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1. 发明授权

US5126393A Water-dispersible binder composition, a process for the production of a stoving filler and a coating prepared therefrom 失效
标题翻译：水分散性组合物，生产填充填料的方法及其制备的涂料
公开(公告)号：US5126393A
公开(公告)日：1992-06-30
申请号：US602595
申请日：1990-10-24
申请人： Harald Blum , Jurgen Meixner , Josef Pedain , Hans-Heribert Burgdorfer
发明人： Harald Blum , Jurgen Meixner , Josef Pedain , Hans-Heribert Burgdorfer
IPC分类号： C08G18/00 , B01F17/42 , C08G18/08 , C08G18/10 , C08G18/12 , C08G18/42 , C08G18/66 , C08G18/75 , C09D161/20 , C09D175/06
CPC分类号： C08G18/12 , C08G18/0823 , C08G18/423 , C08G18/4288 , C08G18/6659 , C08G18/75 , C09D175/06
摘要： The present invention relates to a water-dispersible binder composition which is suitable for the production of a stoving filler to be processed from the aqueous phase and which containsa) 65 to 95% by weight of a urethane-modified polyester resin containing carboxyl groups,b) 5 to 35% by weight of a crosslinker resin andc) 0 to 2% by weight of an emulsifier,wherein the percentages are based on the total weight of components a) to c), characterized in that component a) has an acid value of 15 to 36, a hydroxyl value of at least 40 and a molecular weight (M.sub.w) of 5,000 to 50,000 and has been obtained by reactinga1) 72 to 80% by weight of a polyester polyol having a hydroxyl value of 130 to 200 and an acid value of 1 to 5 anda2) 4 to 7% by weight of a 2,2-bis-(hydroxymethyl)-alkane carboxylic acid or a quantity corresponding to this quantity of acid of a tertiary amine salt of such an acid witha3) 15 to 24% by weight of at least one cycloaliphatic diisocyanate having a molecular weight of 166 to 294,wherein the percentages are based on the total weight of components a1) to a3).The present invention also relates to a process for the production of an aqueous stoving filler which is suitable for the production of chip resistant coatings and to the chip resistant coatings produced therefrom.
摘要翻译：本发明涉及一种水分散性粘合剂组合物，其适用于从水相制备待加工的烘干填料，其含有a）65至95重量％的含有羧基的氨基甲酸酯改性的聚酯树脂， b）5〜35重量％的交联剂树脂和c）0〜2重量％的乳化剂，其中所述百分比基于组分a）至c）的总重量，其特征在于组分a）具有酸值为15〜36，羟基值为40以上，分子量（Mw）为5,000〜50,000，通过使a1〜72〜80重量％的羟基值为130的聚酯多元醇与 200，酸值1〜5，a2）4〜7重量％的2,2-双 - （羟甲基） - 烷烃羧酸，或相当于该量的这种叔胺盐的酸量酸与a3）15至24重量％的至少一种具有分子的脂环族二异氰酸酯 166至294的百分比，其中百分比基于组分a1）至a3）的总重量。本发明还涉及一种用于生产水性烘干填料的方法，该方法适用于生产耐屑涂层和由其制备的耐芯片涂层。

2. 发明授权

US5280062A Aqueous polyesters, a process for their production and their use in high-solids stoving lacquers 失效
标题翻译：水性聚酯，其生产方法及其在高固体烘干漆中的应用
公开(公告)号：US5280062A
公开(公告)日：1994-01-18
申请号：US821102
申请日：1992-01-15
申请人： Harald Blum , Hans-Heribert Burgdorfer , Armin Sickert , Peter Hohlein
发明人： Harald Blum , Hans-Heribert Burgdorfer , Armin Sickert , Peter Hohlein
IPC分类号： C08G18/00 , C08G18/08 , C08G18/10 , C08G18/12 , C08G18/65 , C08G18/66 , C09D5/00 , C09D175/04 , C09D175/06 , C08J3/00 , C08K3/20 , C08L75/00
CPC分类号： C08G18/12 , C08G18/0823 , C08G18/10 , C08G18/6659 , C09D175/06
摘要： The present invention relates to aqueous polyesters for high-solids stoving coatings which containa) 35.0 to 65.0% by weight of a polyester resin containing urethane, carboxyl and hydroxyl groups and containing the reaction product of77 to 89% by weight of a branched polyester polyol having a hydroxyl number of 125 to 175, an acid number of less than 4 and a molecular weight of 2,500 to 6,500,2) 2.5 to 4.5% by weight of a 2,2-bis-(hydroxymethyl)alkane carboxylic acid,3) 0 to 3.5% by weight of a diol component having a molecular weight of 62 to 250 and4) 9 to 19% by weight of a diisocyanate component, wherein the percentages of a1), a2), a3) and a4) add up to 100%, based on the weight of a1), a2), a3) and a4),b) 0.1 to 1.5% by weight of a basic neutralizing agent which is sufficient to convert 35 to 100% of the carboxyl groups of component a) to carboxylate groups,c) 0 to 7.5% by weight of an organic auxiliary solvent andd) 26 to 64.9% by weight water,wherein the percentages of a), b), c) and d) add up to 100%, based on the weight of a), b), c) and d).
摘要翻译：含有a）35至65重量％的含有氨基甲酸酯，羧基和羟基的聚酯树脂的水性聚酯，b）0.1至1.5重量％的碱性中和剂，c）0至7.5重量％的有机溶剂，和d）26-64.9重量％的水，其中氨基甲酸酯改性的聚酯树脂a）已经通过选择的原料反应制备; 其粘合剂基本上包含这些聚酯，交联树脂和任选的其它羟基官能聚合物的水性烘烤搪瓷（油漆，清漆）以及在涂料，涂料组合物和密封剂中使用聚酯，任选地与交联树脂和其它水相容的粘合剂组合。

3. 发明授权

US5135987A Modified copolymers, a process for their production, binders containing the modified copolymers and their use in coating compositions and sealing compounds 失效
标题翻译：改性共聚物，其制备方法，含有改性共聚物的粘合剂及其在涂料组合物和密封化合物中的用途
公开(公告)号：US5135987A
公开(公告)日：1992-08-04
申请号：US648537
申请日：1991-02-22
申请人： Christian Wamprecht , Harald Blum , Josef Pedain , Peter Hohlein
发明人： Christian Wamprecht , Harald Blum , Josef Pedain , Peter Hohlein
IPC分类号： C08F8/00 , C08F8/30
CPC分类号： C08F8/30 , C08F8/00
摘要： Binders for moisture-hardening coating or sealing compositions contain modified copolymers having a weight average molecular weight of from 1,500 to 75,000 determined by gel permeation chromatography of olefinically unsaturated compounds containing chemically incorporated moieties which are addition-reactive to amino wherein the modified copolymers contain both(i) intramolecular carboxylic anhydride moieties and(ii) olefinically unsaturated (meth)acrylate moieties in chemically bound form as the moieties which are addition-reactive to amino, with the anhydride equivalent weight being in the range from 392 to 9,800 and the (meth)acrylate equivalent weight in the range from 284 to 7,100.
摘要翻译：用于湿润硬化涂层或密封组合物的粘合剂含有通过凝胶渗透色谱法测定的重均分子量为1,500至75,000的改性共聚物，其含有与氨基加成反应的化学引入部分的烯属不饱和化合物，其中改性共聚物含有（ i）分子内羧酸酐部分和（ii）具有化学结合形式的烯属不饱和（甲基）丙烯酸酯部分作为与氨基加成反应的部分，酸酐当量为392-9,800，和（甲基）丙烯酸酯当量在284至7100的范围内。

4. 发明授权

US4990583A Copolymers containing isocyanate and acid anhydride groups, a process for their preparation and their use as a binder components 失效
标题翻译：含有异氰酸酯和酸酐基团的共聚物，其制备方法及其作为粘合剂组分的用途
公开(公告)号：US4990583A
公开(公告)日：1991-02-05
申请号：US305744
申请日：1989-02-03
申请人： Christian Wamprecht , Josef Pedain , Harald Blum
发明人： Christian Wamprecht , Josef Pedain , Harald Blum
IPC分类号： C09K3/10 , C08F220/36 , C08F222/04 , C08F246/00 , C08G18/62 , C08G18/72 , C09D133/06 , C09D175/04
CPC分类号： C08G18/728 , C08F220/36 , C08F222/04 , C08F246/00 , C09D133/064
摘要： Copolymers useful in binders for two-component coating compounds or sealing compounds are copolymers having a weight average molecular weight, determined by the gel permeation chromatography method, of from 1500 to 75,000 of olefinically unsaturated compounds containing chemically incorporated moieties capable of undergoing an addition reaction with hydroxyls wherein the copolymers contain, as hydroxyl reactive groups, both(i) from 0.3 to 7.0% by weight of free isocyanate groups and(ii) from 1 to 25% by weight of acid anhydride groups, calculated as C.sub.4 H.sub.2 O.sub.3,in a chemically bound form.
摘要翻译：用于双组分涂料化合物或密封化合物的粘合剂中的共聚物是具有通过凝胶渗透色谱法测定的重均分子量为1500至75,000的含有化学引入的部分的烯属不饱和化合物的共聚物，其能够经历与羟基，其中共聚物含有（i）0.3至7.0重量％的游离异氰酸酯基团和（ii）按化学键合计算为1至25重量％的以C 4 H 2 O 3计算的酸酐基团，作为羟基反应性基团形成。

5. 发明授权

US06197874B1 Polyurethane-polyacrylate hybrid dispersions containing allophanate groups 失效
标题翻译：含有脲基甲酸酯基团的聚氨酯 - 聚丙烯酸酯混合分散体
公开(公告)号：US06197874B1
公开(公告)日：2001-03-06
申请号：US09234866
申请日：1999-01-21
申请人： Christoph Irle , Harald Blum , Martin Brahm , Wolfgang Kremer , Rolf Roschu , Erhard Lühmann , Josef Pedain , Christian Wamprecht
发明人： Christoph Irle , Harald Blum , Martin Brahm , Wolfgang Kremer , Rolf Roschu , Erhard Lühmann , Josef Pedain , Christian Wamprecht
IPC分类号： C08J300
CPC分类号： C08G18/12 , C08G18/0823 , C08G18/7837 , C09D175/04 , C08G18/3228 , C08L33/00
摘要： The present invention relates to polyurethane-polyacrylate hybrid dispersions comprising A) 20 to 99% by weight, based on resin solids, of a polyurethane wherein i) the polyurethane is rendered hydrophilic by ionic and/or nonionic hydrophilic groups and ii) the polyisocyanate component used to prepare the polyurethane contains an aliphatic or cycloaliphatic polyisocyanate containing allophanate groups, and B) 1 to 80% by weight, based on resin solids) of a polyacrylate polymer, wherein the sum of components A and B is 100%, based on the total weight of A) and B). The present invention also relates to the use of these hybrid dispersions for coating substrates, in particular wood.
摘要翻译：本发明涉及聚氨酯 - 聚丙烯酸酯混合分散体，其包含A）基于树脂固体为20至99重量％的聚氨酯，其中i）通过离子和/或非离子亲水基团使聚氨酯变得亲水，和ii）所使用的多异氰酸酯组分为了制备聚氨酯，含有含有脲基甲酸酯基团的脂肪族或脂环族多异氰酸酯，B）1〜80重量％，基于树脂固体）聚丙烯酸酯聚合物，其中组分A和B的总和为100重量％，基于总重量的A）和B）。本发明还涉及这些混合分散体用于涂覆基材，特别是木材的用途。

6. 发明授权

US5268428A Binder compositions and their use in coating compositions and sealing compositions 失效
标题翻译：粘合剂组合物及其在涂料组合物和密封组合物中的用途
公开(公告)号：US5268428A
公开(公告)日：1993-12-07
申请号：US748297
申请日：1991-08-21
申请人： Christian Wamprecht , Harald Blum , Josef Pedain
发明人： Christian Wamprecht , Harald Blum , Josef Pedain
IPC分类号： C08G59/20 , C08G59/00 , C08G59/32 , C08K5/05 , C08L35/00 , C08L63/00 , C08L75/04 , C09D5/34 , C09D133/14 , C09D163/00 , C09D167/00 , C08F8/14 , C08L33/08
CPC分类号： C09D133/14 , C09D167/00 , C09D5/34 , C08L75/04
摘要： The present invention relates to binder compositions containingA) 10 to 99 parts by weight of a copolymer component containing at least one copolymer prepared from olefinically unsaturated compositions having a weight average molecular weight of 1,500 to 75,000 and having in chemically bound form both(i) 1 to 30% by weight of cyclic carboxylic anhydride groups (calculated as C.sub.4 H.sub.2 O.sub.3) and(ii) 1 to 29% by weight of epoxide groups (calculated as C.sub.2 H.sub.3 O) andB) 1 to 90 parts by weight of a hydroxyl component containing at least one organic polyol having at least two hydroxyl groups per molecule,provided that for every anhydride group of component A) there are 0.1 to 10 hydroxyl groups of component B).The present invention also relates to the use of these binder compositions as binders for heat-curing coating compositions or sealing compositions optionally containing paint auxiliaries and additives or as binders for room-temperature-curing sealing or coating compositions containing catalysts and, optionally, other paint auxiliaries and additives.
摘要翻译：本发明涉及粘合剂组合物，其包含A）10至99重量份的共聚物组分，所述共聚物组分含有至少一种由烯属不饱和组合物制备的共聚物，其重均分子量为1,500至75,000，并具有化学键合形式，（i） 1至30重量％的环状羧酸酐基团（以C 4 H 2 O 3计）和（ii）1至29重量％的环氧基团（以C 2 H 3 O计算）和B）1至90重量份的至少含有至少一个每分子具有至少两个羟基的有机多元醇，条件是对于组分A）的每个酸酐基团，组分B）中都有0.1至10个羟基。本发明还涉及这些粘合剂组合物作为粘合剂用于热固化涂料组合物或任选地含有涂料助剂和添加剂的密封组合物或用作室温固化密封剂的粘合剂或含有催化剂和任选的其它涂料的涂料组合物的粘合剂助剂和助剂。

7. 发明授权

US5189176A Bis-oxazolidines, oxazolidine mixtures consisting essentially thereof and their use as hardeners for plastics precursors containing isocyanate groups 失效
标题翻译： BIS-氧杂环丁烷，氧杂环丁烷混合物及其作为含有异氰酸酯基团的塑料前体的硬化剂
公开(公告)号：US5189176A
公开(公告)日：1993-02-23
申请号：US723863
申请日：1991-07-01
申请人： Harald Blum , Josef Pedain , Karl-Heinz Hentschel
发明人： Harald Blum , Josef Pedain , Karl-Heinz Hentschel
IPC分类号： C07D263/04 , C08G18/32 , C08G18/38
CPC分类号： C07D263/04 , C08G18/3296 , C08G18/3844
摘要： The present invention relates to bis-oxazolidines corresponding to formula (II) ##STR1## wherein R represents a branched, saturated, aliphatic hydrocarbon radical containing 5 to 8 carbon atoms.The present invention also relates to oxazolidine mixtures, which are also suitable as hardeners for plastics precursors containing isocyanate groups, consisting essentially ofa) bis-oxazolidines corresponding to formula (II) above andb) 0.03 to 0.3 moles per mole of component (a), of compounds corresponding to formula (III) ##STR2## wherein R represents a saturated, branched, aliphatic hydrocarbon radical containing 5 to 8 carbon atoms.The present invention additionally relates to a process for the production of these oxazolidine mixtures and to their use in combination with polymer precursors containing isocyanate groups for coating or sealing compositions.
摘要翻译：本发明涉及对应于式（II）的二恶唑烷（II）其中R表示含有5-8个碳原子的支链饱和脂族烃基。本发明还涉及恶唑烷混合物，其也适合作为含有异氰酸酯基团的塑料前体的硬化剂，其基本上由a）对应于上述式（II）的双恶唑烷和b）每摩尔组分0.03至0.3摩尔（a ），对应于式（III）的化合物其中R表示含有5至8个碳原子的饱和支链脂族烃基。本发明还涉及制备这些恶唑烷混合物的方法，以及它们与含有用于涂覆或密封组合物的异氰酸酯基团的聚合物前体组合使用的方法。

8. 发明授权

US4937293A Moisture-hardening binder compositions, a process for their production and their use 失效
标题翻译：水分固化粘合剂组合物，其制备方法及其用途
公开(公告)号：US4937293A
公开(公告)日：1990-06-26
申请号：US170941
申请日：1988-03-21
申请人： Harald Blum , Josef Pedain , Christian Wamprecht
发明人： Harald Blum , Josef Pedain , Christian Wamprecht
IPC分类号： C09K3/10 , C08K5/29 , C08L33/04 , C08L33/06 , C08L35/00 , C09D133/02 , C09D133/04 , C09D135/00 , C09D151/00
CPC分类号： C08K5/29 , C09D135/00
摘要： Binder compositions comprising(A) copolymers having a molecular weight of from 1500 to 75000 of maleic acid anhydride with other selected olefinically unsaturated monomers,(B) organic polyamines with aldimine- and/or ketimine-blocked amino groups and, optionally, reaction products containing amide groups of (i) copolymers (A) with (ii) polyamines having free and blocked amino groups,a process for the production of these compositions by mixing components (A) and (B) and optionally partially blocked polyamines which react with a part of component (A) under formation of component (C) as well as the use of these binder compositions as binder in lacquers, coating compositions or sealing compounds.
摘要翻译：粘合剂组合物，其包含（A）分子量为1500至75000的马来酸酐与其它选择的烯属不饱和单体的共聚物，（B）具有亚胺基和/或酮亚胺封端的氨基的有机多胺，以及任选地含有（i）共聚物（A）与（ii）具有游离和封闭氨基的多胺的酰胺基团，通过混合组分（A）和（B）并任选部分封闭的多胺与部分反应的方法制备这些组合物的方法的组分（A），以及这些粘合剂组合物作为涂料，涂料组合物或密封化合物中的粘合剂的用途。

9. 发明授权

US5741849A Aqueous binder compositions having a long processing time and their use in coating compositions 失效
标题翻译：具有长处理时间的水性粘合剂组合物及其在涂料组合物中的用途
公开(公告)号：US5741849A
公开(公告)日：1998-04-21
申请号：US666166
申请日：1996-06-19
申请人： Harald Blum , Eberhard Arning , Rolf Roschu , Josef Pedain
发明人： Harald Blum , Eberhard Arning , Rolf Roschu , Josef Pedain
IPC分类号： C08L75/04 , C08G18/00 , C08G18/08 , C08G18/42 , C08G18/46 , C08G18/64 , C08L75/00 , C09D175/00 , C09D175/04 , C09D175/06 , C08J3/00 , B32B27/00 , C08K3/20
CPC分类号： C09D175/04 , C09D175/06 , Y10T428/31551
摘要： The invention relates to an aqueous binder composition having a long processing time (time within which the mixture can be processed without loss of quality) based on aqueous dispersions or solutions of binder mixtures, which contain at least one hydroxyl-group containing polyester dispersion or solution, at least one physically drying, aqueous polyurethane dispersion that is substantially free from hydroxyl or amino groups, and a polyisocyanate. The present invention also relates to the use of these binders in lacquers and coating compositions, in particular for coating rigid, non-flexible substrates.
摘要翻译：本发明涉及基于包含至少一种含羟基的聚酯分散体或溶液的粘合剂混合物的水性分散体或溶液具有长的处理时间（混合物可以在不损失质量的时间内处理时间）的水性粘合剂组合物，至少一种基本上不含羟基或氨基的物理干燥的水性聚氨酯分散体和多异氰酸酯。本发明还涉及这些粘合剂在漆和涂料组合物中的用途，特别是用于涂覆刚性的非柔性基材。

10. 发明授权

US5294665A Water soluble or water dispersible polyisocyanate mixtures and their use in stoving compositions 失效
标题翻译：水溶性或水分散性多异氰酸酯混合物及其在烘烤组合物中的用途
公开(公告)号：US5294665A
公开(公告)日：1994-03-15
申请号：US82224
申请日：1993-06-24
申请人： Josef Pedain , Heino Muller , Dieter Mager , Harald Blum , Holger Casselmann
发明人： Josef Pedain , Heino Muller , Dieter Mager , Harald Blum , Holger Casselmann
IPC分类号： C08G18/83 , C08G18/00 , C08G18/08 , C08G18/10 , C08G18/42 , C08G18/66 , C08G18/70 , C08G18/80 , C09D175/00 , C09D175/06
CPC分类号： C08G18/8061 , C08G18/0823 , C08G18/4277 , C08G18/6659 , C08G18/706 , C08G18/8048
摘要： The present invention relates to a polyisocyanate mixture which has blocked isocyanate groups and an average NCO-functionality, based on reversibly blocked isocyanate groups, of 2.0 to 2.6, and is the reaction product, converted into the salt form by the at least partial neutralization of the incorporated carboxyl groups, ofi) at least one organic diisocyanate having a molecular weight of 168 to 300 withii) at least one monofunctional blocking agent for isocyanate groups,iii) at least one monobasic or dibasic hydroxycarboxylic acid,iv) 1 to 15 wt. %, based on the weight of component i), of at least one dihydric to hexahydric alcohol having a molecular weight of 62 to 182 andv) 50 to 500 wt. %, based on the weight of component i), of at least one diol having a molecular weight of 350 to 950 and containing ester groups.The present invention also relates to the use of this polyisocyanate mixture in combination with water dispersible or water soluble polyhydroxyl compounds for the production of aqueous stoving lacquers.
摘要翻译：本发明涉及具有封端异氰酸酯基团和基于可逆封端异氰酸酯基团的平均NCO官能度为2.0至2.6的多异氰酸酯混合物，并且是反应产物，通过至少部分中和 i）至少一种分子量为168至300的有机二异氰酸酯，ii）至少一种用于异氰酸酯基团的单官能封端剂，iii）至少一种一元或二元羟基羧酸，iv）1至15 重量至少一种分子量为62至182的二羟基至六元醇，v）50至500重量％，基于组分i）的重量％基于组分i）的重量，至少一种分子量为350至950的二醇并含有酯基。本发明还涉及这种多异氰酸酯混合物与水分散性或水溶性多羟基化合物的组合用于生产含水烘烤漆的用途。

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