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1. 发明授权

US10421909B2 Mixed alkali-aluminum phosphites, method for producing same, and the use thereof 有权
公开(公告)号：US10421909B2
公开(公告)日：2019-09-24
申请号：US14362871
申请日：2012-11-28
申请人： Harald Bauer , Sebastian Hoerold , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Martin Sicken
IPC分类号： C09K21/04 , C01F7/00 , C01B25/163 , C08K3/32 , C08K7/14 , C08K5/56
摘要： The invention relates to mixed alkali-aluminum phosphites of the formula (I) Al2.00Mz(HPO3)y(OH)vx(H2O)w (I) in which M represents alkali metal ions, z is 0.01 to 1.5, y is 2.63 to 3.5, v is 0 to 2, w is 0 to 4; to a process for preparation thereof and to the use thereof.

2. 发明授权

US10202549B2 Mixtures of aluminum phosphite with sparingly soluble aluminum salts and foreign ions, process for the production thereof and the use thereof 有权
公开(公告)号：US10202549B2
公开(公告)日：2019-02-12
申请号：US14362881
申请日：2012-11-28
申请人： Harald Bauer , Sebastian Hoerold , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Martin Sicken
IPC分类号： C08K3/32 , C09K21/04 , C01B25/163
摘要： The invention relates to mixtures of aluminum phosphite with sparingly soluble aluminum salts and nitrogen-free extraneous ions, comprising 80 to 99.898% by weight of aluminum phosphite of the formula (I) Al2(HPO3)3xH2O (I) in which x is 0 to 4, 0.1 to 10% by weight of sparingly soluble aluminum salts and 0.002 to 10% by weight of nitrogen-free extraneous ions; to a process for preparation thereof and use thereof.

3. 发明申请

US20150005427A1 Mixtures of Aluminum Phosphite with Sparingly Soluble Aluminum Salts and Foreign Ions, Process for the Production Thereof and The Use Thereof 审中-公开
标题翻译：亚磷酸铝与可溶性铝盐和外来离子的混合物，其生产工艺及其用途
公开(公告)号：US20150005427A1
公开(公告)日：2015-01-01
申请号：US14362881
申请日：2012-11-28
申请人： Harald Bauer , Sebastian Hoerold , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Martin Sicken
IPC分类号： C09K21/04 , C08K3/32
CPC分类号： C09K21/04 , C01B25/163 , C01P2004/61 , C01P2006/11 , C01P2006/62 , C01P2006/63 , C01P2006/64 , C01P2006/80 , C01P2006/82 , C08K3/32
摘要： Mixtures of aluminum phosphite with sparingly soluble aluminum salts and extraneous ions, process for preparation thereof and use thereofThe invention relates to mixtures of aluminum phosphite with sparingly soluble aluminum salts and nitrogen-free extraneous ions, comprising 80 to 99.898% by weight of aluminum phosphite of the formula (I) Al2(HPO3)3×H2O (I) in which x is 0 to 4, 0.1 to 10% by weight of sparingly soluble aluminum salts and 0.002 to 10% by weight of nitrogen-free extraneous ions; to a process for preparation thereof and use thereof.
摘要翻译：亚磷酸铝与微溶性铝盐和外来离子的混合物，其制备方法及其用途本发明涉及亚磷酸铝与微溶铝盐和无氮外来离子的混合物，其包含80至99.898重量％的亚磷酸铝式（I）其中x为0至4的式（I）Al 2（HPO 3）3×H 2 O（I），0.1至10重量％的微溶铝盐和0.002至10重量％的无氮外来离子; 涉及其制备方法及其应用。

4. 发明授权

US07259200B2 Phosphorus-containing flame retardant agglomerates 有权
标题翻译：含磷阻燃剂
公开(公告)号：US07259200B2
公开(公告)日：2007-08-21
申请号：US10959515
申请日：2004-10-06
申请人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
IPC分类号： C08K5/5313
CPC分类号： C08K5/0066 , C08J3/223 , C08J2367/02 , C08J2377/02 , C08J2377/06 , C08K5/5313
摘要： The invention relates to phosphorus-containing flame retardant agglomerates comprising a) from 99.99 to 80% by weight of aggregates and/or primary particles composed of a phosphinic salt of the formula (I) and/or composed of a diphosphinic salt of the formula (II), and/or composed of polymers of these, where R1,R2 are identical or different and are C1-C6-alkyl, linear or branched, and/or aryl; R3 is C1-C10-alkylene, linear or branched, C6-C10-arylene, -alkylarylene or -arylalkylene; M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Fe, Zr, Ce, Bi, Sr, Mn, Li, Na, K and/or a protonated nitrogen base; m is from 1 to 4; n is from 1 to 4; x is from 1 to 4 and b) from 0.01 to 20% by weight of auxiliaries. The invention likewise relates to a process for the production of these phosphorus-containing flame retardant agglomerates, and also to polymeric compositions and moldings which comprise these phosphorus-containing flame retardant agglomerates.
摘要翻译：本发明涉及含磷阻燃附聚物，其包含a）99.99至80重量％的由式（I）的次膦酸盐组成的和/或由式（I）的次膦酸盐和/或由式（I）的二膦酸盐组成的聚集体和/ II）和/或由它们的聚合物组成，其中R 1，R 2，R 2相同或不同，为C 1 -C 3烷基，直链或支链的亚烷基，和/或芳基; R 3是C 1 -C 10 - 亚烷基，直链或支链C 6 -C 13 - - 亚芳基， - 烷基亚芳基或 - 芳基亚烷基; M是Mg，Ca，Al，Sb，Sn，Ge，Ti，Fe，Zr，Ce，Bi，Sr，Mn，Li，Na，K和/或质子化氮碱; m为1〜4; n为1至4; x为1至4，和b）0.01至20重量％的助剂。本发明同样涉及一种生产这些含磷阻燃附聚物的方法，以及包含这些含磷阻燃剂附聚物的聚合物组合物和模制品。

5. 发明授权

US09505904B2 Mixtures of aluminum hydrogenphosphites with aluminum salts, process for the production thereof and the use thereof 有权
标题翻译：亚磷酸氢铝与铝盐的混合物，其制备方法及其用途
公开(公告)号：US09505904B2
公开(公告)日：2016-11-29
申请号：US14362884
申请日：2012-11-28
申请人： Harald Bauer , Sebastian Hoerold , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Martin Sicken
IPC分类号： C08K3/32 , C01B25/163 , C01B25/165 , C08K7/14
CPC分类号： C08K3/32 , C01B25/163 , C01B25/165 , C01P2004/61 , C01P2006/11 , C01P2006/62 , C01P2006/63 , C01P2006/64 , C01P2006/82 , C08K7/14 , C08K2003/329
摘要： The invention relates to mixtures of aluminum hydrogenphosphites of the formula (I) Al2.00(HPO3)v(H2PO3)yx(H2O)z (I) and aluminum salts comprising 91 to 99.9% aluminum hydrogenphosphites of the formula (I) 0.1 to 9% aluminum salts and 0 to 50% water (of crystallization), where v in formula (I) is 2 to 2.99, y is 2 to 0.01 and z is 0 to 4, to processes for preparation thereof and to the use thereof.

6. 发明申请

US20130190432A1 Flame Retardant-Stabilizer Combination For Thermoplastic Polymers 审中-公开
标题翻译：阻燃稳定剂组合热塑性聚合物
公开(公告)号：US20130190432A1
公开(公告)日：2013-07-25
申请号：US13878145
申请日：2011-09-30
申请人： Werner Krause , Harald Bauer , Martin Sicken , Sebastian Hoerold , Wolfgang Wanzke , Elke Schlosser
发明人： Werner Krause , Harald Bauer , Martin Sicken , Sebastian Hoerold , Wolfgang Wanzke , Elke Schlosser
IPC分类号： C08K5/5313 , C08K5/3492 , C08K5/10 , C08K3/22 , C08K5/5317 , C08K5/56 , C08K5/52 , C08K3/38
CPC分类号： C08K5/5313 , C08K3/22 , C08K3/38 , C08K5/0008 , C08K5/10 , C08K5/34922 , C08K5/34924 , C08K5/52 , C08K5/5317 , C08K5/56
摘要： A novel flame retardant-stabilizer combination for thermoplastic polymers, comprising as component A 20 to 99% by weight of a dialkylphosphinic salt of the formula (I) and/or of a diphosphinic salt of the formula (II) and/or polymers thereof in which R1, R2 are the same or different and are each C1-C6-alkyl, linear or branched; R3 is C1-C10-alkylene, linear or branched, C6-C10-arylene, C7-C20-alkylarylene or C7-C20-arylalkylene; M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Zn, Fe, Zr, Ce, Bi, Sr, Mn, Li, Na, K and/or a protonated nitrogen base; m is 1 to 4; n is 1 to 4; x is 1 to 4, as component B 1 to 80% by weight of a salt of the phosphorous acid with the general formula (III) [HP(═O)O2]2−Mm+ (III) in which M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Zn, Fe, Zr, Ce, Bi, Sr, Mn, Li, Na and/or K and m is 1 to 4, as component C 0 to 30% by weight of a nitrogen-containing synergist and/or of a phosphorus/nitrogen flame retardant, as component D 0 to 10% by weight of a zinc salt and/or of a basic or amphoteric oxide, hydroxide, carbonate, silicate, borate, stannate, mixed oxide hydroxide, oxide hydroxide carbonate, hydroxide silicate and/or hydroxide borate and/or mixtures of these substances, as component E 0 to 3% by weight of a phosphonite and/or of a mixture of a phosphonite and a phosphite, and as component F 0 to 3% by weight of an ester and/or salt of long-chain aliphatic carboxylic acids (fatty acids) which typically have chain lengths of C14 to C40, where the sum of the components is always 100% by weight.
摘要翻译：一种热塑性聚合物的新型阻燃稳定剂组合物，其包含作为组分A 20至99重量％的式（I）的二烷基次膦酸盐和/或式（II）的二膦酸盐和/或其聚合物其中R 1，R 2相同或不同，并且各自为直链或支链的C 1 -C 6烷基; R3是C1-C10-亚烷基，直链或支链的C6-C10亚芳基，C7-C20-烷基亚芳基或C7-C20-芳基亚烷基; M是Mg，Ca，Al，Sb，Sn，Ge，Ti，Zn，Fe，Zr，Ce，Bi，Sr，Mn，Li，Na，K和/或质子化氮碱; m为1〜4; n为1〜4; x为1〜4，作为成分B，通式（III）的亚磷酸盐为1〜80重量％[HP（= O）O 2] 2 -Mm +（III），其中M为Mg，Ca ，Al，Sb，Sn，Ge，Ti，Zn，Fe，Zr，Ce，Bi，Sr，Mn，Li，Na和/或K和m为1〜4，作为组分C 0〜30重量％含氮增效剂和/或磷/氮阻燃剂，作为组分D 0至10重量％的锌盐和/或碱性或两性氧化物，氢氧化物，碳酸盐，硅酸盐，硼酸盐，锡酸盐，混合氧化物氢氧化物，氢氧化物碳酸盐，氢氧化硅酸盐和/或氢氧化物硼酸盐和/或这些物质的混合物，作为组分E 0至3重量％的亚膦酸盐和/或亚磷酸盐和亚磷酸盐的混合物，并且作为组分F 0至3重量％的通常具有C14至C40链长度的长链脂族羧酸（脂肪酸）的酯和/或盐，其中组分的总量总是为100重量％。

7. 发明授权

US07273901B2 Flame retardant dispersion 有权
标题翻译：阻燃分散体
公开(公告)号：US07273901B2
公开(公告)日：2007-09-25
申请号：US10794019
申请日：2004-03-05
申请人： Martin Sicken , Susanne Knop , Sebastian Hoerold , Harald Bauer
发明人： Martin Sicken , Susanne Knop , Sebastian Hoerold , Harald Bauer
IPC分类号： C08K5/5313
CPC分类号： C08K5/17 , C08K5/51 , H05K1/0373
摘要： The invention relates to a novel flame retardant dispersion for thermoplastic and thermoset polymers, comprising, as component A, a phosphinic salt of the formula (I), and/or a diphosphinic salt of the formula (II), and/or polymers of these, where R1 and R2 are identical or different and are C1-C6-alkyl, linear or branched, and/or aryl; R3 is C1-C10-alkylene, linear or branched, C6-C10-arylene, -alkylarylene, or -arylalkylene; M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Zn, Fe, Zr, Ce, Bi, Sr, Mn, Li, Na and/or K; m is from 1 to 4; n is from 1 to 4; x is from 1 to 4, and, as component B, a nitrogen-containing synergist or a phosphorus/nitrogen flame retardant, and, as component C, a liquid compound.
摘要翻译：本发明涉及用于热塑性和热固性聚合物的新型阻燃分散体，其包含作为组分A的式（I）的次膦酸盐和/或式（II）的二膦酸盐，和/或这些其中R 1和R 2相同或不同，为C 1 -C 6 - 烷基，线性或支链和/或芳基; R 3是C 1 -C 10 - 亚烷基，直链或支链C 6 -C 13 - - 亚芳基， - 亚烷基亚芳基或 - 芳基亚烷基; M是Mg，Ca，Al，Sb，Sn，Ge，Ti，Zn，Fe，Zr，Ce，Bi，Sr，Mn，Li，Na和/或K; m为1〜4; n为1至4; x为1〜4，作为组分B，含氮增效剂或磷/氮阻燃剂，作为组分C，为液态化合物。

8. 发明申请

US20060208239A1 Compacted flame-retardant composition 审中-公开
标题翻译：压实阻燃组合物
公开(公告)号：US20060208239A1
公开(公告)日：2006-09-21
申请号：US11438594
申请日：2006-05-22
申请人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
IPC分类号： C09K21/00
CPC分类号： C08K5/5313
摘要： The invention relates to a compacted flame-retardant composition comprising an organophosphorus flame-retardant component, prepared by compacting an organophosphorus flame-retardant component with or without a compacting auxiliary, and to a process for preparing these flame-retardant compositions, and to polymer molding compositions which comprise these flame-retardant compositions.
摘要翻译：本发明涉及一种压实的阻燃组合物，其包含通过压实有或无压实助剂的有机磷阻燃组分制备的有机磷阻燃组分，以及制备这些阻燃组合物的方法和聚合物成型包含这些阻燃组合物的组合物。

9. 发明申请

US20070203270A1 FLAME RETARDANT DISPERSION 有权
标题翻译：阻燃剂分散剂
公开(公告)号：US20070203270A1
公开(公告)日：2007-08-30
申请号：US10794019
申请日：2004-03-05
申请人： Martin Sicken , Susanne Knop , Sebastian Hoerold , Harald Bauer
发明人： Martin Sicken , Susanne Knop , Sebastian Hoerold , Harald Bauer
IPC分类号： C08K5/53
CPC分类号： C08K5/17 , C08K5/51 , H05K1/0373
摘要： The invention relates to a novel flame retardant dispersion for thermoplastic and thermoset polymers, comprising, as component A, a phosphinic salt of the formula (I), and/or a diphosphinic salt of the formula (II), and/or polymers of these, where R1 and R2 are identical or different and are C1-C6-alkyl, linear or branched, and/or aryl; R3 is C1-C10-alkylene, linear or branched, C6-C10-arylene, -alkylarylene, or -arylalkylene; M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Zn, Fe, Zr, Ce, Bi, Sr, Mn, Li, Na and/or K; m is from 1 to 4; n is from 1 to 4; x is from 1 to 4, and, as component B, a nitrogen-containing synergist or a phosphorus/nitrogen flame retardant, and, as component C, a liquid compound.
摘要翻译：本发明涉及用于热塑性和热固性聚合物的新型阻燃分散体，其包含作为组分A的式（I）的次膦酸盐和/或式（II）的二膦酸盐，和/或这些其中R 1和R 2相同或不同，为C 1 -C 6 - 烷基，线性或支链和/或芳基; R 3是C 1 -C 10 - 亚烷基，直链或支链C 6 -C 13 - - 亚芳基， - 亚烷基亚芳基或 - 芳基亚烷基; M是Mg，Ca，Al，Sb，Sn，Ge，Ti，Zn，Fe，Zr，Ce，Bi，Sr，Mn，Li，Na和/或K; m为1〜4; n为1至4; x为1〜4，作为组分B，含氮增效剂或磷/氮阻燃剂，作为组分C，为液态化合物。

10. 发明申请

US20060020064A1 Flame-retardant polymer molding compositions 审中-公开
标题翻译：阻燃聚合物模塑组合物
公开(公告)号：US20060020064A1
公开(公告)日：2006-01-26
申请号：US11182693
申请日：2005-07-15
申请人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
发明人： Harald Bauer , Sebastian Hoerold , Werner Krause , Martin Sicken
IPC分类号： C08K5/49
CPC分类号： B82Y30/00 , C08K5/5313 , C08K2201/011 , C08L21/00
摘要： The invention relates to a flame-retardant polymer molding composition which comprises a nanoparticulate phosphorus-containing flame retardant system which comprises at least one phosphinic salt of the formula (I) and/or diphosphinic salt of the formula (II) and/or their polymers, where R1 and R2 are identical or different and are C1-C6-alkyl, linear or branched, and/or aryl; R3 is C1-C10-alkylene, linear or branched, C6-C10-arylene, -alkylarylene, or -arylalkylene; M is Mg, Ca, Al, Sb, Sn, Ge, Ti, Fe, Zr, Zn, Ce, Bi, Sr, Mn, Li, Na, K, and/or a protonated nitrogen base; m is from 1 to 4; n is from 1 to 4; x is from 1 to 4.
摘要翻译：本发明涉及一种阻燃聚合物模塑组合物，其包含纳米颗粒含磷阻燃体系，其包含至少一种式（I）的次膦酸盐和/或式（II）的二膦酸盐和/或其聚合物其中R 1和R 2相同或不同，为C 1 -C 6 - 烷基，线性或支链和/或芳基; R 3是C 1 -C 10 - 亚烷基，直链或支链C 6 -C 13 - - 亚芳基， - 亚烷基亚芳基或 - 芳基亚烷基; M是Mg，Ca，Al，Sb，Sn，Ge，Ti，Fe，Zr，Zn，Ce，Bi，Sr，Mn，Li，Na，K和/或质子化氮碱; m为1〜4; n为1至4; x为1至4。

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