, and an upper electrode on a support substrate, wherein the water content of the organic light-emission medium does not exceed 0.05 wt. %. By so controlling the water content of the organic light-emission medium, it is possible to prevent shrinkage of a light-emission area based on production of non-emission parts or non-emission spots for a long time at both high temperature and room temperature conditions. A method of making the organic electroluminescent device is disclosed also.
摘要翻译：一种有机电致发光器件，包括在支撑衬底上的下电极，有机发光介质和上电极，其中有机发光介质的含水量不超过0.05重量％。％。通过这样控制有机发光介质的含水量，可以防止在高温和室温下长时间产生非发射部分或非发光斑点的发光区域的收缩条件。还公开了制造有机电致发光器件的方法

6. 发明授权

US06995507B2 Method for depositing thin film for element, and organic electroluminescence element 失效
标题翻译：用于沉积元素薄膜的方法和有机电致发光元件
公开(公告)号：US06995507B2
公开(公告)日：2006-02-07
申请号：US10608138
申请日：2003-06-30
申请人： Hiroshi Tokailin , Yoshikazu Nagasaki
发明人： Hiroshi Tokailin , Yoshikazu Nagasaki
IPC分类号： H05B33/00
CPC分类号： H01L51/0008 , C09K11/06 , C23C14/12 , C23C14/24 , H01L51/001 , H01L51/005 , H01L51/0059 , H01L51/007 , H01L51/0081 , H01L2251/308 , H05B33/10 , H05B33/14 , Y10S428/917
摘要： The present invention concerns a method of forming one or more thin films on a substrate by depositing two or more materials by vacuum evaporation, comprising, depositing each material under such control that ni value of the each material is k±0.5 wherein k is a constant from 2 to 5, when relationship between a deposition position and a film thickness of a material i on the substrate is approximated by the following equation (1): Di/D0i∝(L0/Li)3cosniθi (1) wherein L0 is a distance from an evaporation source to a plane of the substrate in a perpendicular direction, D0i is a film thickness of the material i at an intersection point of a perpendicular line from the evaporation source to the plane of the substrate, and Di is a film thickness of the material i at a position on the substrate which is apart from the evaporation source by a distance Li in a direction of an angle θi against the perpendicular line. By the method, a homogenous thin film layer for an element can be formed even on a substrate having large screen.
摘要翻译：本发明涉及一种通过真空蒸发沉积两种或更多种材料在衬底上形成一种或多种薄膜的方法，包括：在每种材料的ni值为k±0.5的情况下沉积每种材料，其中k为常数从2到5，当衬底上的材料i的沉积位置和膜厚之间的关系由下式近似时

7. 发明授权

US06649210B2 Method for forming thin-film layer for device and organic electroluminescence device 失效
标题翻译：用于器件和有机电致发光器件的薄膜层的形成方法
公开(公告)号：US06649210B2
公开(公告)日：2003-11-18
申请号：US09959655
申请日：2001-11-02
申请人： Hiroshi Tokailin , Yoshikazu Nagasaki
发明人： Hiroshi Tokailin , Yoshikazu Nagasaki
IPC分类号： C23C1424
CPC分类号： H01L51/0008 , C09K11/06 , C23C14/12 , C23C14/24 , H01L51/001 , H01L51/005 , H01L51/0059 , H01L51/007 , H01L51/0081 , H01L2251/308 , H05B33/10 , H05B33/14 , Y10S428/917
摘要： The present invention concerns a method of forming one or more thin films on a substrate by depositing two or more materials by vacuum evaporation, comprising, depositing each material under such control that ni value of the each material is k±0.5 wherein k is a constant from 2 to 5, when relationship between a deposition position and a film thickness of a material i on the substrate is approximated by the following equation (1): Di/D0i∝(L0/Li)3 cosni&thgr;i (1) wherein L0 is a distance from an evaporation source to a plane of the substrate in a perpendicular direction, D0i is a film thickness of the material i at an intersection point of a perpendicular line from the evaporation source to the plane of the substrate, and Di is a film thickness of the material i at a position on the substrate which is apart from the evaporation source by a distance Li in a direction of an angle &thgr;i against the perpendicular line. By the method, a homogenous thin film layer for an element can be formed even on a substrate having large screen.
摘要翻译：本发明涉及一种通过真空蒸发沉积两种或更多种材料在衬底上形成一种或多种薄膜的方法，包括：在每种材料的ni值为k±0.5的情况下沉积每种材料，其中k为常数从2到5，当衬底上的材料i的沉积位置和膜厚之间的关系由下面的等式（1）近似时：其中L0是垂直于基底的蒸发源到平面的距离方向，D0i是从蒸发源到基板的平面的垂直线的交点处的材料i的膜厚度，Di是基板上位于与基板不同的位置处的材料i的膜厚度蒸发源在与垂直线成角度的方向上距离为Li。通过该方法，即使在具有大屏幕的基板上也可以形成均匀的元件用薄膜层。

8. 发明授权

US07501189B2 White organic electroluminescent device 失效
标题翻译：白色有机电致发光器件
公开(公告)号：US07501189B2
公开(公告)日：2009-03-10
申请号：US11254852
申请日：2005-10-21
申请人： Hiroshi Tokailin , Hitoshi Kuma , Mineyuki Kubota , Masakazu Funahashi
发明人： Hiroshi Tokailin , Hitoshi Kuma , Mineyuki Kubota , Masakazu Funahashi
IPC分类号： H01L51/54
CPC分类号： H01L51/006 , C07C211/54 , C07C211/58 , C07C211/61 , C07C2601/14 , C07C2603/24 , C07C2603/54 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , H01L51/0052 , H01L51/0054 , H01L51/0056 , H01L51/0058 , H01L51/007 , H01L51/0081 , H01L51/5036 , H01L2251/308 , H05B33/14 , Y10S428/917 , Y10T428/24942
摘要： A white organic electroluminescent device (1) including an emitting layer (5, 6 and 7) interposed between an anode (2) and a cathode (9), the emitting layer (5, 6 and 7) emitting blue light, green light and red light, the emitting layer (6) containing a green dopant that is an aromatic amine compound represented by formula (1), wherein A1, A2 and R12 are a hydrogen atom, an alkyl group, an aryl group, a cycloalkyl group, an alkoxy group, an aryloxy group, an arylamino group, an alkylamino group or a halogen atom; d and e are independently 1 to 5; h is 1 to 9; R11 is a secondary or tertiary alkyl or cycloalkyl group; f is 1 to 9; g is 0 to 8 and f+g+h is 2 to 10.
摘要翻译：一种白色有机电致发光器件（1），包括介于阳极（2）和阴极（9）之间的发射层（5,6和7），发射蓝光的发光层（5,6和7），绿光和红色光，包含作为由式（1）表示的芳族胺化合物的绿色掺杂剂的发光层（6），其中A1，A2和R12是氢原子，烷基，芳基，环烷基，烷氧基，芳氧基，芳基氨基，烷基氨基或卤素原子; d和e独立地为1〜5; h为1〜9; R11是仲或叔烷基或环烷基; f为1〜9; g为0〜8，f + g + h为2〜10。

9. 发明授权

US06509109B1 Organic electroluminescent device 有权
标题翻译：有机电致发光器件
公开(公告)号：US06509109B1
公开(公告)日：2003-01-21
申请号：US09281953
申请日：1999-03-31
申请人： Hiroaki Nakamura , Chishio Hosokawa , Kenichi Fukuoka , Hiroshi Tokailin
发明人： Hiroaki Nakamura , Chishio Hosokawa , Kenichi Fukuoka , Hiroshi Tokailin
IPC分类号： H05B3300
CPC分类号： H01L51/5092 , H01L51/002 , H01L51/0052 , H01L51/0058 , H01L51/0059 , H01L51/006 , H01L51/007 , H01L51/0081 , H01L51/5012 , H01L2251/308 , Y10S428/917
摘要： An organic EL device is improved to produce an increased luminance and have a prolonged lifetime. In an organic EL device comprising a cathode layer 16, an electron injection region 14, a light emission region 12 and an anode layer 10 as laminated in that order, the electron injection region 14 contains an aromatic compound composed of carbon and hydrogen or an aromatic compound composed of carbon, hydrogen and oxygen, along with a reducing dopant, and the electron affinity of the electron injection region is controlled to fall between 1.8 and 3.6 eV; or the electron injection region 14 contains an electron-transporting compound and a reducing dopant having a work function of at most 2.9 eV, and the electron affinity of the electron injection region is controlled to fall between 1.8 and 3.6 eV.
摘要翻译：有机EL器件被改进以产生增加的亮度并且具有延长的寿命。在包括依次层叠的阴极层16，电子注入区域14，发光区域12和阳极层10的有机EL器件中，电子注入区域14含有由碳和氢或芳族化合物构成的芳族化合物由碳，氢和氧组成的化合物以及还原性掺杂剂，电子注入区的电子亲和力控制在1.8和3.6eV之间; 或电子注入区域14含有电子传输性化合物和功函数为2.9eV以下的还原性掺杂剂，电子注入区域的电子亲和力控制在1.8〜3.6eV之间。

10. 发明授权

US6093864A Aromatic dimethylidyne compounds 失效
标题翻译：芳香族二甲基化合物
公开(公告)号：US6093864A
公开(公告)日：2000-07-25
申请号：US87134
申请日：1993-07-02
申请人： Hiroshi Tokailin , Hisahiro Higashi , Chishio Hosokawa
发明人： Hiroshi Tokailin , Hisahiro Higashi , Chishio Hosokawa
IPC分类号： C07C13/28 , C07C15/52 , C07C15/58 , C07C15/60 , C07C43/215 , C09K11/06 , H01L51/00 , H01L51/30 , H01L51/50 , H05B33/14 , C07C43/20
CPC分类号： H05B33/14 , C07C13/28 , C07C15/52 , C07C15/58 , C07C15/60 , C07C43/215 , C09K11/06 , H01L51/005 , H01L51/0052 , H01L51/0059 , H01L51/0062 , H01L51/0067 , C07C2101/14 , H01L2251/308 , H01L51/0053 , H01L51/007 , H01L51/5012 , Y10S428/917
摘要： An aromatic dimethylidyne compound of the formula: ##STR1## wherein X and Y are the same or different and are each an alkyl having 1 to 4 carbons, a phenyl, a cyclohexyl, a naphthyl, or a pyridyl and Ar' is ##STR2## A process for preparing an aromatic dimethylidyne compound which comprises condensing a phosphorus compound and a ketone compound.
摘要翻译：具有下式的芳族二甲基化合物：其中X和Y相同或不同，并且各自为具有1至4个碳的烷基，苯基，环己基，萘基或吡啶基，Ar'是用于制备芳族化合物的方法包括使磷化合物和酮化合物缩合的二甲基化合物。

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