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1. 发明授权

US07365152B2 Method for producing highly reactive, low halogen polyisobutenes 有权
标题翻译：生产高反应性低卤聚异丁烯的方法
公开(公告)号：US07365152B2
公开(公告)日：2008-04-29
申请号：US10584138
申请日：2004-12-29
申请人： Hans Peter Rath , Thomas Perner , Eckard Schauss
发明人： Hans Peter Rath , Thomas Perner , Eckard Schauss
IPC分类号： C08F6/08 , C08F10/10
CPC分类号： C08F8/26 , C08F110/10 , C08F10/10 , C08F4/14 , C08F2500/02
摘要： A process is described for preparing polyisobutene having a low halogen content, in which isobutene is polymerized in the presence of a catalyst which comprises a halogenated Lewis acid, the catalyst is removed and/or deactivated, and the resulting polyisobutene is contacted with a zeolite of an average pore size of from 5 to 15 Å.
摘要翻译：描述了一种制备具有低卤素含量的聚异丁烯的方法，其中异丁烯在包含卤化路易斯酸的催化剂存在下聚合，将催化剂除去和/或失活，并将得到的聚异丁烯与平均孔径为5至15埃。

2. 发明申请

US20070155930A1 Method for producing highly reactive, low halogen polyisobutenes 有权
标题翻译：生产高反应性低卤聚异丁烯的方法
公开(公告)号：US20070155930A1
公开(公告)日：2007-07-05
申请号：US10584138
申请日：2004-12-29
申请人： Hans Rath , Thomas Perner , Eckard Schauss
发明人： Hans Rath , Thomas Perner , Eckard Schauss
IPC分类号： C08F10/00
CPC分类号： C08F8/26 , C08F110/10 , C08F10/10 , C08F4/14 , C08F2500/02
摘要： A process is described for preparing polyisobutene having a low halogen content, in which isobutene is polymerized in the presence of a catalyst which comprises a halogenated Lewis acid, the catalyst is removed and/or deactivated, and the resulting polyisobutene is contacted with a zeolite of an average pore size of from 5 to 15 Å.
摘要翻译：描述了一种制备具有低卤素含量的聚异丁烯的方法，其中异丁烯在包含卤化路易斯酸的催化剂存在下聚合，将催化剂除去和/或失活，并将得到的聚异丁烯与平均孔径为5至15埃。

3. 发明授权

US07217773B2 Method for producing polyisobutene 有权
标题翻译：生产聚异丁烯的方法
公开(公告)号：US07217773B2
公开(公告)日：2007-05-15
申请号：US10542928
申请日：2004-01-23
申请人： Hans Peter Rath , Thomas Perner , Helmut Mach
发明人： Hans Peter Rath , Thomas Perner , Helmut Mach
IPC分类号： C08F4/14 , C08F110/10
CPC分类号： C08F110/10 , Y02P20/582 , C08F4/14 , C08F2500/02 , C08F2500/03
摘要： A process is described for preparing polyisobutene having a content of terminal vinylidene groups of at least 75 mol % by polymerizing isobutene or isobutenic hydrocarbon mixtures in the liquid phase in the presence of a boron trifluoride complex catalyst of the composition (BF3)a.L1b.L2c.L3d where L1 is water, a primary C1–C5-alkanol and/or a secondary C3–C5-alkanol, L2 is at least one aldehyde and/or one ketone, L3 is an ether having at least 5 carbon atoms, a secondary alkanol having at least 6 carbon atoms, a primary alkanol having at least 6 carbon atoms and/or a tertiary alkanol, the b:a ratio is in the range from 0.9 to 3.0, the c:a ratio is in the range from 0.01 to 0.5, and the d:a ratio is in the range from 0 to 1.0.
摘要翻译：描述了一种制备具有至少75mol％的末端亚乙烯基含量的聚异丁烯的方法，通过在液相中聚合异丁烯或异丁烯烃混合物，在三元组配合物催化剂存在下，描述=“在线公式”end =“lead”？>（BF 3） a β-in-line-formula description =“In-line-formula”=“In- 其中L 1是水，主要C 1 -C 5 - 烷醇和/或仲C 3 -C 5 - 烷醇，L 2是至少一种醛和/或一种酮，L 3， SUP>是具有至少5个碳原子的醚，具有至少6个碳原子的仲链烷醇，具有至少6个碳原子的伯烷醇和/或叔链烷醇，b：a的比例在0.9至 3.0，c：a的比例在0.01至0.5的范围内，d:a的比例为范围从0到1.0。

4. 发明授权

US06465608B1 Method for drying and degassing polyolefins 失效
标题翻译：干燥和脱气聚烯烃的方法
公开(公告)号：US06465608B1
公开(公告)日：2002-10-15
申请号：US09980566
申请日：2001-11-15
申请人： Michael Witt , Paulus De Lange , Thomas Perner , Andreas Deckers , Kaspar Evertz , Dieter Lilge
发明人： Michael Witt , Paulus De Lange , Thomas Perner , Andreas Deckers , Kaspar Evertz , Dieter Lilge
IPC分类号： C08F600
CPC分类号： C08F6/005 , C08F210/16 , C08F210/14 , C08F2500/12 , C08F2500/13
摘要： The invention relates to a method for drying and degassing polyolefins in which the polymerization product leaving a polymerization reactor is brought into contact with a degassing medium and simultaneously decompressed. The degassing medium employed according to the invention is the monomer to be polymerized, which, in particular, flows through a decompression tank in a circulation process and which is preferably also enriched with ethylene or other low-boiling olefins in an amount in the range from 0 to 100 mol %, based on the total amount of circulating gas. A polymerization in an amount of up to 10%, based on the total polymerization conversion, takes place in accordance with the invention inside the decompression tank.
摘要翻译：本发明涉及一种干燥脱气聚烯烃的方法，其中离开聚合反应器的聚合产物与脱气介质接触并同时减压。根据本发明使用的脱气介质是待聚合的单体，其特别是在循环过程中流过减压槽，并且其优选还富含乙烯或其它低沸点烯烃，其量为 0〜100摩尔％，基于循环气体的总量。根据本发明，在减压槽内进行基于总聚合转化率高达10％的聚合。

5. 发明授权

US4956402A Synthetic resin with basic nitrogen groups from resins reacted with the ketimine-urethane product of an alkanolamine, a ketone and anisocyanate 失效
标题翻译：来自树脂的具有碱性氮基团的合成树脂与烷醇胺，酮和异氰酸酯的酮亚胺 - 氨基甲酸酯产物反应
公开(公告)号：US4956402A
公开(公告)日：1990-09-11
申请号：US210499
申请日：1988-06-23
申请人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
发明人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
IPC分类号： C08G59/30 , C08G18/64 , C08G59/14 , C08G59/28 , C08G59/40 , C09D5/44 , C09D163/00
CPC分类号： C09D5/4438 , C08G18/643 , C08G59/4014 , C08G59/4042 , Y10T428/31511 , Y10T428/31522 , Y10T428/31529
摘要： A synthetic resin which carries basic nitrogen groups and is water-dilutable by protonation with acid is obtainable by reacting(A) an epoxy resin having an average molecular weight M.sub.n of from 200 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(B) a ketimine of a primary amine additionally containing one or more urethane groups and optionally also with(C) a diketimine of a diprimary amine containing no urethane groups and optionally also with(D) a secondary amine which may contain a tertiary amimo group also, a ketimine of a primary monoamine and/or a ketimine of a primary/tertiary diamine.
摘要翻译：通过使（A）平均分子量Mn为200〜6,000的环氧树脂和每分子平均1.5〜3.0个环氧基的环氧树脂与（B）另外含有一个或多个氨基甲酸酯基团的伯胺的酮亚胺，以及任选地还含有（C）不含氨基甲酸酯基团的二原子胺的二酮亚胺，并且任选地还可以含有（D）可含有叔胺摩尔组的仲胺也可以是伯/叔二胺的伯胺和/或酮亚胺的酮亚胺。

6. 发明授权

US4981884A Synthetic resin with basic nitrogen groups, preparation and use thereof 失效
标题翻译：具有碱性氮基团的合成树脂，其制备和用途
公开(公告)号：US4981884A
公开(公告)日：1991-01-01
申请号：US210502
申请日：1988-06-23
申请人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
发明人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
IPC分类号： C08L63/00 , C08G59/00 , C08G59/28 , C09D5/44 , C09D163/00
CPC分类号： C09D5/4473 , C09D5/4434
摘要： A synthetic resin which carries basic nitrogen groups and is water-dilutable by protonation with an acid, containing(A) a chain-extended, amine-modified epoxy resin obtainable by reacting(a.sub.1) an epoxy resin having an average molecular weight M.sub.n of from 300 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(a.sub.2) a diketimine of a diprimary diamine, which diprimary diamine contains no further groups reactive with epoxy groups under mild conditions and(B) an amino-modified epoxy resin obtainable by reactingb.sub.1) an epoxy resin having an average molecular weight M.sub.n of from 800 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(b.sub.2) a secondary amine or a secondary-tertiary diamine, a ketimine of a primary monoamine or a ketimine of a primary/tertiary diamine or a mixture of these (b.sub.2) components, with the proviso that (A) and (B) are different.
摘要翻译：一种合成树脂，其承载碱性氮基团并且可通过用酸质子化而进行水稀释，所述合成树脂含有（A）伸长的胺改性的环氧树脂，其通过使（a1）平均分子量Mn为 300〜6000，平均每个分子具有1.5〜3.0个环氧基，（a2）二元二胺的二酮亚胺，该二元二胺在温和条件下不含有与环氧基反应的其它基团，（B）可得到的氨基改性环氧树脂通过使b1）平均分子量Mn为800至6000，平均每分子具有1.5至3.0个环氧基的环氧树脂与（b2）仲胺或仲叔胺，伯胺的酮亚胺或伯（叔）二胺的酮亚胺或这些（b2）成分的混合物，条件是（A）和（B）不同。

7. 发明授权

US5015673A Synthetic resin with basic nitrogen groups, preparation and use thereof using a urethane carrying ketimine 失效
公开(公告)号：US5015673A
公开(公告)日：1991-05-14
申请号：US528374
申请日：1990-05-25
申请人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
发明人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
IPC分类号： C08G59/30 , C08G18/64 , C08G59/14 , C08G59/28 , C08G59/40 , C09D5/44 , C09D163/00
CPC分类号： C09D5/4438 , C08G18/643 , C08G59/4014 , C08G59/4042 , Y10T428/31511 , Y10T428/31522 , Y10T428/31529
摘要： A synthetic resin which carries basic nitrogen groups and is water-dilutable by protonation with acid is obtainable by reacting(A) an epoxy resin having an average molecular weight M.sub.n of from 300 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(B) a ketimine of a primary amine additionally containing one or more urethane groups and optionally also with(C) a diketimine of a diprimary amine containing no urethane groups and optionally also with(D) a secondary amine which may contain a tertiary amino group also, a ketimine of a primary monoamine and/or a ketimine of a primary/tertiary diamine.

8. 发明授权

US5015672A Synthetic resin with basic nitrogen groups, preparation and use thereof using a urethane carrying ketimine 失效
标题翻译：具有碱性氮基团的合成树脂，其制备和使用使用氨基甲酸乙酯携带酮亚胺
公开(公告)号：US5015672A
公开(公告)日：1991-05-14
申请号：US528377
申请日：1990-05-25
申请人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
发明人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
IPC分类号： C08G59/30 , C08G18/64 , C08G59/14 , C08G59/28 , C08G59/40 , C09D5/44 , C09D163/00
CPC分类号： C09D5/4438 , C08G18/643 , C08G59/4014 , C08G59/4042 , Y10T428/31511 , Y10T428/31522 , Y10T428/31529
摘要： A synthetic resin which carries basic nitrogen groups and is water-dilutable by protonation with acid is obtainable by reacting(A) an epoxy resin having an average molecular weight M.sub.n of from 300 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(B) a ketimine of a primary amine additionally containing one or more urethane groups and optionally also with(C) a diketimine of a diprimary amine containing no urethane groups and optionally also with(D) a secondary amine which may contain a tertiary amino group also, a ketimine of a primary monoamine and/or a ketimine of a primary/tertiary diamine.

9. 发明申请

US20060063901A1 Method for producing polyisobutene 有权
标题翻译：生产聚异丁烯的方法
公开(公告)号：US20060063901A1
公开(公告)日：2006-03-23
申请号：US10542928
申请日：2004-01-23
申请人： Hans Rath , Thomas Perner , Helmut Mach
发明人： Hans Rath , Thomas Perner , Helmut Mach
IPC分类号： C08F4/14
CPC分类号： C08F110/10 , Y02P20/582 , C08F4/14 , C08F2500/02 , C08F2500/03
摘要： A process is described for preparing polyisobutene having a content of terminal vinylidene groups of at least 75 mol % by polymerizing isobutene or isobutenic hydrocarbon mixtures in the liquid phase in the presence of a boron trifluoride complex catalyst of the composition (BF3)a.L1b.L2c.L3d where L1 is water, a primary C1-C5-alkanol and/or a secondary C3-C5-alkanol, L2 is at least one aldehyde and/or one ketone, L3 is an ether having at least 5 carbon atoms, a secondary alkanol having at least 6 carbon atoms, a primary alkanol having at least 6 carbon atoms and/or a tertiary alkanol, the b:a ratio is in the range from 0.9 to 3.0, the c:a ratio is in the range from 0.01 to 0.5, and the d:a ratio is in the range from 0 to 1.0.
摘要翻译：描述了一种制备具有至少75mol％的末端亚乙烯基含量的聚异丁烯的方法，其通过在液相中在混合物的三氟化硼配合物催化剂存在下聚合异丁烯或异丁烯烃混合物

10. 发明授权

US06270729B1 Apparatus and process for the intensive degassing of PVC suspensions and dispersions 失效
标题翻译： PVC悬浮液和分散体强化脱气的装置和方法
公开(公告)号：US06270729B1
公开(公告)日：2001-08-07
申请号：US08518719
申请日：1995-08-24
申请人： Thomas Perner , Gunter Elzer
发明人： Thomas Perner , Gunter Elzer
IPC分类号： B32B2704
CPC分类号： B01D19/001 , C08F6/003 , C08L27/06
摘要： An apparatus for the intensive degassing of polyvinyl chloride-containing dispersions comprising a polymerization reactor (1), a cooling device (2), and a vacuum unit (3), where the polymerization reactor (1) contains a steam inlet (4) in the lower half, and the polymerization reactor (1), the cooling device (2) and the vacuum unit (3) are connected to one another via a connector (5). The invention also relates to the use of this apparatus and to a process for intensive degassing using this apparatus.
摘要翻译：一种用于对包含聚合反应器（1），冷却装置（2）和真空单元（3）进行强制脱气的聚氯乙烯分散体的装置，其中聚合反应器（1）含有蒸汽入口（4）下半部分和聚合反应器（1），冷却装置（2）和真空单元（3）经由连接器（5）彼此连接。本发明还涉及使用该装置和使用该装置进行强化脱气的方法。

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