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1. 发明专利

JP2001155727A POSITIVE ELECTRODE ACTIVE MATERIAL FOR USE IN NON-AQUEOUS LITHIUM SECONDARY BATTERY AND METHOD OF FABRICATING IT 失效
公开(公告)号：JP2001155727A
公开(公告)日：2001-06-08
申请号：JP33242699
申请日：1999-11-24
申请人： HITACHI METALS LTD , HITACHI LTD
发明人： TANAKA MUNEYUKI , NAKAJIMA MOTOE , UCHIKAWA TERUO , KASAI MASAHIRO , YAMAKI TAKAHIRO
IPC分类号： C01G45/00 , H01M4/131 , H01M4/505 , H01M10/05 , H01M4/58 , H01M4/02 , H01M10/40
摘要： PROBLEM TO BE SOLVED: To provide a positive electrode active material for a non-aqueous lithium secondary battery that has high output discharge characteristics and stable cycle characteristics with long life. SOLUTION: A lithium secondary battery comprises a negative electrode of a carbonic material joined with a positive electrode coated with a complex oxide consisting of Li and transition metal as the positive active material through a separator and non-aqueous electrolyte filled inside. The positive active material is a lithium and manganese complex compound of spinel structure that consists of primary particles, and secondary particles obtained by condensing the primary particles. The primary particles have average particle size of 1-50 μm, including particles with octahedral crystal face (111) by at least 3%.

2. 发明专利

JP2003203632A POSITIVE ELECTRODE ACTIVE MATERIAL FOR LITHIUM SECONDARY BATTERY AND ITS MANUFACTURING METHOD, LITHIUM SECONDARY BATTERY USING THE SAME, AND BATTERY PACK MODULE 审中-公开
公开(公告)号：JP2003203632A
公开(公告)日：2003-07-18
申请号：JP2002001965
申请日：2002-01-09
申请人： HITACHI LTD , HITACHI METALS LTD , SHIN KOBE ELECTRIC MACHINERY
发明人： KASAI MASAHIRO , KUMASHIRO YOSHIAKI , NAKAJIMA MOTOE , UCHIKAWA TERUO , NAKAI KENJI
IPC分类号： C01G45/00 , C01G51/00 , H01M2/10 , H01M4/36 , H01M4/505 , H01M10/05 , H01M10/0525 , H01M10/0566 , H01M4/58 , H01M10/40
摘要： PROBLEM TO BE SOLVED: To provide a positive electrode active material for a lithium secondary battery that has characteristics of high output and maintaining the high output for a long period of time and its manufacturing method, and a lithium secondary battery using the same, and a battery pack module combining it plural pieces. SOLUTION: This is a positive electrode active material for a lithium secondary battery which is made of an aggregated body in which oxides of a primary particle shape containing lithium and manganese are coagulated electrostatically and/or mechanically and the aggregated body is separated into individual primary particles by a physical outside force, and its manufacturing method, and a lithium secondary battery using the same, and a battery pack module combining it plural pieces. COPYRIGHT: (C)2003,JPO

3. 发明专利

JP2011155003A Cathode active material for nonaqueous lithium secondary battery and producing method therefor 有权
标题翻译：用于非水锂二次电池的阴极活性材料及其生产方法
公开(公告)号：JP2011155003A
公开(公告)日：2011-08-11
申请号：JP2011001686
申请日：2011-01-07
申请人： Hitachi Ltd , Hitachi Metals Ltd , 日立金属株式会社 , 株式会社日立製作所
发明人： TANAKA MUNEYUKI , NAKAJIMA MOTOE , UCHIKAWA TERUO , KASAI MASAHIRO , YAMAKI TAKAHIRO
IPC分类号： H01M4/505 , C01G45/12
CPC分类号： Y02P70/54
摘要： PROBLEM TO BE SOLVED: To provide a cathode active material for a nonaqueous lithium secondary battery with stable high output discharge characteristics and cycle characteristics, and with a long life. SOLUTION: A method of producing a cathode active material for a nonaqueous lithium secondary battery composed of a spinel-structured lithium-manganese composite oxide includes steps of: granulating a mixture powder of a raw material of the cathode active material into granules; performing a first calcination of calcinating the cathode active material at temperatures 800-1,100°C in an atmosphere; then further shredding it; and performing a second calcination of calcinating it again at temperatures of 600±100°C. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供具有稳定的高输出放电特性和循环特性以及长寿命的非水锂二次电池用正极活性物质。解决方案：制备由尖晶石结构的锂锰复合氧化物构成的非水锂二次电池用正极活性物质的方法包括以下步骤：将正极活性物质的原料的混合粉末粒化成颗粒; 在大气中在800-1100℃的温度下进行煅烧阴极活性材料的第一次煅烧; 然后进一步切碎它; 并在600±100℃的温度下再次进行煅烧。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2005150102A Cathode active material for lithium secondary cell and its manufacturing mathod as well as nouaqueous lithium secondary cell 有权
标题翻译：用于锂二次电池的阴极活性材料及其作为NOUAQUEOUS锂二次电池的制造方法
公开(公告)号：JP2005150102A
公开(公告)日：2005-06-09
申请号：JP2004306421
申请日：2004-10-21
申请人： Hitachi Metals Ltd , 日立金属株式会社
发明人： NAKAJIMA MOTOE , INADA FUMI , UCHIKAWA TERUO
IPC分类号： C01G53/00 , H01M4/131 , H01M4/505 , H01M4/525 , H01M4/58 , H01M10/05 , H01M4/02 , H01M10/40
CPC分类号： Y02P70/54
摘要： PROBLEM TO BE SOLVED: To provide a cathode active material with suppressed aggregation and a raised coating property and its manufacturing method as well as a lithium secondary cell having a good output property using the cathode active material by providing a distinction index whether the cathode active material is aggregated.
SOLUTION: The cathode active material for a lithium secondary cell which is a nonaqueous lithium secondary cell being a lithium-containing compound oxide as a cathode active material absorbing and releasing a lithium ion has a median radius D50 ratio of the cathode active material (a value of D50 (without ultrasonic waves)/D50 (with ultrasonic waves)) of 1 or more and 2 or less by calculating laser diffractions when the cathode active material is dispersed in ethanol with the ultrasonic waves, and without using the ultrasonic waves. The cathode active material is manufactured with processes up to classification and packing after calcination under an environment of 20g(20g/m
3 ) or less of a water vapor content per cubic meter.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：为了提供具有抑制聚集和提高的涂层性能的正极活性材料及其制造方法以及使用阴极活性材料具有良好输出性能的锂二次电池，通过提供一种区别指数正极活性物质聚集。解决方案：作为吸收和释放锂离子的正极活性物质的作为含锂复合氧化物的非水锂二次电池用锂二次电池用正极活性物质，正极活性物质的中值半径D50比例（超声波）的D50（超声波）/ D50（超声波））为1以上且2以下时，通过计算激光衍射，当超声波分散在乙醇中时，不使用超声波。在20g（20g / m 3 / SP）以下的水蒸汽含量/立方米的环境下煅烧后，制造直至分类和包装的正极活性物质。版权所有（C）2005，JPO＆NCIPI

5. 发明专利

JP2005150057A Cathode active material for nonaqueous system lithium secondary battery, its manufacturing method, and nonaqueous system lithium secondary battery using the material 有权
标题翻译：用于非水系统锂离子电池的阴极活性材料，其制造方法和使用材料的非水系统锂二次电池
公开(公告)号：JP2005150057A
公开(公告)日：2005-06-09
申请号：JP2003390194
申请日：2003-11-20
申请人： Hitachi Metals Ltd , 日立金属株式会社
发明人： INADA FUMI , NAKAJIMA MOTOE , UCHIKAWA TERUO
IPC分类号： C01G53/00 , H01M4/505 , H01M4/525 , H01M10/05 , H01M4/58 , H01M4/02 , H01M10/40
CPC分类号： Y02P70/54
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method for a positive active material for a nonaqueous lithium secondary battery providing high output, and also to provide the positive active material and the lithium secondary battery using it.
SOLUTION: In the nonaqueous system lithium secondary battery with a complex oxide composed of lithium and transition metal as the cathode active material, the cathode active material is expressed in a composition formula: Li
a Mn
x Ni
y M
z O
2 [M=at least either of Co, Al] and is a compound having a lamellar crystal structure of:x+y+z=1 within a range of 1≤a≤1.2, 0.2≤x≤0.5, 0.35≤y≤0.5, 0≤z≤0.45. When the cathode active material is dispersed with pure water (pH 7.2-7.5) in an amount of 5 weight times, the pH of its supernatant liquid is 10.0-12.0.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：解决的问题：提供一种提供高输出的非水锂二次电池的正极活性材料的制造方法，并且还提供使用它的正极活性物质和锂二次电池。解决方案：在具有由锂和过渡金属组成的复合氧化物作为正极活性物质的非水系锂二次电池中，正极活性物质以组成式表示：Li a SB> x Ni M O [M = Co，Al中的至少任一种]，并且是具有在1≤a≤1.2,0.2≤x≤0.5,0.35≤y≤0.5,0≤z≤0.45的范围内的x + y + z = 1的层状晶体结构。当阴极活性物质以5重量倍的纯水（pH7.2-7.5）分散时，其上清液的pH为10.0-12.0。版权所有（C）2005，JPO＆NCIPI

6. 发明专利

JP2004311427A Positive electrode active material for lithium secondary battery and its manufacturing method and non-aqueous lithium secondary battery 有权
公开(公告)号：JP2004311427A
公开(公告)日：2004-11-04
申请号：JP2004086963
申请日：2004-03-24
申请人： Hitachi Metals Ltd , 日立金属株式会社
发明人： NAKAJIMA MOTOE , INADA FUMI , UCHIKAWA TERUO
IPC分类号： C01G53/00 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/05 , H01M4/58 , H01M4/02 , H01M10/40
CPC分类号： Y02P70/54
摘要： PROBLEM TO BE SOLVED: To provide a lithium secondary battery of which increase of output and impairment of output due to inner resistance decrease is prevented and to provide a positive electrode active material to be used for this and its manufacturing method. SOLUTION: In the non-aqueous lithium secondary battery using a composite oxide consisting of lithium and a transition metal as a positive electrode active material, filling property (%) of the positive electrode active material for the lithium secondary battery which is represented by (tap density/actual density)×100 is less than 55%. For the positive electrode active material, size of a crystallite measured by the Hall method is 400Å to 850Å and represented by the composition formula Li a Mn x Ni y X z O 2 (X: at least one of Co and A1), and is preferably a composite oxide having a layer structure for satisfying the ranges below: 1≤a≤1.2, 0.2≤x≤0.5, 0.35≤y≤0.8, 0≤z≤0.45, x+y+z=1. COPYRIGHT: (C)2005,JPO&NCIPI

7. 发明专利

JP2003077474A Positive electrode active material for lithium secondary battery and its manufacturing method 审中-公开
标题翻译：用于锂二次电池的正极电极活性材料及其制造方法
公开(公告)号：JP2003077474A
公开(公告)日：2003-03-14
申请号：JP2001270342
申请日：2001-09-06
申请人： Hitachi Metals Ltd , 日立金属株式会社
发明人： NAKAJIMA MOTOE , UCHIKAWA TERUO , INADA FUMI
IPC分类号： C01G45/00 , C01G51/00 , H01M4/505 , H01M10/05 , H01M4/58 , H01M4/02 , H01M10/40
CPC分类号： Y02P70/54
摘要： PROBLEM TO BE SOLVED: To provide a positive electrode active material that is superior in high temperature standing characteristics at charge and discharge, and its manufacturing method.
SOLUTION: This is a positive electrode active material that is mainly made of a lithium manganese composite oxide as expressed by the following formula, Li
1+x Mn
2-x-y A
y O
4 (where A is at least one element selected from Co and Al, and 0
摘要翻译：要解决的问题：提供一种在充放电时的高温静置特性优异的正极活性物质及其制造方法。解决方案：这是一种主要由如下式表示的锂锰复合氧化物Li1 + xMn2-xyAaO4（其中A为选自Co和Al中的至少一种元素）和0

8. 发明专利

JP2002110156A MANUFACTURING METHOD OF POSITIVE POLE ACTIVE MATERIAL FOR NONAQUEOUS LITHIUM SECONDARY BATTERY, AND ITS POSITIVE POLE ACTIVE MATERIAL AND NONAQUEOUS LITHIUM SECONDARY BATTERY USING IT 失效
公开(公告)号：JP2002110156A
公开(公告)日：2002-04-12
申请号：JP2000295712
申请日：2000-09-28
申请人： HITACHI METALS LTD
发明人： TANAKA MUNEYUKI , NAKAJIMA MOTOE , UCHIKAWA TERUO
IPC分类号： C01G45/00 , C01G51/00 , H01M4/131 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/05 , H01M4/58 , H01M4/02 , H01M10/40
摘要： PROBLEM TO BE SOLVED: To make the charge and discharge capacity of a nonaqueous lithium secondary battery, which uses transition metal oxide lithium positive pole active material in a positive pole, larger than traditional one. SOLUTION: The lithium transition metal oxide is produced by mixing and baking at least one type from compound of Co, Mn, etc., and lithium compound. The baked particle is heat-treated in oxygen atmosphere on coagulating and balling after melting the surface by heat-treating the baked particle by plasma, for example. The positive pole active material produced by returning the crystal structure to the one of the lithium transition metal oxide exhibits large charge and discharge capacity.

9. 发明专利

JPH06290952A LAMINATED INDUCTOR AND INDUCTANCE ADJUSTING METHOD THEREOF 失效
公开(公告)号：JPH06290952A
公开(公告)日：1994-10-18
申请号：JP7654593
申请日：1993-04-02
申请人： HITACHI METALS LTD , HITACHI FERRITE LTD
发明人： KURIHARA KOICHIRO , TAKEDA SHIGERU , OGAWA KYOZO , TANAKA MUNEYUKI , UCHIKAWA TERUO
IPC分类号： G01R27/26 , H01F17/00 , H01F41/00 , H01F41/04
摘要： PURPOSE:To enable a laminated inductor to be easily controlled in inductance by a method wherein a through-hole is provided in a laminating direction to the center of the laminated green sheets where a coiled conductor pattern is formed, external electrode terminals are provided to both side faces of the conductor pattern, and a conductor is inserted into the through-hole. CONSTITUTION:A green sheet 1 where a conductor pattern 2 is so printed as to be aligned with a through-hole 3 is cut into a prescribed size through a position aligning method wherein a guide pin and a guide hole are used. The green sheets 1 where conductor patterns 2 are printed are laminated in a lamination mold and thermocompressed into a laminate. A through-hole 7 is bored in the laminate at a prescribed position. Then, the laminate is cut into a chip, outer electrodes 4 are provided and plated with Ni and solder. Lastly, a copper conductor 8 is inserted into the through-hole 7.

10. 发明专利

JP2009021260A Positive active material for nonaqueous lithium secondary battery, positive electrode using the active material, and nonaqueous lithium secondary battery 有权
标题翻译：非活性锂二次电池的正极活性物质，使用活性材料的正极和非碱性锂二次电池
公开(公告)号：JP2009021260A
公开(公告)日：2009-01-29
申请号：JP2008245751
申请日：2008-09-25
申请人： Hitachi Metals Ltd , 日立金属株式会社
发明人： NAKAJIMA MOTOE , UCHIKAWA TERUO , INADA FUMI
IPC分类号： H01M10/052 , H01M4/131 , H01M4/1391 , H01M4/505 , H01M4/525 , H01M10/0566
CPC分类号： Y02T10/7011
摘要： PROBLEM TO BE SOLVED: To increase discharge capacity of a positive electrode of a nonaqueous lithium secondary battery using a lithium-transition metal composite oxide in the positive electrode than conventional one. SOLUTION: A lithium secondary battery has a negative electrode, a positive electrode formed by coating a composite oxide including lithium and transition metal as the positive active material, a separator interposed between the negative electrode and the positive electrode, and a nonaqueous electrolyte. The positive active material of the lithium secondary battery is globular particles obtained in such a way that a transition metal compound, a lithium compound and water are mixed in a prescribed ratio to prepare slurry, the slurry is sprayed with a spray dryer having a four fluid nozzle, dried, and baked. The globular particles have an average particle diameter of 1-20 μm and a maximum particle diameter of 50 μm or less. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：使用正极中的锂 - 过渡金属复合氧化物，提高非水锂二次电池的正极的放电容量比常规锂离子电池的放电容量大。解决方案：锂二次电池具有负极，通过涂覆包含锂和过渡金属的复合氧化物作为正极活性材料形成的正极，插入在负极和正极之间的隔膜，以及非水电解质。锂二次电池的正极活性物质是以过渡金属化合物，锂化合物和水以规定的比例混合以制备浆料而获得的球状颗粒，用具有四种流体的喷雾干燥器喷嘴，干燥并烘烤。球状颗粒的平均粒径为1-20μm，最大粒径为50μm以下。版权所有（C）2009，JPO＆INPIT

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