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1. 发明授权

US4871808A Binders water-dilutable by protonation with acid 失效
标题翻译：通过用酸质子化可水稀释的粘合剂
公开(公告)号：US4871808A
公开(公告)日：1989-10-03
申请号：US116868
申请日：1987-11-05
申请人： Thomas Schwerzel , Rolf Osterloh , Eberhard Schupp , Thomas Perner , Klaas Ahlers
发明人： Thomas Schwerzel , Rolf Osterloh , Eberhard Schupp , Thomas Perner , Klaas Ahlers
IPC分类号： C08G59/14 , C08G59/00 , C08G59/40 , C08G59/50 , C08L63/00 , C09D5/44 , C09D163/00
CPC分类号： C09D5/4434 , C08G59/50 , C09D163/00
摘要： A binder which is water-dilutable on protonation with acid and obtainable by a reaction of(A) an epoxy resin having an average molecular weight of from 300 to 6,000 and on average from 1.5 to 3.0 epoxide groups per molecule and(B) from 20 to 30 mol %, based on the amount of epoxide groups present in epoxy resin (A), of one or more secondary amine and/or alkanolamine of up to 40 carbon atomsand subsequent reaction with(C) a copolymer which is based on butadiene and acrylonitrile and contains primary and/or secondary amino groups, the amount of (C) being so dimensioned that the number of primary and secondary amino groups corresponds to from 1 to 50 mol % of the epoxide groups present in the epoxy resin (A), and also(D) with one or more primary and/or secondary amine to convert any epoxide groups still present, is usedin particular for cathodic electrocoating.
摘要翻译：可用酸质子化水可稀释的粘合剂，可通过（A）平均分子量为300〜6,000的环氧树脂和每分子平均1.5〜3.0个环氧基团的反应得到（B）20 至多30摩尔％，基于环氧树脂（A）中存在的环氧基团的量，至多40个碳原子的一种或多种仲胺和/或链烷醇胺，随后与（C）基于丁二烯的共聚物反应和丙烯腈，并且包含伯和/或仲氨基，（C）的量的尺寸使得伯和仲氨基的数量对应于环氧树脂（A）中存在的环氧基团的1至50摩尔％，以及（D）与一种或多种伯和/或仲胺以转化仍存在的任何环氧基团，特别用于阴极电涂覆。

2. 发明授权

US5015673A Synthetic resin with basic nitrogen groups, preparation and use thereof using a urethane carrying ketimine 失效
公开(公告)号：US5015673A
公开(公告)日：1991-05-14
申请号：US528374
申请日：1990-05-25
申请人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
发明人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
IPC分类号： C08G59/30 , C08G18/64 , C08G59/14 , C08G59/28 , C08G59/40 , C09D5/44 , C09D163/00
CPC分类号： C09D5/4438 , C08G18/643 , C08G59/4014 , C08G59/4042 , Y10T428/31511 , Y10T428/31522 , Y10T428/31529
摘要： A synthetic resin which carries basic nitrogen groups and is water-dilutable by protonation with acid is obtainable by reacting(A) an epoxy resin having an average molecular weight M.sub.n of from 300 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(B) a ketimine of a primary amine additionally containing one or more urethane groups and optionally also with(C) a diketimine of a diprimary amine containing no urethane groups and optionally also with(D) a secondary amine which may contain a tertiary amino group also, a ketimine of a primary monoamine and/or a ketimine of a primary/tertiary diamine.

3. 发明授权

US5015672A Synthetic resin with basic nitrogen groups, preparation and use thereof using a urethane carrying ketimine 失效
标题翻译：具有碱性氮基团的合成树脂，其制备和使用使用氨基甲酸乙酯携带酮亚胺
公开(公告)号：US5015672A
公开(公告)日：1991-05-14
申请号：US528377
申请日：1990-05-25
申请人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
发明人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
IPC分类号： C08G59/30 , C08G18/64 , C08G59/14 , C08G59/28 , C08G59/40 , C09D5/44 , C09D163/00
CPC分类号： C09D5/4438 , C08G18/643 , C08G59/4014 , C08G59/4042 , Y10T428/31511 , Y10T428/31522 , Y10T428/31529
摘要： A synthetic resin which carries basic nitrogen groups and is water-dilutable by protonation with acid is obtainable by reacting(A) an epoxy resin having an average molecular weight M.sub.n of from 300 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(B) a ketimine of a primary amine additionally containing one or more urethane groups and optionally also with(C) a diketimine of a diprimary amine containing no urethane groups and optionally also with(D) a secondary amine which may contain a tertiary amino group also, a ketimine of a primary monoamine and/or a ketimine of a primary/tertiary diamine.

4. 发明授权

US4956402A Synthetic resin with basic nitrogen groups from resins reacted with the ketimine-urethane product of an alkanolamine, a ketone and anisocyanate 失效
标题翻译：来自树脂的具有碱性氮基团的合成树脂与烷醇胺，酮和异氰酸酯的酮亚胺 - 氨基甲酸酯产物反应
公开(公告)号：US4956402A
公开(公告)日：1990-09-11
申请号：US210499
申请日：1988-06-23
申请人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
发明人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
IPC分类号： C08G59/30 , C08G18/64 , C08G59/14 , C08G59/28 , C08G59/40 , C09D5/44 , C09D163/00
CPC分类号： C09D5/4438 , C08G18/643 , C08G59/4014 , C08G59/4042 , Y10T428/31511 , Y10T428/31522 , Y10T428/31529
摘要： A synthetic resin which carries basic nitrogen groups and is water-dilutable by protonation with acid is obtainable by reacting(A) an epoxy resin having an average molecular weight M.sub.n of from 200 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(B) a ketimine of a primary amine additionally containing one or more urethane groups and optionally also with(C) a diketimine of a diprimary amine containing no urethane groups and optionally also with(D) a secondary amine which may contain a tertiary amimo group also, a ketimine of a primary monoamine and/or a ketimine of a primary/tertiary diamine.
摘要翻译：通过使（A）平均分子量Mn为200〜6,000的环氧树脂和每分子平均1.5〜3.0个环氧基的环氧树脂与（B）另外含有一个或多个氨基甲酸酯基团的伯胺的酮亚胺，以及任选地还含有（C）不含氨基甲酸酯基团的二原子胺的二酮亚胺，并且任选地还可以含有（D）可含有叔胺摩尔组的仲胺也可以是伯/叔二胺的伯胺和/或酮亚胺的酮亚胺。

5. 发明授权

US4981884A Synthetic resin with basic nitrogen groups, preparation and use thereof 失效
标题翻译：具有碱性氮基团的合成树脂，其制备和用途
公开(公告)号：US4981884A
公开(公告)日：1991-01-01
申请号：US210502
申请日：1988-06-23
申请人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
发明人： Thomas Perner , Rolf Osterloh , Eberhard Schupp , Thomas Schwerzel , Klaas Ahlers
IPC分类号： C08L63/00 , C08G59/00 , C08G59/28 , C09D5/44 , C09D163/00
CPC分类号： C09D5/4473 , C09D5/4434
摘要： A synthetic resin which carries basic nitrogen groups and is water-dilutable by protonation with an acid, containing(A) a chain-extended, amine-modified epoxy resin obtainable by reacting(a.sub.1) an epoxy resin having an average molecular weight M.sub.n of from 300 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(a.sub.2) a diketimine of a diprimary diamine, which diprimary diamine contains no further groups reactive with epoxy groups under mild conditions and(B) an amino-modified epoxy resin obtainable by reactingb.sub.1) an epoxy resin having an average molecular weight M.sub.n of from 800 to 6,000 and on average from 1.5 to 3.0 epoxy groups per molecule with(b.sub.2) a secondary amine or a secondary-tertiary diamine, a ketimine of a primary monoamine or a ketimine of a primary/tertiary diamine or a mixture of these (b.sub.2) components, with the proviso that (A) and (B) are different.
摘要翻译：一种合成树脂，其承载碱性氮基团并且可通过用酸质子化而进行水稀释，所述合成树脂含有（A）伸长的胺改性的环氧树脂，其通过使（a1）平均分子量Mn为 300〜6000，平均每个分子具有1.5〜3.0个环氧基，（a2）二元二胺的二酮亚胺，该二元二胺在温和条件下不含有与环氧基反应的其它基团，（B）可得到的氨基改性环氧树脂通过使b1）平均分子量Mn为800至6000，平均每分子具有1.5至3.0个环氧基的环氧树脂与（b2）仲胺或仲叔胺，伯胺的酮亚胺或伯（叔）二胺的酮亚胺或这些（b2）成分的混合物，条件是（A）和（B）不同。

6. 发明授权

US4769420A Binder which is rendered water-dilutable by protonation with an acid, from carboxyl terminated butadiene/acrylonitrile copolymers 失效
标题翻译：由羧基封端的丁二烯/丙烯腈共聚物通过酸质子化而使水可稀释的粘合剂
公开(公告)号：US4769420A
公开(公告)日：1988-09-06
申请号：US934562
申请日：1986-11-25
申请人： Thomas Schwerzel , Rolf Osterloh , Eberhard Schupp , Klaas Ahlers
发明人： Thomas Schwerzel , Rolf Osterloh , Eberhard Schupp , Klaas Ahlers
IPC分类号： C08G59/42 , C08G59/58 , C09D5/44 , C09D151/00 , C09D163/00 , B05D1/28 , B05D7/02
CPC分类号： C09D5/4488 , C08G59/4292 , C08G59/58 , C09D163/00
摘要： Binders which are rendered water-dilutable by protonation with an acid, a process for their preparation and their use.These binders are obtainable by reacting a(A) Reaction product of a(a) carboxyl-containing component, consisting of a(a1) carboxyl-containing butadiene/acrylonitrile copolymer having a molecular weight of from 500 to 8,000, if necessary as a mixture with(a2) a dicarboxylic acid which differs from (a1) and, if appropriate,(a3) a monocarboxylic acid and(b) a diprimary and/or primary/secondary amine, with the proviso that from 0.7 to 5 moles of the said amine are used per mole of carboxyl groups of component (a), with one or more(B) epoxy resins having a mean molecular weight from 300 to 6,000 and containing on average from 1.5 to 3.0 epoxide groups per molecule and, if required,(C) an aliphatic or cycloaliphatic secondary amine.In combination with a crosslinking agent, they are useful as coating materials, in particular for cathodic electrocoating.
摘要翻译：通过用酸质子化可水稀释的粘合剂，其制备方法及其用途。这些粘合剂可以通过使（A）含羧基组分的反应产物（如有必要）与由（a1）分子量为500-8,000的（a1）含羧基的丁二烯/丙烯腈共聚物组成的混合物与（a1）和（a1）不同的二羧酸和（a3）一元羧酸和（b）二原子和/或伯/仲胺，如果合适的话，条件是0.7-5摩尔所述胺组分（a）的每摩尔羧基使用，一种或多种（B）环氧树脂的平均分子量为300至6,000，每分子平均含有1.5至3.0个环氧基团，如果需要，（ C）脂族或脂环族仲胺。与交联剂组合，它们可用作涂料，特别是用于阴极电泳涂覆。

7. 发明授权

US4594136A Cathodic electrocoating binders 失效
标题翻译：阴极电泳粘合剂
公开(公告)号：US4594136A
公开(公告)日：1986-06-10
申请号：US755725
申请日：1985-07-17
申请人： Eberhard Schupp , Werner Loch , Rolf Osterloh , Klaas Ahlers
发明人： Eberhard Schupp , Werner Loch , Rolf Osterloh , Klaas Ahlers
IPC分类号： C08G18/64 , C08G18/67 , C08G18/81 , C09D5/44 , C25D13/00
CPC分类号： C09D5/4419 , C08G18/643 , C08G18/6705 , C08G18/8158 , Y10S524/901
摘要： Binders useful for cathodic electrocoating are water-dilutable on addition of acid and comprise a mixture of(A) a polyadduct which carries basic nitrogen groups and contains groups of the formula (I) and/or (II) ##STR1## where R.sup.1 and R.sup.2 are hydrogen or methyl and R.sup.3 and R.sup.4 are alkyl or hydroxyalkyl or together are a 5- or 6-membered ring, and(B) a reaction product of a polyisocyanate and an olefinically unsaturated amine which carries a secondary amino group and a methacrylamide or methacrylate group.
摘要翻译：用于阴极电泳的粘合剂在加入酸时是可水稀释的，并且包含（A）含有碱性氮基团并含有式（I）和/或（II）的基团的多加成物的混合物。（II）其中R1和R2是氢或甲基，R3和R4是烷基或羟基烷基或一起是5-或6-元环，和（B）多异氰酸酯和烯属不饱和胺的反应产物，其携带仲氨基和甲基丙烯酰胺或甲基丙烯酸酯基。

8. 发明授权

US4576979A Heat-curable surface-coating agents, and their use 失效
标题翻译：可热固化的表面涂层剂及其用途
公开(公告)号：US4576979A
公开(公告)日：1986-03-18
申请号：US547094
申请日：1983-10-31
申请人： Eberhard Schupp , Werner Loch , Rolf Osterloh , Klaas Ahlers
发明人： Eberhard Schupp , Werner Loch , Rolf Osterloh , Klaas Ahlers
IPC分类号： C09D5/03 , C08G18/08 , C08G18/64 , C08G18/67 , C08G18/80 , C09D5/44 , C09D5/46 , C09D175/00 , C08K3/20 , C08L63/02
CPC分类号： C08G18/0814 , C08G18/643 , C08G18/6705 , C08G18/808 , C09D5/4496 , C08G2150/20 , Y10S524/901 , Y10S524/904 , Y10S525/934 , Y10T428/31529
摘要： Heat-curable surface-coating agents useful not only for application as solvent-containing finishes and for powder coating but also, in their protonated form, for cathodic electrocoating contain, as a binder, a mixture of (A) a polyadduct, polycondensate or other polymer having an average molecular weight M.sub.n of from 500 to 10,000 and, per molecule, on average two or more OH and/or primary and/or secondary amino groups and (B) a reaction product of (a) one or more polyisocyanates, (b) one or more secondary monoamines and, if appropriate, (c) one or more polyalcohols having two or more hydroxyl groups.
摘要翻译：用于阴离电涂层的热固化性表面涂层剂不仅可用作含溶剂的表面处理剂和粉末涂料，而且以其质子化形式用作含有（A）多加成物，缩聚物或其它物质的混合物作为粘合剂平均分子量＆gt; Mn为500至10,000，并且每分子平均有两个或更多个OH和/或伯和/或仲氨基的聚合物和（B）一种或多种多异氰酸酯的反应产物，（b）一种或多种二级单胺，如果合适，（c）一种或多种具有两个或多个羟基的多元醇。

9. 发明授权

US4699937A Synthetic resin carrying basic nitrogen groups, its preparation, coating materials produced using this resin, and cathodic electrocoating 失效
标题翻译：携带碱性氮基团的合成树脂，其制备方法，使用该树脂制备的涂料，以及阴极电泳涂料
公开(公告)号：US4699937A
公开(公告)日：1987-10-13
申请号：US808281
申请日：1985-12-12
申请人： Werner Loch , Eberhard Schupp , Rolf Osterloh , Klaas Ahlers
发明人： Werner Loch , Eberhard Schupp , Rolf Osterloh , Klaas Ahlers
IPC分类号： C08G59/40 , C08G59/56 , C09D5/44 , C08G59/46
CPC分类号： C09D5/4434 , C08G59/4042 , C08G59/56
摘要： A synthetic resin carrying basic nitrogen groups, its preparation, coating materials prepared from this resin, and a process for cathodic electrocoating.This synthetic resin is obtained by reacting(A) an epoxy resin which(B) a diketimine of a diprimary amineand, if required,(C) with a secondary amine, which may additionally contain a tertiary amino group, with a ketimine of a primary monoamine and/or with a ketimine of a primary/tertiary diamine,a diketimine obtained from(B.sub.1) a ketone and(B.sub.2) a branched aliphatic diprimary diamine of 5 to 9 carbon atoms and/or(B.sub.3) one or more diaminodiamides which are obtained by condensation of 2 moles of diamine (B.sub.2) and 1 mole of a dicarboxylic acidbeing employed as component (B).After protonation with an acid, this synthetic resin is useful as a binder for cathodic electrocoating.
摘要翻译：携带碱性氮基团的合成树脂，其制备方法，由该树脂制备的涂料，以及阴极电泳方法。该合成树脂通过使（A）环氧树脂与（B）二胺的二酮亚胺和（如果需要的话）（C）与另外含有叔氨基的仲胺和（B1）酮和（B2）碳原子数为5〜9的支链脂肪族二元二胺和/或（B3）一种或多种二氨基二胺的二酮亚胺，其主要单胺和/或与伯/叔二胺的酮亚胺，通过2摩尔二胺（B2）和1摩尔作为组分（B）的二羧酸的缩合获得。在用酸质子化后，该合成树脂可用作阴极电涂层的粘合剂。

10. 发明授权

US4557814A Synthetic resin carrying basic nitrogen groups, and its preparation 失效
标题翻译：携带碱性氮基的合成树脂及其制备方法
公开(公告)号：US4557814A
公开(公告)日：1985-12-10
申请号：US629762
申请日：1984-07-11
申请人： Eberhard Schupp , Werner Loch , Rolf Osterloh , Klaas Ahlers
发明人： Eberhard Schupp , Werner Loch , Rolf Osterloh , Klaas Ahlers
IPC分类号： C08G18/00 , C08G18/58 , C08G59/00 , C08G59/14 , C08G59/40 , C09D5/44 , C09D163/00 , C09D175/00 , C08G59/50
CPC分类号： C09D5/4438 , C08G59/4028 , C08G59/4042 , C09D163/00
摘要： A synthetic resin which carries basic nitrogen groups and can be diluted with water as a result of protonation with an acid can be obtained by reacting an epoxy resin, having a mean molecular weight M.sub.n of from 300 to 6,000 and containing on average from 1.5 to 3.0 epoxide groups per molecule, with a diketimine of a primary diamine and, if appropriate, a secondary amine, which may additionally contain a tertiary amino group, a ketimine of a primary monoamine and/or a ketimine of a primary/tertiary diamine.These resins are useful as binders for coating agents, in particular for the cathodic electrocoating of electrically conductive substrates.
摘要翻译：携带碱性氮基并可用酸质子化的水稀释的合成树脂可以通过使平均分子量＆Upbar＆Mn的平均分子量＆Mn> 300至6,000并且平均含有1.5的环氧树脂与每个分子具有3.0个环氧基团，与一个二胺的二酮亚胺和如果合适的话，可以另外含有叔氨基的仲胺，伯/叔二胺的伯胺和/或酮亚胺的酮亚胺。这些树脂可用作涂层剂的粘合剂，特别是用于导电基材的阴极电涂层。

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