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1. 发明授权

US4894475A Alpha-acyloxyketone derivatives 失效
标题翻译： α-酰氧基酮衍生物
公开(公告)号：US4894475A
公开(公告)日：1990-01-16
申请号：US138076
申请日：1987-12-28
申请人： Hiroaki Tan , Koji Kato , Junichi Imuta , Noriaki Kihara
发明人： Hiroaki Tan , Koji Kato , Junichi Imuta , Noriaki Kihara
IPC分类号： C07D233/64 , C07C67/00 , C07C313/00 , C07C323/44 , C07D233/54
CPC分类号： C07D233/64 , C07C323/44
摘要： Disclosed are alpha-acyloxyketone derivatives which are useful as intermediates for production of N-cyano-N'-methyl-N"-[2-{(5-methyl-1H-imidazol-4-yl)methylthio}ethyl]guanidine (common name: Cimetidine; Cimetidine applies hereinafter) and Cimetidine-related compounds which have an action of controlling secretion of gastric acid and are useful as a drug for treating gastric ulcer.

2. 发明授权

US4886910A Cyanoguanidine derivative and process for preparation thereof 失效
公开(公告)号：US4886910A
公开(公告)日：1989-12-12
申请号：US156658
申请日：1988-02-17
申请人： Hiroaki Tan , Koji Kato , Junichi Imuta , Noriaki Kihara
发明人： Hiroaki Tan , Koji Kato , Junichi Imuta , Noriaki Kihara
IPC分类号： C07C319/20 , C07C67/00 , C07C313/00 , C07C323/44 , C07D233/54 , C07D233/64
CPC分类号： C07D233/64 , C07C323/44
摘要： The present invention provides a cyanoguanidine derivtive which is a precursor for the synthesis of N-cyano-N'-methyl-N"-[2-{(5-methyl-1H-imidazol-4-yl)methylothio}ethyl]-guanidine (Cimetidine) or its relted compound, which has an action of controlling secretion of acid in the stomach based on the histamine H.sub.2 receptor antagonism and is valuable as a drug for treating gastric ulcer. This cyanoguanidine derivative is prepared by reacting a haloketone derivative with an ammonium salt and a lower fatty acid salt or by reacting other cyanoguanidine derivative with an ammonium salt.

3. 发明授权

US5072007A Process for preparing polyalkyl-2-alkoxy-7-hydroxychroman derivatives 失效
标题翻译：制备聚烷基-2-羟基-7-羟基喹啉衍生物的方法
公开(公告)号：US5072007A
公开(公告)日：1991-12-10
申请号：US547132
申请日：1990-07-03
申请人： Daisuke Fukuoka , Takeshi Ishitoku , Katsuya Takahashi , Takashi Tashiro , Junichi Imuta , Hiroaki Tan , Masaharu Ishiguro , Noriaki Kihara , Teruaki Mukaiyama
发明人： Daisuke Fukuoka , Takeshi Ishitoku , Katsuya Takahashi , Takashi Tashiro , Junichi Imuta , Hiroaki Tan , Masaharu Ishiguro , Noriaki Kihara , Teruaki Mukaiyama
IPC分类号： C07D311/20
CPC分类号： C07D311/20
摘要： Process for preparing polyalkyl-2-alkoxy-7-hydroxychroman derivative of the general formula (V): ##STR1## wherein R.sup.1 denotes lower primary alkyl, R.sup.2 denotes hydrogen or lower primary alkyl and R.sup.3 denotes loweralkyl, by reacting resorcin with either an aliphatic ketone of the general formula (I): ##STR2## wherein R.sup.1 and R.sup.2 are as defined above, and an alcohol of the formula (II):R.sup.3 OH (II)wherein R.sup.3 is as defined above, in the presence of an acid catalyst, or an aliphatic ketone acetal of the general formula (III): ##STR3## wherein R.sup.1, R.sup.2 and R.sup.3 are as defined above, in the presence of an acid catalyst.

4. 发明授权

US5175313A Process for preparing dihydrofuranone derivatives 失效
标题翻译：制备二氢呋喃酮衍生物的方法
公开(公告)号：US5175313A
公开(公告)日：1992-12-29
申请号：US695323
申请日：1991-05-03
申请人： Junichi Imuta , Aiichiro Ori , Noriaki Kihara
发明人： Junichi Imuta , Aiichiro Ori , Noriaki Kihara
IPC分类号： C07D307/33
CPC分类号： C07D307/33
摘要： The present invention provides a process for preparing dihydrofuranone derivative of the formula (I): ##STR1## wherein R.sup.1 and R.sup.3 are individually lower alkyl, and R.sup.2 is hydrogen or lower alkyl, by reacting a dihydrofuranone derivative of the formula(I): ##STR2## wherein R.sup.1 is as defined above, with a malonic acid derivative of the formula (II): ##STR3## wherein R.sup.2 and R.sup.3 are as defined above, in the presence of an alkalimetal alkoxide and/or an alkalimetal hydroxide.

5. 发明授权

US4973703A Process for purification of N-cyano-N'-methyl-N"-(2-((5-methyl-1Himidazol-4-yl)methylthio)ethyl)guan idine 失效
标题翻译：纯化N-氰基-N'-甲基-N“ - （2 - （（5-甲基-1H-咪唑-4-基）甲硫基）乙基）胍的方法
公开(公告)号：US4973703A
公开(公告)日：1990-11-27
申请号：US267379
申请日：1988-11-04
申请人： Junichi Imuta , Noriaki Kihara , Takeshi Ishitoku
发明人： Junichi Imuta , Noriaki Kihara , Takeshi Ishitoku
IPC分类号： C07D233/54 , C07D233/64
CPC分类号： C07D233/64
摘要： A process for the purification of N-cyano-N'-methyl-N"-[2-{(5-methyl-1H-imidazol-4-yl)methylthio}-ethyl]guanidine, which comprises bringing a crude product of N-cyano-N'-methyl-N"-[2-{(5-methyl-1H-imidazol-4-yl)-methylthio}ethyl]guanidine into contact with activated carbon in water in the presence of an organic acid.

6. 发明授权

US06346070B1 Catalyst for polyester production, process for producing polyester using the catalyst, polyester obtained by the process, and uses of the polyester 有权
标题翻译：用于聚酯生产的催化剂，使用催化剂生产聚酯的方法，通过该方法获得的聚酯和聚酯的用途
公开(公告)号：US06346070B1
公开(公告)日：2002-02-12
申请号：US09470664
申请日：1999-12-22
申请人： Takeshi Ohmatsuzawa , Fujito Ehara , Hideshi Hori , Kazuo Toyota , Kenzaburou Fukutani , Junichi Imuta , Akiyoshi Shimizu , Takayuki Onogi , Seiji Noda , Masayuki Sakai , Shoji Hiraoka , Koji Nakamachi , Michio Tsugawa , Satoru Miyazoe
发明人： Takeshi Ohmatsuzawa , Fujito Ehara , Hideshi Hori , Kazuo Toyota , Kenzaburou Fukutani , Junichi Imuta , Akiyoshi Shimizu , Takayuki Onogi , Seiji Noda , Masayuki Sakai , Shoji Hiraoka , Koji Nakamachi , Michio Tsugawa , Satoru Miyazoe
IPC分类号： C08G6378
CPC分类号： C08G63/85 , C08G63/183 , C08G63/82 , C08G63/88
摘要： The present invention provides a catalyst for polyester production capable of producing a polyester with high catalytic activity and a process for producing a polyester using the catalyst. The catalyst for polyester production comprises a solid titanium compound which is obtained by dehydro-drying a hydrolyzate obtained by hydrolysis of a titanium halide and which has a molar ratio (OH/Ti) of a hydroxyl group (OH) to titanium (Ti) exceeding 0.09 and less than 4. The present invention also provides a method to obtain a polyester having a small increase of the acetaldehyde content during the molding. This method comprises bringing a polyester, which is obtained by the use of a titanium compound catalyst and in which the reaction has been completed, into contact with a phosphoric ester aqueous solution or the like having a concentration of not less than 10 ppm in terms of phosphorus atom. The present invention further provides a polyester having excellent transparency and tint and molded products of the polyester such as a blow molded article, a film, a sheet and a fiber. The polyester is obtained by polycondensing an aromatic dicarboxylic acid or an ester-forming derivative thereof and an aliphatic diol or an ester-forming derivative thereof in the presence of a catalyst for polyester production which comprises a polycondensation catalyst component comprising a solid titanium compound and a co-catalyst component comprising a magnesium compound. This polyester has a titanium content of 1 to 100 ppm, a magnesium content of 1 to 200 ppm and a weight ratio (Mg/Ti) of magnesium to titanium of not less than 0.01.
摘要翻译：本发明提供一种能够生产具有高催化活性的聚酯的聚酯制造催化剂和使用该催化剂生产聚酯的方法。用于聚酯生产的催化剂包括固体钛化合物，其通过脱水干燥由卤化钛水解得到的水解产物并且具有羟基（OH）与钛（Ti）的摩尔比（OH / Ti）超过钛 0.09以上且低于4.本发明还提供一种在成型时获得乙醛含量增加少的聚酯的方法。该方法包括使通过使用钛化合物催化剂获得的反应已完成的聚酯与浓度不小于10ppm的磷酸酯水溶液等接触，换算为磷原子。本发明还提供一种聚酯，其具有优异的透明度和色调，并且聚酯的成型产品如吹塑制品，薄膜，片材和纤维。在聚酯制造用催化剂的存在下，通过将芳香族二羧酸或其成酯性衍生物和脂肪族二醇或其成酯衍生物缩聚得到聚酯，该催化剂包括含有固体钛化合物的缩聚催化剂组分和助催化剂组分包含镁化合物。该聚酯的钛含量为1〜100ppm，镁含量为1〜200ppm，镁与钛的重量比（Mg / Ti）为0.01以上。

7. 发明授权

US6004897A Olefin polymerization catalyst, process for preparing olefin polymer, and olefin polymer 失效
标题翻译：烯烃聚合催化剂，制备烯烃聚合物的方法和烯烃聚合物
公开(公告)号：US6004897A
公开(公告)日：1999-12-21
申请号：US683068
申请日：1996-07-16
申请人： Junichi Imuta , Masayasu Yoshida , Yasushi Tohi
发明人： Junichi Imuta , Masayasu Yoshida , Yasushi Tohi
IPC分类号： C07F17/00 , C08F4/42 , C08F4/64 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F110/02 , C08F110/06 , C08F210/16
CPC分类号： C07F17/00 , C08F10/00 , C08F110/02 , C08F110/06 , C08F210/16 , C08F4/65908 , C08F4/65912 , C08F4/65916 , C08F4/65927 , Y10S526/943
摘要： The olefin polymerization catalyst of the invention is formed from a Group IVB transition metal compound represented by the following formula (I) and an organoaluminum oxy-compound or a compound which reacts with the transition metal compound to form an ion pair. In the olefin polymerization process of the invention using this catalyst or a catalyst formed from a Group IVB transition metal compound represented by the following formula (II) and an organoaluminum oxy-compound or a compound which reacts with the transition metal compound to form an ion pair, an olefin (co)polymer having a high molecular weight can be obtained with high polymerization activities, and besides an olefin copolymer having a high comonomer content can be obtained even if a comonomer is used in a small amount. ##STR1## wherein, M is a transition metal of Group IVB, at least one of R.sup.1 is an aryl group and the remainder is hydrogen or the like, R.sup.2 is hydrogen, an alkyl group or the like, R.sup.3 and R.sup.4 are each hydrogen, an alkyl group or the like, R.sup.6 is hydrogen, an alkyl group or the like, R.sup.7 is hydrogen, an alkyl group or the like, any one of R.sup.8 and R.sup.9 is an alkyl group, and X.sup.1 and X.sup.2 are each halogen, a hydrocarbon group or the like.
摘要翻译：本发明的烯烃聚合催化剂由下式（I）表示的ⅣB族过渡金属化合物和有机铝氧化合物或与过渡金属化合物反应形成离子对的化合物形成。在使用该催化剂的本发明的烯烃聚合方法或由下式（II）表示的IVB族过渡金属化合物和有机铝氧化合物或与过渡金属化合物反应形成离子的化合物形成的催化剂可以以高聚合活性获得具有高分子量的烯烃（共）聚合物，并且即使使用少量共聚单体，也可以获得具有高共聚单体含量的烯烃共聚物。其中，M是IVB族的过渡金属，R 1中的至少一个是芳基，其余是氢等，R 2是氢，烷基等，R 3和R 4各自是氢，烷基 R 6为氢，烷基等，R 7为氢，烷基等，R 8和R 9中的任一个为烷基，X 1和X 2各自为卤素，烃基或喜欢。

8. 发明授权

US5629254A Substituted indenyl ring containing metallocene catalyst for propylene polymerization process 失效
标题翻译：用于丙烯聚合方法的含有茂金属催化剂的取代的茚基环
公开(公告)号：US5629254A
公开(公告)日：1997-05-13
申请号：US486642
申请日：1995-06-07
申请人： Daisuke Fukuoka , Takashi Tashiro , Koji Kawaai , Junji Saito , Takashi Ueda , Yoshihisa Kiso , Junichi Imuta , Terunori Fujita , Masatoshi Nitabaru , Masayasu Yoshida
发明人： Daisuke Fukuoka , Takashi Tashiro , Koji Kawaai , Junji Saito , Takashi Ueda , Yoshihisa Kiso , Junichi Imuta , Terunori Fujita , Masatoshi Nitabaru , Masayasu Yoshida
IPC分类号： C07C45/46 , C07C49/67 , C07C49/697 , C07F17/00 , C08F4/60 , C08F4/602 , C08F4/619 , C08F4/6192 , C08F4/64 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F10/06 , C08F110/06 , C08F210/06 , C08F210/16
CPC分类号： C08F210/16 , C07C45/46 , C07C49/67 , C07C49/697 , C07F17/00 , C08F10/00 , C08F10/06 , C08F110/06 , C08F210/06 , C08F4/61912 , C08F4/61927 , C08F4/65908 , C08F4/65912 , C08F4/65916 , C08F4/65927 , Y10S526/904 , Y10S526/943
摘要： The novel transition metal catalyst of the invention is represented by the following formula (I): ##STR1## wherein M is a zirconium or hafnium; R.sup.1 is a hydrocarbon group of 2 to 6 carbon atoms, R.sup.2 is an aryl group of 6 to 16 carbon atoms; X.sup.1 and X.sup.2 are each a halogen atom; and Y is a divalent hydrocarbon group, a divalent silicon-containing group.
摘要翻译：本发明的新型过渡金属催化剂由下式（I）表示： R 1是2至6个碳原子的烃基，R 2是6至16个碳原子的芳基; X1和X2各自为卤素原子; Y为二价烃基，二价含硅基团。

9. 发明授权

US07714087B2 Polar group-containing olefin copolymer, process for preparing the same, thermoplastic resin composition containing the copolymer, and uses thereof 有权
标题翻译：含极性基团的烯烃共聚物，其制备方法，含有共聚物的热塑性树脂组合物及其用途
公开(公告)号：US07714087B2
公开(公告)日：2010-05-11
申请号：US12153003
申请日：2008-05-12
申请人： Junichi Imuta , Norio Kashiwa , Seiji Ota , Satoru Moriya , Tadahito Nobori , Kazumi Mizutani
发明人： Junichi Imuta , Norio Kashiwa , Seiji Ota , Satoru Moriya , Tadahito Nobori , Kazumi Mizutani
IPC分类号： C08F232/08
CPC分类号： C08F297/02 , C08F4/65912 , C08F4/6592 , C08F210/00 , C08F210/02 , C08F210/06 , C08F210/08 , C08F210/14 , C08F210/16 , C08J5/18 , C08J2351/06 , C08J2371/02 , C08J2387/00 , C08L53/00 , C08L2666/02 , C09J153/00 , C08F4/65927 , C08F222/06 , C08F2500/03 , C08F2500/12 , C08F2500/09 , C08F216/00
摘要： A polar group-containing olefin copolymer having excellent adhesion properties to metals or polar resins and excellent compatibility therewith, a process for preparing the copolymer, a thermoplastic resin composition containing the copolymer, and uses thereof. The polar group-containing olefin copolymer comprises a constituent unit derived from an □-olefin of 2 to 20 carbon atoms, and a constituent unit derived from a straight-chain, branched or cyclic polar group-containing monomer having at the end a polar group such as a hydroxyl group or an epoxy group and/or a constituent unit derived from a macromonomer having at the end a polymer segment obtained by anionic polymerization, ring-opening polymerization or polycondensation. The polar group-containing olefin copolymer can be prepared by polymerizing the α-olefin with the polar group-containing monomer and/or the macromonomer in the presence of a metallocene catalyst. The polar group-containing olefin copolymer and the thermoplastic resin composition containing the copolymer are used for films, sheets, modifiers, building/civil engineering materials, automobile exterior trim, electric/electronic parts, coating bases, compatibilizing agents, etc.
摘要翻译：含有金属或极性树脂的粘合性优异的极性基团的烯烃共聚物，与其相容性优异的共聚物的制备方法，含有共聚物的热塑性树脂组合物及其用途。含有极性基团的烯烃共聚物包含衍生自2〜20个碳原子的α-烯烃的结构单元，以及衍生自具有极性基团的直链，支链或环状极性基团单体的结构单元例如羟基或环氧基和/或衍生自大分子单体的结构单元，其末端具有通过阴离子聚合，开环聚合或缩聚获得的聚合物链段。含极性基团的烯烃共聚物可以通过在茂金属催化剂的存在下与含极性基团的单体和/或大分子单体进行聚合来制备。含有极性基团的烯烃共聚物和含有共聚物的热塑性树脂组合物用于薄膜，片材，改性剂，建筑/土木工程材料，汽车外饰件，电气/电子部件，涂料基料，相容剂等。

10. 发明申请

US20090137757A1 Polar group-containing olefin copolymer, process for preparing the same, thermoplastic resin composition containing the copolymer, and uses thereof 有权
标题翻译：含极性基团的烯烃共聚物，其制备方法，含有共聚物的热塑性树脂组合物及其用途
公开(公告)号：US20090137757A1
公开(公告)日：2009-05-28
申请号：US12153003
申请日：2008-05-12
申请人： Junichi Imuta , Norio Kashiwa , Seiji Ota , Satoru Moriya , Tadahito Nobori , Kazumi Mizutani
发明人： Junichi Imuta , Norio Kashiwa , Seiji Ota , Satoru Moriya , Tadahito Nobori , Kazumi Mizutani
IPC分类号： C08F4/44
CPC分类号： C08F297/02 , C08F4/65912 , C08F4/6592 , C08F210/00 , C08F210/02 , C08F210/06 , C08F210/08 , C08F210/14 , C08F210/16 , C08J5/18 , C08J2351/06 , C08J2371/02 , C08J2387/00 , C08L53/00 , C08L2666/02 , C09J153/00 , C08F4/65927 , C08F222/06 , C08F2500/03 , C08F2500/12 , C08F2500/09 , C08F216/00
摘要： A polar group-containing olefin copolymer having excellent adhesion properties to metals or polar resins and excellent compatibility therewith, a process for preparing the copolymer, a thermoplastic resin composition containing the copolymer, and uses thereof. The polar group-containing olefin copolymer comprises a constituent unit derived from an □-olefin of 2 to 20 carbon atoms, and a constituent unit derived from a straight-chain, branched or cyclic polar group-containing monomer having at the end a polar group such as a hydroxyl group or an epoxy group and/or a constituent unit derived from a macromonomer having at the end a polymer segment obtained by anionic polymerization, ring-opening polymerization or polycondensation. The polar group-containing olefin copolymer can be prepared by polymerizing the α-olefin with the polar group-containing monomer and/or the macromonomer in the presence of a metallocene catalyst. The polar group-containing olefin copolymer and the thermoplastic resin composition containing the copolymer are used for films, sheets, modifiers, building/civil engineering materials, automobile exterior trim, electric/electronic parts, coating bases, compatibilizing agents, etc.
摘要翻译：含有金属或极性树脂的粘合性优异的极性基团的烯烃共聚物，与其相容性优异的共聚物的制备方法，含有共聚物的热塑性树脂组合物及其用途。含有极性基团的烯烃共聚物包含衍生自2〜20个碳原子的α-烯烃的结构单元，以及衍生自具有极性基团的直链，支链或环状极性基团单体的结构单元例如羟基或环氧基和/或衍生自大分子单体的结构单元，其末端具有通过阴离子聚合，开环聚合或缩聚获得的聚合物链段。含极性基团的烯烃共聚物可以通过在金属茂催化剂的存在下将α-烯烃与含极性基团的单体和/或大分子单体进行聚合来制备。含有极性基团的烯烃共聚物和含有共聚物的热塑性树脂组合物用于薄膜，片材，改性剂，建筑/土木工程材料，汽车外饰件，电气/电子部件，涂料基料，相容剂等。

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