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    • 10. 发明专利
    • Preparation of high-purity silicon and its apparatus
    • 高纯硅及其设备的制备
    • JPS58185427A
    • 1983-10-29
    • JP6607382
    • 1982-04-20
    • Hitachi Ltd
    • UTAKA MASATOSHI
    • C01B33/02C01B33/037
    • PURPOSE: To enable the production of high-purity silicon efficiently and safely for a long time, by precipitating silicon from a silicon-containing gas on high- purity silicon particles in a fluidized bed reactor equipped with a heating materil in it.
      CONSTITUTION: In the fluidized bed reactor 1, high-purity silicon fine particles are fed from the fine particle feed pipe 2 to it, a mixed gas of trichlorosilane or dichlorosilane and hydrogen is fed from the gas feed pipe 3, a silicon-containing gas is prepared, and a fluidized bed is formed. While, electricity is applied from the contact terminals 6 and 6' to the plural heating materials 5 consiting of silicon bard set at equal spaces on the circumference of the concentrated circle of the inner wall of the cylindrical container 1, the inside of the container is heated, silicon is deposited from the silicon-containing gas on the fine particles, to form granular high-purity silicon. The bar heating material 5 may have a circular or square shape, or a silicon cylinder having pores may be used.
      COPYRIGHT: (C)1983,JPO&Japio
    • 目的:为了能够长时间高效,安全地生产高纯度硅,通过在装有加热材料的流化床反应器中,通过在高纯度硅颗粒上的含硅气体中沉淀出硅。 构成:在流化床反应器1中,从细颗粒供给管2向其供给高纯度硅微粒,从气体供给管3供给三氯硅烷或二氯硅烷与氢的混合气体,含硅气体 并且形成流化床。 同时从接触端子6,6'向从圆筒形容器1的内壁的圆周的等间距设置的多个加热材料5施加电力,容器的内部为 加热后,将硅从含硅气体沉积在微粒上,形成粒状高纯度硅。 棒状加热材料5可以具有圆形或正方形形状,或者可以使用具有孔的硅圆筒。