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1. 发明授权

US5905130A Process for the production of polysilazane 失效
标题翻译：聚硅氮烷生产工艺
公开(公告)号：US5905130A
公开(公告)日：1999-05-18
申请号：US894663
申请日：1997-08-25
申请人： Hirohiko Nakahara , Osamu Funayama , Takeshi Isoda
发明人： Hirohiko Nakahara , Osamu Funayama , Takeshi Isoda
IPC分类号： C08G77/62 , C08G77/08
CPC分类号： C08G77/62
摘要： Disclosed is a process for the production of a polysilazane containing Si--N linkages in the main chain thereof. According to the present invention, the polysilazane is produced by reacting a polyaminosilane compound with a polyhydrogenated nitrogen-containing compound in the presence of a basic catalyst or by reacting a polyhydrogenated silicon compound with a polyhydrogenated nitrogen-containing compound in the presence of a basic solid oxide catalyst.
摘要翻译： PCT No.PCT / JP97 / 00005 Sec。 371日期1997年8月25日第 102（e）日期1997年8月25日PCT 1997年1月6日PCT PCT。出版物WO97 / 24391 日期1997年7月10日公开是在其主链中生产含有Si-N键的聚硅氮烷的方法。根据本发明，聚硅氮烷是在碱性催化剂的存在下使聚氨基硅烷化合物与多氢化含氮化合物反应制备的，或者是通过使多氢化硅化合物与多氢化含氮化合物在碱性固体氧化物催化剂。

2. 发明授权

US5436398A Polymetalosilazane, process of producing same, silicon nitride based ceramic, and process of preparing same 失效
标题翻译：聚甲硅氮烷，其制备方法，氮化硅基陶瓷及其制备方法
公开(公告)号：US5436398A
公开(公告)日：1995-07-25
申请号：US223866
申请日：1994-04-06
申请人： Yasuo Shimizu , Hirohiko Nakahara , Tomoko Aoki , Osamu Funayama , Takeshi Isoda
发明人： Yasuo Shimizu , Hirohiko Nakahara , Tomoko Aoki , Osamu Funayama , Takeshi Isoda
IPC分类号： C04B35/589 , C08G77/48 , C08G77/62 , C08G79/00 , D01F9/10 , C08L83/04
CPC分类号： D01F9/10 , C04B35/589 , C08G77/62 , C08G79/00
摘要： A preceramic polymetalosilazane substantially free of Si-O groups is produced by reacting a polysilazane with a metal alkoxide in the presence of an alkylsilazane or alkylsilane. The preceramic polymer gives a high strength and heat resistant ceramic body which remains amorphous when calcined at 1,600.degree. C. for 10 hours in the atmosphere of nitrogen.
摘要翻译：通过在烷基硅氮烷或烷基硅烷的存在下使聚硅氮烷与金属醇盐反应来制备基本上不含Si-O基的预陶瓷聚金属硅氮烷。陶瓷聚合物提供了一种高强度和耐热的陶瓷体，当在氮气气氛中在1600℃下煅烧10小时时，其保持无定形。

3. 发明授权

US5459114A Method for producing ceramic products 失效
标题翻译：陶瓷制品的制造方法
公开(公告)号：US5459114A
公开(公告)日：1995-10-17
申请号：US256807
申请日：1994-07-25
申请人： Hiroshi Kaya , Kiyoshi Sato , Hiroki Morozumi , Atushi Tezuka , Tomoko Aoki , Hirohiko Nakahara , Tadashi Suzuki , Takeshi Isoda
发明人： Hiroshi Kaya , Kiyoshi Sato , Hiroki Morozumi , Atushi Tezuka , Tomoko Aoki , Hirohiko Nakahara , Tadashi Suzuki , Takeshi Isoda
IPC分类号： C04B35/589 , C04B35/80 , C04B41/45 , C04B41/50 , C04B41/52 , C04B41/81 , C04B41/87 , C04B41/89 , C04B35/58
CPC分类号： C04B41/009 , C04B35/589 , C04B35/80 , C04B35/806 , C04B41/4554 , C04B41/5053 , C04B41/52 , C04B41/81 , C04B41/87 , C04B41/89
摘要： Repetition of a process of impregnating a metal fiber or ceramic fiber preform or porous ceramic with (3) a mixture of polysilazane-type polymers with a number average molecular weight of 200-3000 and a viscosity adjusted to 100 Pa.s or lower at the impregnation temperature, prepared by mixing (1) one or more types of polysilazane-type polymers with a number average molecular weight of 200-3000 and a viscosity of less than 1 Pa.s at the impregnation temperature with (2) one or more types of polysilazane-type polymers with a number average molecular weight of 200-100,000 and having a viscosity of 1 Pa.s or higher or solid at the impregnation temperature, which are selected from polysilazanes whose main repeating unit is --[(SiH.sub.2).sub.n (NH).sub.r ]-- (where n and r are 1, 2 or 3), and copolymers, modified polymers and crosslinked polymers based thereon, and performing crosslinking curing and then firing, is performed for its conversion into a ceramic. The above polysilazane may be, for example, an inorganic polysilazane, an inorganic polysiloxazane, a polyorgano(hydro)silazane, a modified polysilazane or a polymetallosilazane. By performing the CVD coating before or after said process of impregnation, curing and firing, delamination of the fibers may be minimized.
摘要翻译： PCT No.PCT / JP93 / 01730 Sec。 371日期：1994年7月25日 102（e）日期1994年7月25日PCT提交1993年11月26日PCT公布。公开号WO94 / 12448 日期：1994年6月9日。重复使用（3）数均分子量为200-3000的聚硅氮烷型聚合物和粘度调节至100的混合物浸渍金属纤维或陶瓷纤维预制体或多孔陶瓷的方法通过在浸渍温度下混合（1）数均分子量为200-3000和粘度小于1Pa.s的一种或多种聚硅氮烷型聚合物制备的浸渍温度下的Pa.s或更低，（2）一种或多种数均分子量为200-100,000，粘度为1Pa·s或更高的聚硅氮烷型聚合物或浸渍温度下的固体，其选自聚硅氮烷，其主要重复单元为 - [（SiH2）n（NH）r] - （其中n和r为1,2或3），并且基于其进行交联固化，然后进行烧结的共聚物，改性聚合物和交联聚合物进行转化为陶瓷。上述聚硅氮烷可以是例如无机聚硅氮烷，无机聚硅氮烷，聚有机（氢）硅氮烷，改性聚硅氮烷或聚金属硅氮烷。通过在所述浸渍，固化和焙烧过程之前或之后进行CVD涂层，可以使纤维的分层最小化。

4. 发明授权

US5166104A Polysiloxazanes, silicon oxynitride fibers and processes for producing same 失效
标题翻译：聚硅氧烷，氧氮化硅纤维及其制造方法
公开(公告)号：US5166104A
公开(公告)日：1992-11-24
申请号：US756046
申请日：1991-09-06
申请人： Osamu Funayama , Mikiro Arai , Hayato Nishii , Takeshi Isoda
发明人： Osamu Funayama , Mikiro Arai , Hayato Nishii , Takeshi Isoda
IPC分类号： C04B35/589 , C08G77/54
CPC分类号： C08G77/54 , C04B35/589
摘要： Novel polysiloxazanes comprising [SiH.sub.2).sub.n NH-- and [SiH.sub.2).sub.m O-- as the main repeating units are provided. The polysiloxazanes are produced by reacting a dihalosilane or an adduct thereof with a Lewis base, with ammonia and water vapor or oxygen. From the polysiloxazane, novel silicon oxynitride shapes can be produced and the silicon oxynitride shapes are essentially composed of silicon, nitride (5 mol % or more) and oxygen (5 mol % or more).
摘要翻译：提供了以[SiH 2] nNH-和[SiH 2）mO-为主要重复单元的新型聚硅氧氮烷。聚硅氧烷是通过使二氯硅烷或其加合物与路易斯碱反应，与氨和水蒸汽或氧气反应而制备的。从聚硅氮烷可以制造新的氮氧化硅形状，氮氧化硅形状主要由硅，氮化物（5摩尔％以上）和氧（5摩尔％以上）组成。

5. 发明授权

US5128286A Boron-containing, silicon nitride-based ceramic shaped body 失效
标题翻译：含硼含量，基于硅的陶瓷形状体
公开(公告)号：US5128286A
公开(公告)日：1992-07-07
申请号：US539177
申请日：1990-06-18
申请人： Osamu Funayama , Mikiro Arai , Hiroyuki Aoki , Yuuji Tashiro , Toshio Katahata , Kiyoshi Sato , Takeshi Isoda , Tadashi Suzuki , Ichiro Kohshi
发明人： Osamu Funayama , Mikiro Arai , Hiroyuki Aoki , Yuuji Tashiro , Toshio Katahata , Kiyoshi Sato , Takeshi Isoda , Tadashi Suzuki , Ichiro Kohshi
IPC分类号： C04B35/589 , C08G77/60
CPC分类号： C04B35/589 , C08G77/60
摘要： A shaped body is disclosed which comprises substantially amorphous, silicon nitride-based ceramic containing Si, N and B as essential components and O, C and H as optional components in amounts providing the following atomic ratios:N/Si: 0.05 to 2.5,B/Si: 0.01-3,O/Si: 2.0 or less,C/Si: 1.5 or less, andH/Si: 0.1 or less.

6. 发明授权

US5032551A Silicon nitride based ceramic fibers, process of preparing same and composite material containing same 失效
标题翻译：氮化硅基陶瓷纤维，其制备方法和含有它们的复合材料
公开(公告)号：US5032551A
公开(公告)日：1991-07-16
申请号：US318175
申请日：1989-03-02
申请人： Yuuji Tashiro , Osamu Funayama , Mikiro Arai , Hiroyuki Aoki , Takeshi Isoda , Hiroshihi Kaya , Tadashi Suzuki , Toshio Katahata , Mutsuo Haino , Genshiro Nishimura
发明人： Yuuji Tashiro , Osamu Funayama , Mikiro Arai , Hiroyuki Aoki , Takeshi Isoda , Hiroshihi Kaya , Tadashi Suzuki , Toshio Katahata , Mutsuo Haino , Genshiro Nishimura
IPC分类号： C04B35/589 , C04B35/622 , C04B35/80 , C08G77/62 , C08G79/00 , D01F9/10
CPC分类号： C04B35/80 , C04B35/589 , C04B35/62227 , C08G77/62 , C08G79/00 , D01F9/10
摘要： Silicon nitride based ceramic fibers containing Si, N, O and at least one metal M in amounts providing the atomic ratios N/Si of 0.3 to 3, O/Si of 0.0001 to 15 and M/Si of 0.001 to 5 and exhibiting an X-ray small angle scattering such that the ratio of the intensity of the small angle scattering of the fibers to that of air is 1 to 20. The ceramic fibers are produced by spinning of a polymetallosilazane into fibers and calcining the spun fibers and are useful as reinforcing fibers for composite artices having a metal or resin matrix.

7. 发明授权

US4933160A Reformed, inorganic polysilazane 失效
标题翻译：改性无机聚硅氮烷
公开(公告)号：US4933160A
公开(公告)日：1990-06-12
申请号：US323375
申请日：1989-03-14
申请人： Osamu Funayama , Mikiro Arai , Takeshi Isoda
发明人： Osamu Funayama , Mikiro Arai , Takeshi Isoda
IPC分类号： C08G77/62
CPC分类号： C08G77/62
摘要： A novel, reformed, inorganic polysilazane which is liquid or solid at room temperature and soluble in o-xylene at room temperature and which has (a) a number-average molecular weight of 200-500,000, (b) contents of Si, N and H of 50-70% by weight, 20-34% by weight and 5-9% by weight, respectively; and (c) --SiH.sub.2 -- and --SiH.sub.3 groups, the molar ratio of the --SiH.sub.2 -- groups to the --SiH.sub.3 groups being 2.0:1 to 8.4:1. The reformed polysilazane is obtained by reaction of a solution of a polysilazane in an organic base-containing solvent to polycondense the polysilazane.
摘要翻译：一种新型的改性的无机聚硅氮烷，其在室温下为液体或固体，并且在室温下可溶于邻二甲苯，其具有（a）数均分子量为200-500,000，（b）Si，N和 H为50-70重量％，20-34重量％和5-9重量％和（c）-SiH 2 - 和-SiH 3基团，-SiH 2 - 基团与-SiH 3基团的摩尔比为2.0:1至8.4:1。重整的聚硅氮烷通过聚硅氮烷在含有机碱的溶剂中的溶液与聚硅氮烷缩聚得到。

8. 发明授权

US5030744A Polyborosilazane and process for producing same 失效
标题翻译：聚硼硅氮烷及其制备方法
公开(公告)号：US5030744A
公开(公告)日：1991-07-09
申请号：US466962
申请日：1990-01-18
申请人： Osamu Funayama , Mikiro Arai , Yuuji Tashiro , Takeshi Isoda , Kiyoshi Sato
发明人： Osamu Funayama , Mikiro Arai , Yuuji Tashiro , Takeshi Isoda , Kiyoshi Sato
IPC分类号： C08G77/56 , C08G77/62 , C08G79/08
CPC分类号： C08G77/56 , C08G77/62 , C08G79/08
摘要： Disclosed is a polyborosilazane having a B/Si atomic ratio of 0.01 to 3 and a number-average molecular weight of about 200 to about 500,000 which can be pyrolyzed to give ceramics. The polyborosilazane is produced by reacting a polysilazane having a number-average molecular weight of about 100 to about 50,000 with a boron compound.

9. 发明授权

US4965058A Polysiloxazanes, silicon oxynitride fibers and processes for producing same 失效
标题翻译：聚硅氧烷，氧氮化硅纤维及其制造方法
公开(公告)号：US4965058A
公开(公告)日：1990-10-23
申请号：US382713
申请日：1989-07-19
申请人： Osamu Funayama , Mikiro Arai , Hayato Nishii , Takeshi Isoda
发明人： Osamu Funayama , Mikiro Arai , Hayato Nishii , Takeshi Isoda
IPC分类号： D01F9/10 , C04B35/589 , C08G77/48 , C08G77/54
CPC分类号： C04B35/589 , C08G77/54
摘要： Novel polysiloxazanes comprising --SiH.sub.2).sub.n NH-- and --SiH.sub.2).sub.m O-- as the main repeating units are provided. The polysiloxazanes are produced by reacting a dihalosilane or an adduct thereof with a Lewis base, with ammonia and water vapor or oxygen. From the polysiloxazane, novel silicon oxynitride shapes can be produced and the silicon oxynitride shapes are essentially composed of silicon, nitride (5 mols % or more) and oxygen (5 mol % or more).

10. 发明授权

US4818611A High-purity silicon nitride fibers 失效
标题翻译：高纯氮化硅纤维
公开(公告)号：US4818611A
公开(公告)日：1989-04-04
申请号：US930803
申请日：1986-11-13
申请人： Mikiro Arai , Osamu Funayama , Hayato Nishii , Takeshi Isoda
发明人： Mikiro Arai , Osamu Funayama , Hayato Nishii , Takeshi Isoda
IPC分类号： D01F9/08 , C01B21/068 , C04B35/589 , D01F9/10 , D02G3/00
CPC分类号： D01F9/10 , C04B35/589 , Y10T428/2904 , Y10T428/2913
摘要： Silicon nitride fibers having a carbon content of 5 weight percent or less have high heat insulating properties and favorable mechanical properties and are useful as heat resistant, highly insulating materials or reinforcing agents for composite materials, particularly in the aerospace industry. Such high purity silicon nitride fibers are produced by spinning a solution of perhydropolysilazanes, an inert solvent and a spinning agent into fibers, preferably continuous fibers, and firing the spun fibers at 800.degree. to 1300.degree. C. in an inert atmosphere to form silicon nitride fibers of high purity.
摘要翻译：碳含量为5重量％以下的氮化硅纤维具有高绝热性和良好的机械性能，并且可用作复合材料特别是在航天工业中的耐热，高绝缘性材料或增强剂。通过将全氢聚硅氮烷，惰性溶剂和纺丝剂的溶液旋转到纤维中，优选连续纤维，并在惰性气氛中在800〜1300℃下焙烧纺丝纤维，从而形成氮化硅高纯度纤维。

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