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1. 发明申请

US20080146708A1 Salts of asymmetrically substituted bis (1-hydroxymethyl)phosphinic acids 审中-公开
标题翻译：不对称取代的双（1-羟甲基）次膦酸的盐
公开(公告)号：US20080146708A1
公开(公告)日：2008-06-19
申请号：US12002136
申请日：2007-12-14
申请人： Harald Bauer , Werner Krause , Wiebke Maas
发明人： Harald Bauer , Werner Krause , Wiebke Maas
IPC分类号： C08K5/51 , C07F9/30
CPC分类号： C09K21/12 , C07F9/301 , C08K5/5313
摘要： The invention relates to salts of asymmetrically substituted bis(1-hydroxymethyl)phosphinic acids, of the formula (I) A-P(═O)(OX)—B (I) in whichA is R1R2C(OH)— and B is R3R4C(OH)—, with the proviso that the respective groups R1R2C(OH)— and —C(OH)R3R4 are always different, and where R1, R2, R3, and R4 are hydrogen, alkyl, alkenyl, alkynyl, aralkyl, aryl and/or substituted aryl, andX is an element of the first main group, an element of the second main or transition group, an element of the third main or transition group, an element of the fourth main or transition group, an element of the eighth transition group and/ora nitrogen base.
摘要翻译：本发明涉及不对称取代的双（1-羟甲基）次膦酸的式（I）的化合物<？in-line-formula description =“In-line formula”end =“lead”？> AP（-O）（OX）-B（I）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中A是R 1 R 2 C（OH） - 和B是R 3 R 4 C（OH） - ，条件是各个基团R 1， R 2 C（OH） - 和-C（OH）R 3 R 4 R 3总是不同的，并且其中R 1， R 2，R 3，R 3和R 4是氢，烷基，烯基，炔基，芳烷基，芳基和/或取代的芳基，X是第一主要组分的元素，第二主要或转移基团的元素，第三主要或转移基团的元素，第四主体或转移基团的元素，第八过渡组的元素和/或氮碱。

2. 发明授权

US08097753B2 Mixtures composed or monocarboxy-functionalized dialkylphosphinic acids, their use and a process for their preparation 有权
标题翻译：混合物或单羧基官能化二烷基次膦酸，其用途及其制备方法
公开(公告)号：US08097753B2
公开(公告)日：2012-01-17
申请号：US11714482
申请日：2007-03-06
申请人： Wiebke Maas , Werner Krause , Harald Bauer
发明人： Wiebke Maas , Werner Krause , Harald Bauer
IPC分类号： C07F9/22
CPC分类号： C08K5/5313 , C07F9/301 , C07F9/306 , C08K2201/014
摘要： The invention relates to mixtures composed of monocarboxy-functionalized dialkylphosphinic acids and of further components, which comprise A) from 98 to 100% by weight of monocarboxy-functionalized dialkylphosphinic acids of the formula (I) in which R1, R2, R3, R4, R5, R6, and R7 are identical or different and, independently of one another, are H, methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, tert-butyl, and/or phenyl, X and Y are identical or different and, independently of one another, are H, Li, Na, K, or NH4, and B) from 0 to 2% by weight of halogens, where the entirety of the components always amounts to 100% by weight.
摘要翻译：本发明涉及由单羧基官能化的二烷基次膦酸和其它组分组成的混合物，其包含A）98至100重量％的式（I）的单羧基官能化二烷基次膦酸，其中R 1，R 2，R 3，R 4， R 5，R 6和R 7是相同或不同的，彼此独立地是H，甲基，乙基，正丙基，异丙基，正丁基，异丁基，叔丁基和/或苯基，X和Y是相同的或者不同，并且彼此独立地是H，Li，Na，K或NH 4，和B）0-2重量％的卤素，其中整个组分总计为100重量％。

3. 发明申请

US20070213563A1 Mixtures composed of monocarboxy-functionalized dialkylphosphinic acid salts, their use und a process for their preparation 审中-公开
标题翻译：由单羧基官能化的二烷基次膦酸盐组成的混合物，其用途及其制备方法
公开(公告)号：US20070213563A1
公开(公告)日：2007-09-13
申请号：US11714331
申请日：2007-03-06
申请人： Wiebke Maas , Werner Krause , Harald Bauer
发明人： Wiebke Maas , Werner Krause , Harald Bauer
IPC分类号： C07F9/02
CPC分类号： C08K5/5313 , C07F9/301
摘要： The invention relates to mixtures composed of monocarboxy-functionalized dialkylphosphinic salts and of further components, which comprise A) from 98 to 100% by weight of monocarboxy-functionalized dialkylphosphinic salts of the formula (I) in which X and Y are different, where X is Ca, Al, or Zn, and Y is methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, tert-butyl, phenyl, 2-hydroxyethyl, 2,3-dihydroxypropyl, 2-hydroxypropyl, 3-hydroxypropyl, 4-hydroxybutyl, 3-hydroxybutyl, 2-hydroxybutyl, and/or 6-hydroxyhexyl, allyl and/or glycerol; or X and Y are different and are Mg, Sb, Sn, Ge, Ti, Fe, Zr, Ce, Bi, Sr, Mn, Cu, Ni, Li, Na, K, H, and/or a protonated nitrogen base; or X and Y are identical or different and each is then Ca, Al, or Zn; R1, R2, R3, R4, R5, R6, and R7 are identical or different and, independently of one another, are H, methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, tert-butyl, and/or phenyl, and B) from 0 to 2% by weight of halogens, where the entirety of the components always amounts to 100% by weight; and to a process for their preparation and to their use.
摘要翻译：本发明涉及由单羧基官能化的二烷基次膦酸盐和其它组分组成的混合物，其包含A）98至100重量％的式（I）的单羧基官能化二烷基次膦酸盐，其中X和Y不同，其中X 是Ca，Al或Zn，Y是甲基，乙基，正丙基，异丙基，正丁基，异丁基，叔丁基，苯基，2-羟乙基，2,3-二羟丙基，2-羟丙基，，4-羟基丁基，3-羟基丁基，2-羟基丁基和/或6-羟基己基，烯丙基和/或甘油; 或X和Y不同，分别为Mg，Sb，Sn，Ge，Ti，Fe，Zr，Ce，Bi，Sr，Mn，Cu，Ni，Li，Na，K，H和/或质子化氮碱; 或X和Y相同或不同，然后分别为Ca，Al或Zn; R 1，R 2，R 3，R 4，R 5， R 6和R 7相同或不同，彼此独立地为H，甲基，乙基，正丙基，异丙基，正丁基，异丁基，叔丁基和/或苯基，和B）0至2重量％的卤素，其中全部组分总计为100重量％以及其准备和使用过程。

4. 发明授权

US07485745B2 Mixtures composed of monocarboxy-functionalized dialkylphosphinic esters and of further components 失效
标题翻译：由单羧基官能化的二烷基次膦酸酯和其它组分组成的混合物
公开(公告)号：US07485745B2
公开(公告)日：2009-02-03
申请号：US11714481
申请日：2007-03-06
申请人： Wiebke Maas , Werner Krause , Harald Bauer
发明人： Wiebke Maas , Werner Krause , Harald Bauer
IPC分类号： C07F9/22
CPC分类号： C08K5/5313 , C07F9/3211
摘要： The invention relates to mixtures composed of dialkylphosphinic esters and of further components, which comprise A) from 98 to 100% by weight of monocarboxy-functionalized dialkylphosphinic esters of the formula (I) in which R1, R2, R3, R4, R5, R6, and R7 are identical or different and, independently of one another, are H, methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, tert-butyl, and/or phenyl, Y is methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, tert-butyl, phenyl, 2-hydroxyethyl, 2,3-dihydroxypropyl, 2-hydroxypropyl, 3-hydroxypropyl, 4-hydroxybutyl, 3-hydroxybutyl, 2-hydroxybutyl, and/or 6-hydroxyhexyl, allyl, and/or glycerol, X is H, Li, Na, K or NH4, or X is defined as for Y, and then X and Y are two identical radicals or two different radicals of the above organic radicals, and B) from 0 to 2% by weight of halogens, where the entirety of the components always amounts to 100% by weight.
摘要翻译：本发明涉及由二烷基次膦酸酯和其它组分组成的混合物，其包含A）98至100重量％的式（I）的单羧基官能化二烷基次膦酸酯，其中R 1，R 2，R 3，R 4，R 5，R 6 和R7是相同或不同的，并且彼此独立地是H，甲基，乙基，正丙基，异丙基，正丁基，异丁基，叔丁基和/或苯基，Y是甲基，乙基，丙基，异丙基，正丁基，异丁基，叔丁基，苯基，2-羟乙基，2,3-二羟丙基，2-羟丙基，3-羟丙基，4-羟基丁基，3-羟基丁基，2-羟基丁基和/或6 - 羟基己基，烯丙基和/或甘油，X是H，Li，Na，K或NH 4，或X定义为Y，然后X和Y是上述有机基团的两个相同基团或两个不同基团， B）0至2重量％的卤素，其中全部组分总计为100重量％。

5. 发明申请

US20070213436A1 Mixtures composed or monocarboxy-functionalized dialkylphosphinic acids, their use and a process for their preparation 有权
标题翻译：混合物或单羧基官能化二烷基次膦酸，其用途及其制备方法
公开(公告)号：US20070213436A1
公开(公告)日：2007-09-13
申请号：US11714482
申请日：2007-03-06
申请人： Wiebke Maas , Werner Krause , Harald Bauer
发明人： Wiebke Maas , Werner Krause , Harald Bauer
IPC分类号： C08K5/5313 , C07F9/22
CPC分类号： C08K5/5313 , C07F9/301 , C07F9/306 , C08K2201/014
摘要： The invention relates to mixtures composed of monocarboxy-functionalized dialkylphosphinic acids and of further components, which comprise A) from 98 to 100% by weight of monocarboxy-functionalized dialkylphosphinic acids of the formula (I) in which R1, R2, R3, R4, R5, R6, and R7 are identical or different and, independently of one another, are H, methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, tert-butyl, and/or phenyl, X and Y are identical or different and, independently of one another, are H, Li, Na, K, or NH4, and B) from 0 to 2% by weight of halogens, where the entirety of the components always amounts to 100% by weight.
摘要翻译：本发明涉及由单羧基官能化的二烷基次膦酸和其它组分组成的混合物，其包含A）98至100重量％的式（I）的单羧基官能化二烷基次膦酸，其中R 1 R 2，R 3，R 4，R 5，R 6，和/或R 3， >和R 7相同或不同，彼此独立地为H，甲基，乙基，正丙基，异丙基，正丁基，异丁基，叔丁基和/或苯基，X和Y相同或不同，彼此独立地为H，Li，Na，K或NH 4，和B）0-2重量％的卤素，其中这些组分的总量总计为100重量％。

6. 发明申请

US20070210288A1 Mixtures composed of monocarboxy-functionalized dialkylphosphinic esters and of further components 失效
标题翻译：由单羧基官能化的二烷基次膦酸酯和其它组分组成的混合物
公开(公告)号：US20070210288A1
公开(公告)日：2007-09-13
申请号：US11714481
申请日：2007-03-06
申请人： Wiebke Maas , Werner Krause , Harald Bauer
发明人： Wiebke Maas , Werner Krause , Harald Bauer
IPC分类号： C07F9/02
CPC分类号： C08K5/5313 , C07F9/3211
摘要： The invention relates to mixtures composed of dialkylphosphinic esters and of further components, which comprise A) from 98 to 100% by weight of monocarboxy-functionalized dialkylphosphinic esters of the formula (I) in which R1, R2, R3, R4, R5, R6, and R7 are identical or different and, independently of one another, are H, methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, tert-butyl, and/or phenyl, Y is methyl, ethyl, n-propyl, isopropyl, n-butyl, isobutyl, tert-butyl, phenyl, 2-hydroxyethyl, 2,3-dihydroxypropyl, 2-hydroxypropyl, 3-hydroxypropyl, 4-hydroxybutyl, 3-hydroxybutyl, 2-hydroxybutyl, and/or 6-hydroxyhexyl, allyl, and/or glycerol, X is H, Li, Na, K or NH4, or X is defined as for Y, and then X and Y are two identical radicals or two different radicals of the above organic radicals, and B) from 0 to 2% by weight of halogens, where the entirety of the components always amounts to 100% by weight.
摘要翻译：本发明涉及由二烷基次膦酸酯和其它组分组成的混合物，其包含A）98-100重量％的式（I）的单羧基官能化二烷基次膦酸酯，其中R 1，R 2， R 3，R 3，R 4，R 5，R 6和/或R 5， R 7相同或不同，彼此独立地为H，甲基，乙基，正丙基，异丙基，正丁基，异丁基，叔丁基和/或苯基，Y为甲基，乙基，正丙基，异丙基，正丁基，异丁基，叔丁基，苯基，2-羟乙基，2,3-二羟丙基，2-羟丙基，3-羟基丙基，4-羟基丁基，3-羟基丁基，羟基丁基和/或6-羟基己基，烯丙基和/或甘油，X是H，Li，Na，K或NH 4，或X定义为Y，然后X和Y是两个相同的基团或上述有机基团的两个不同基团，以及B）0至2重量％的卤素，其中整个组分总计为100％，通过重量。

7. 发明申请

US20100190901A1 Alkylphosphonous Acids, Salts and Esters, Methods for the Production Thereof, and Use of the Same 有权
标题翻译：烷基亚磷酸，盐和酯，其生产方法及其用途
公开(公告)号：US20100190901A1
公开(公告)日：2010-07-29
申请号：US12668814
申请日：2008-07-02
申请人： Michael Hill , Harald Bauer , Werner Krause
发明人： Michael Hill , Harald Bauer , Werner Krause
IPC分类号： C08K5/5313 , C07F9/30 , C07F9/32
CPC分类号： C07F9/4866 , C07F9/4816 , C07F9/485 , C08K5/5393
摘要： The invention relates to alkylphosphonous acids, salts and esters of formula (I) A-P(═O)(OX)—H (I) wherein A is C2-C20alkyl, C2-C20alkylene, and C8-C20 alkaryl are optionally substituted, and X is H, alkyl, aryl, alkylaryl, alkenyl, substituted alkyl, aryl, alkaryl, alkenyl, ammonium, primary, secondary, tertiary, quaternary alkyl and/or aryl ammonium, an alkali metal, an alkaline earth metal, a metal of the third and fourth main group and the second, fourth and eight sub-group or a metal of the lanthanoid group. The invention also relates to methods for producing same and to the uses of said compounds.
摘要翻译：本发明涉及烷基亚磷酸，其中A是C 2 -C 20烷基，C 2 -C 20亚烷基和C 8 -C 20烷芳基的式（I）AP（= O）（OX）-H（I）的烷基亚磷酸，盐和酯，是烷基，芳基，烷基芳基，烯基，取代的烷基，芳基，烷芳基，烯基，铵，伯，仲，叔，季烷基和/或芳基铵，碱金属，碱土金属，第三和第四主要组和第二，第四和第八子组或镧系元素的金属。本发明还涉及其生产方法和所述化合物的用途。

8. 发明授权

US07420007B2 Dialkylphosphinic salts 有权
标题翻译：二烷基次膦酸盐
公开(公告)号：US07420007B2
公开(公告)日：2008-09-02
申请号：US11015195
申请日：2004-12-17
申请人： Harald Bauer , Werner Krause , Martin Sicken , Norbert Weferling
发明人： Harald Bauer , Werner Krause , Martin Sicken , Norbert Weferling
IPC分类号： C08K5/5313
CPC分类号： C07F9/301 , C08K5/34928 , C08K5/5313 , C08L21/00
摘要： The invention relates to dialkylphosphinic salts of the formula (I) where R1, R2 identical or different, are C1-C6-alkyl, linear or branched M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Fe, Zr, Zn, Ce, Bi, Sr, Mn, Li, Na, K and/or is a protonated nitrogen base; m is from 1 to 4; wherein the telomer content is from 0.01 to 6% by weight. The invention also relates to glare use in flame retardant compositions, and to flame-retardant polymer molding compositions and flame-retardant polymer moldings which comprise these dialkylphosphinic salts.
摘要翻译：本发明涉及式（I）的二烷基次膦酸盐，其中R 1，R 2，R 2相同或不同，为C 1 -C 3 直链或支链M是Mg，Ca，Al，Sb，Sn，Ge，Ti，Fe，Zr，Zn，Ce，Bi，Sr，Mn，Li，Na，K和/ 是质子化的氮基; m为1〜4; 其中调聚物含量为0.01至6重量％。本发明还涉及阻燃组合物中的眩光用途，以及包含这些二烷基次膦酸盐的阻燃聚合物模塑组合物和阻燃聚合物模制品。

9. 发明授权

US07259200B2 Phosphorus-containing flame retardant agglomerates 有权
标题翻译：含磷阻燃剂
公开(公告)号：US07259200B2
公开(公告)日：2007-08-21
申请号：US10959515
申请日：2004-10-06
申请人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
IPC分类号： C08K5/5313
CPC分类号： C08K5/0066 , C08J3/223 , C08J2367/02 , C08J2377/02 , C08J2377/06 , C08K5/5313
摘要： The invention relates to phosphorus-containing flame retardant agglomerates comprising a) from 99.99 to 80% by weight of aggregates and/or primary particles composed of a phosphinic salt of the formula (I) and/or composed of a diphosphinic salt of the formula (II), and/or composed of polymers of these, where R1,R2 are identical or different and are C1-C6-alkyl, linear or branched, and/or aryl; R3 is C1-C10-alkylene, linear or branched, C6-C10-arylene, -alkylarylene or -arylalkylene; M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Fe, Zr, Ce, Bi, Sr, Mn, Li, Na, K and/or a protonated nitrogen base; m is from 1 to 4; n is from 1 to 4; x is from 1 to 4 and b) from 0.01 to 20% by weight of auxiliaries. The invention likewise relates to a process for the production of these phosphorus-containing flame retardant agglomerates, and also to polymeric compositions and moldings which comprise these phosphorus-containing flame retardant agglomerates.
摘要翻译：本发明涉及含磷阻燃附聚物，其包含a）99.99至80重量％的由式（I）的次膦酸盐组成的和/或由式（I）的次膦酸盐和/或由式（I）的二膦酸盐组成的聚集体和/ II）和/或由它们的聚合物组成，其中R 1，R 2，R 2相同或不同，为C 1 -C 3烷基，直链或支链的亚烷基，和/或芳基; R 3是C 1 -C 10 - 亚烷基，直链或支链C 6 -C 13 - - 亚芳基， - 烷基亚芳基或 - 芳基亚烷基; M是Mg，Ca，Al，Sb，Sn，Ge，Ti，Fe，Zr，Ce，Bi，Sr，Mn，Li，Na，K和/或质子化氮碱; m为1〜4; n为1至4; x为1至4，和b）0.01至20重量％的助剂。本发明同样涉及一种生产这些含磷阻燃附聚物的方法，以及包含这些含磷阻燃剂附聚物的聚合物组合物和模制品。

10. 发明申请

US20060214144A1 Phosphorus-containing thermally stabilized flame retardant agglomerates 审中-公开
标题翻译：含磷热稳定阻燃剂团聚体
公开(公告)号：US20060214144A1
公开(公告)日：2006-09-28
申请号：US11388916
申请日：2006-03-24
申请人： Harald Bauer , Sebastian Hoerold , Werner Krause
发明人： Harald Bauer , Sebastian Hoerold , Werner Krause
IPC分类号： C09K21/00
CPC分类号： C08K5/5313 , C08K5/3492
摘要： The invention relates to phosphorus-containing thermally stabilized flame retardant agglomerates, comprising as component A from 6 to 99.99% by weight of aggregates and/or primary particles composed of a phosphinic salt of the formula (I) and/or of a diphosphinic salt of the formula (II), and/or of their polymers, where R1 and R2 are identical or different and are C1-C6-alkyl, linear or branched, and/or aryl; R3 is C1-C10-alkylene, linear or branched, C6-C10-arylene, -alkylarylene, or -arylalkylene; M is Mg, Ca, Al, Sb, Sn, Ge, Zn, Ti, Fe, Zr, Ce, Bi, Sr, Mn, Li, Na, K, and/or a protonated nitrogen base; m is from 1 to 4; n is from 1 to 4; and x is from 1 to 4; as component B from 0 to 90% by weight of a synergist which comprises a nitrogen compound or which comprises a phosphorus compound, or which comprises a phosphorus-nitrogen compound; as component C from 0 to 20% by weight of compounds of the elements of the second main and transition group; and as component D from 0.01 to 20% by weight of auxiliary. The invention also relates to a process for their production, and to their use.
摘要翻译：本发明涉及含磷热稳定的阻燃附聚物，其包含作为组分A的6至99.99重量％的由式（I）的次膦酸盐和/或由式（I）的次膦酸盐组成的聚集体和/或一次颗粒和/ 式（II）和/或它们的聚合物，其中R 1和R 2相同或不同，为直链或支链的C 1 -C 6 - 烷基，和 /或芳基; R 3是C 1 -C 10 - 亚烷基，直链或支链C 6 -C 13 - - 亚芳基， - 亚烷基亚芳基或 - 芳基亚烷基; M是Mg，Ca，Al，Sb，Sn，Ge，Zn，Ti，Fe，Zr，Ce，Bi，Sr，Mn，Li，Na，K和/或质子化氮碱; m为1〜4; n为1至4; x为1〜4; 作为组分B的0至90重量％的增效剂，其包含氮化合物或包含磷化合物，或包含磷 - 氮化合物; 作为组分C的0至20重量％的第二主要和过渡基团的元素的化合物; 并且作为组分D为辅助剂的0.01至20重量％。本发明还涉及其生产方法及其用途。

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