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1. 发明申请

WO1993016165A1 POWDERED OR GRANULATED, DUST-FREE CONCENTRATES OF ANIONIC SURFACE ACTIVE AGENTS WITH IMPROVED DISSOLVABILITY 审中-公开
标题翻译：粉末状或颗粒状，具有改善溶解性的阴离子表面活性剂的无污染浓度
公开(公告)号：WO1993016165A1
公开(公告)日：1993-08-19
申请号：PCT/EP1993000302
申请日：1993-02-09
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , FUES, Johann , RÄHSE, Wilfried , PAATZ, Kathleen , POLY, Wolfgang , GRUBER, Bert , SYLDATH, Andreas , WELPER, Sven , PATTBERG, Herbert
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： C11D11/00
CPC分类号： C11D11/02 , B01D1/18 , C11D11/0082 , C11D11/04 , C11D17/06 , F26B3/12 , F26B21/04
摘要： Solid, pourable powdered and/or granulated concentrates of anionic surface active agents, which may also constitute compounds admixed with other auxiliary and/or valuable substances suitable for washing and/or cleaning agents, are produced by drying corresponding aqueous compositions until the powder and/or granulate is produced. The teaching of the invention is characterized by the design of the concentrates as a dust-free material, in which the anionic surface active compounds are available at least partially as their washing and/or cleaning active salts. The concentrates of anionic surface active agents have settled apparent densities of at least 150 g/l approximately and are produced by hot-drying the aqueous compositions with overheated steam as the drying gas. Preferred settled apparent densities lie above 200 g/l approximately, in particular around 350 g/l at least. In addition, the bulk and pourable material is preferably designed as a substantially dust-free material thanks to the use of dust-binding auxiliary and/or valuable substances and/or to the regulation of the residual water content. In a preferred embodiment, the concentrate of anionic surface active agents is designed as a porous carrier bead with an absorbent porous inner structure.
摘要翻译：通过干燥相应的含水组合物，可以制备阴离子表面活性剂的固体，可倾倒的粉末和/或颗粒状浓缩物，其也可以构成与适用于洗涤剂和/或清洁剂的其它辅助和/或有价值物质混合的化合物，直到粉末和/ 或颗粒产生。本发明的教导的特征在于将浓缩物设计为无尘材料，其中阴离子表面活性化合物至少部分可用作其洗涤和/或清洁活性盐。阴离子表面活性剂的浓缩物已将至少150g / l的表观密度稳定沉淀，并通过用作为干燥气体的过热蒸汽将含水组合物热干燥来制备。优选的沉降表观密度大约在200g / l以上，特别是至少约350g / l。此外，由于使用防尘结合助剂和/或有价值物质和/或调节残留水含量，本体和可倾倒材料优选地被设计为基本无粉尘的材料。在优选的实施方案中，阴离子表面活性剂的浓缩物被设计为具有吸收性多孔内部结构的多孔载体珠粒。

2. 发明申请

WO1994009109A1 VALUABLE SUBSTANCES AND MIXTURES OF VALUABLE SUBSTANCES FOR WETTING AGENTS, DETERGENTS AND/OR CLEANERS IN A NEW FORM OF PREPARATION 审中-公开
标题翻译： VALUE物质和价值 - 网络，洗涤和/或清洁新剂型
公开(公告)号：WO1994009109A1
公开(公告)日：1994-04-28
申请号：PCT/EP1993002703
申请日：1993-10-04
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , RÄHSE, Wilfried , FUES, Johann, Friedrich , PATTBERG, Herbert , PAATZ, Kathleen
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： C11D11/00
CPC分类号： B01D1/18 , C11D11/02 , C11D17/06 , F26B3/12 , F26B21/04
摘要： The invention pertains to valuable substances and mixtures of valuable substances that can be used in wetting agents, detergents and/or cleaners and that take the form of pourable granular material that is obtained by loading a granular base (carrier bead) with a preparation (applied substance) containing valuable substances of the indicated type. The invention is characterized in that the carrier bead is a material obtained by spray and/or fluidized bed drying in superheated steam. The carrier bead is also preferably constituted using surface active valuable substances, especially anionic surface active agents which at least in part are solids at temperatures of about 100 DEG C. The invention further pertains to the non-loaded carrier beads of the kind previously described, a process for producing the loaded carrier beads and the use of the loaded and non-loaded carrier beads as constituents of wetting agents, detergents and/or cleaners offered in solid form.

3. 发明申请

WO1993015811A1 PROCESS FOR DRYING VALUABLE SUBSTANCES OR THEIR MIXTURES USEFUL AS WETTING, WASHING AND/OR CLEANING AGENTS 审中-公开
标题翻译：干燥有价物质或其混合物的方法可用作湿巾，洗涤和/或清洁剂
公开(公告)号：WO1993015811A1
公开(公告)日：1993-08-19
申请号：PCT/EP1993000264
申请日：1993-02-04
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , RÄHSE, Wilfried , FUES, Johann , BECK, Wilhelm , WELPER, Sven
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： B01D01/18
CPC分类号： F26B3/12 , B01D1/18 , C11D11/02 , C11D11/04 , F26B21/04
摘要： Overheated steam is used as drying gas and is recirculated in the drying stage once the evaporated water has been transferred out. The system is operated at steam temperatures at the outlet of the drying zone of at least 150 DEG C, in particular at least 180 DEG C approximately, and under inner pressures of the steam-filled system in the normal pressure range, but in particular under raised pressures, so that air intrusion into the system, in particular at damaged spots, is avoided. System inner pressures below approximately 50 mbar overpressure are preferred. The given operation parameters for the process allow products with determined properties, for example apparent density, to be obtained in a reproducible manner.
摘要翻译：过热蒸汽用作干燥气体，一旦蒸发的水被转出，就在干燥阶段再循环。该系统在干燥区的出口处的蒸汽温度下操作，至少150℃，特别是至少180℃，在蒸汽填充系统的内压在常压范围内，特别是在提高了压力，从而避免了空气侵入系统，特别是在受损点处。优选系统内部压力低于约50毫巴超压。该方法的给定操作参数允许以可再现的方式获得具有确定性质的产品，例如表观密度。

4. 发明申请

WO1995023841A1 MULTI-SUBSTANCE MIXTURES BASED ON WATER-SOLUBLE ALKALI SILICATE COMPOUNDS AND THEIR USE 审中-公开
标题翻译：更多的水为基础的含碱硅酸盐化合物及其用途
公开(公告)号：WO1995023841A1
公开(公告)日：1995-09-08
申请号：PCT/EP1995000604
申请日：1995-02-20
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , RÄHSE, Wilfried , FUES, Johann, Friedrich , PAATZ, Kathleen , BECK, Wilhelm , HLAVACEK, Wolfgang
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： C11D03/08
CPC分类号： C11D3/046 , C11D3/06 , C11D3/08 , C11D3/10 , C11D3/2075 , C11D3/3761 , C11D11/0082 , C11D11/02
摘要： The invention concerns a solid material (primary dry material) which contains alkali metal silicates in the modules range (SiO2: M2O molar ratio in which M= alkali metal) of 0.8 to 4 in a homogeneous mixture with other inorganic and/or organic valuable and/or auxiliary substances. This solid material has been dried, by means of a hot gas flow, from a finely sprayed aqueous preparation of mixtures of the alkali metal silicates and the inorganic and/or organic valuable and/or auxiliary substances. The solid material according to the invention is characterized in that, as a primary dry material in a homogeneous mixture with the alkali silicate, it has at least 10 wt % water-soluble inorganic and/or organic salts, apparent densities of at least 150 g/l and a microporous, absorbent inner material structure, and has been dried by means of superheated steam as the hot gas flow. The invention further relates, in particular, to builder systems for detergents and washing agents based on these multi-substance systems containing super-dried alkali silicate and their use for subsequent treatment with further, flowable, valuable substances and valuable substance mixtures from the field of detergents and washing agents, and to the detergents and washing agents produced thereby.
摘要翻译：本发明公开了所述模块区域的碱金属硅酸盐：0.8（摩尔比的SiO 2 :M 2 O，其中M =碱金属）至4与其它无机和/或有机有用的材料和/或固体材料（主要干基料）含有赋形剂-在均匀的混合物，由细碎通过热气体流的装置中的碱金属硅酸盐和无机和/或有机的材料，并且/或助剂的混合物的喷涂水性制剂已经枯竭。本发明的固体材料的特征在于它含有如在均匀的混合物的主干材料与碱金属硅酸盐是至少10重量的水溶性无机和/或有机盐％，至少150克/升的堆积密度有，除此之外，具有微孔的，吸收性Gutinnenstruktur和干燥了由过热蒸汽的装置的热气体流。本发明还涉及在用于洗涤和清洁基于含有多组分体系以及它们用于从洗涤剂和清洁剂领域的可流动的其它有用的材料和有用的材料的混合物的随后的应用中使用这些过干Alakalisilikat组合物和所产生的洗涤和清洁剂特别洗剂体系。

5. 发明申请

WO1995025065A1 LONG-SHELF-LIFE FIXED HYDROGEN PEROXIDE-CONTAINING MULTI-SUBSTANCE MIXTURES IN SOLID FORM, PROCESS FOR THEIR PRODUCTION AND THEIR USE 审中-公开
标题翻译：储存稳定的固定含氢更含有固体形式，其制造方法相同，它们的用途
公开(公告)号：WO1995025065A1
公开(公告)日：1995-09-21
申请号：PCT/EP1995000820
申请日：1995-03-06
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , RÄHSE, Wilfried , FUES, Johann, Friedrich , PAATZ, Kathleen , UPADEK, Horst
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： C01B15/10
CPC分类号： C11D3/3942 , C01B15/00 , C01B15/10
摘要： The invention describes a water-soluble multi-substance compound as a solid mixture which can in particular be used as a bleaching and/or disinfecting agent, containing absorbed and/or bonded hydrogen peroxide and possibly per compounds formed in situ through its action, included in a mixture of (K1) solid alkaline silicates of the modular range (mol ratio SiO2:M2O, where M = alkaline metal) from 0.8 to 10 and (K2) at least one other solid component from the class of water-soluble inorganic and/or organic salts which can in particular bond H2O and/or H2O2. The invention is characterised in that, in the multi-substance compound, the proportion (K1) is at least 5 wt % and that (K2) is at least 10 wt % - in relation to the sum (K1) + (K2) - where (K1) and (K2) are present in a microdispersed homogenous mixture through drying from a common aqueous preparation, and the H2O2 is included in the multi-substance compound during said drying and/or subsequently. The invention also relates to corresponding multi-functional multi-substance compounds in solid form for use in washing and/or cleaning agents, the process for producing the multi-substance compounds and their use in washing and cleaning agents.
摘要翻译：本发明描述了一种水溶性的多组分化合物，为固体混合物，其可特别用作漂白和/或消毒剂含有吸附和/或结合的过氧化氢，和任选在原位形成每化合物的作用下，包含在共混物（K1）模块面积的固体碱金属硅酸盐（摩尔比的SiO 2 :M 2 O，其中M =碱金属）为0.8至10，和（K2）从类的在特定的水溶性无机和/或有机盐为H 2 O的H 2 O 2的结合和/或至少一种其它固体组分能。本发明的教导的特征在于，（K1）至少5重量％和播放（K2）的量在于在至少10的多燃料化合物重量％的比例 - 重量％的总和（K1）+ （K2） - ，另外，（K1）和（K2）的存在通过从微分散-均匀混合物的一般的水性制剂干燥生产的，并且该H 2 O 2在此干燥随后进入向上和/或在多燃料化合物。本发明是在固体形式用于洗涤剂和/或清洁剂，在制造多组分化合物和它们在洗涤剂中的使用和清洁剂的方法中的其它合适的多官能多组分化合物。

6. 发明申请

WO1995023763A1 SILICATE BUILDERS AND THEIR USE IN DETERGENTS AND WASHING AGENTS, AND MULTI-SUBSTANCE MIXTURES FOR USE IN THIS FIELD 审中-公开
标题翻译：硅质建设者和它们在洗涤剂和清洗剂而愈包含使用在这一领域
公开(公告)号：WO1995023763A1
公开(公告)日：1995-09-08
申请号：PCT/EP1995000605
申请日：1995-02-20
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , RÄHSE, Wilfried , FUES, Johann, Friedrich , PAATZ, Kathleen , STEIN, Norbert , BAUER, Volker , KOTTWITZ, Beatrix , JACOBS, Jochen , POETHKOW, Jörg
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： C01B33/32
CPC分类号： C11D11/02 , B01D1/18 , C01B33/325 , C11D3/08
摘要： The subject matter of the invention is alkali metal silicates in the modulus range (SiO2 to M2O molar ratio in which M = alkali metal) of 1 to 4 as a solid material which has been dried, by means of a hot gas flow, from an aqueous alkali metal silicate preparation sprayed in droplet form (primary dry material) but which can also be comminuted and/or compacted by the simultaneous and/or subsequent effect of mechanical force (secondary dry material). The teaching of the invention is characterized in that the primary dry material has apparent densities of less than 150 g/l and is produced by means of superheated steam as the hot gas flow. This primary dry material can be broken up and/or compacted in particular into the form of flakes (secondary dry material). The primary dry material and thus also the material which has possibly been comminuted or compacted is preferably in the form of superdried material having maximum water contents of approximately 15 wt %. The subject matter of the invention is further multi-substance mixtures, in particular from the field of detergents and washing agents, characterized in that they contain these superdried alkali metal silicates. Finally, the subject matter of the invention is the use of X-ray amorphous superdried alkali metal silicates as multi-purpose mixing components having a builder effect and a high absorption capacity for flowable auxiliary and valuable substances in mixtures in the field of solid detergents and washing agents.
摘要翻译：本发明涉及的模块面积的碱金属硅酸盐（摩尔比的SiO 2 :M 2 O，其中M =碱金属）为1〜4作为已经从以液滴喷洒干燥了的固体材料形成由热气体流（初次干燥）的装置中的碱金属硅酸盐的水性制剂，还通过同时可压碎的和机械力和/或压实的（次级干基料）/或后续的动作。本发明的教导的特征在于，具有低于150克/升的堆积密度的初级干燥材料并通过过热蒸汽的手段已经被制备为热气流。该初级干燥材料可以特别破碎碎片以形成和/或压实（二次干基料）。初级干燥材料并因此也任选粉碎或压缩材料优选作为具有至多约15重量％的水含量过干的材料。本发明进一步的多组分混合物，特别是从洗涤剂和清洁产品，其特征在于这样的内容的领域过干燥的碱金属硅酸盐。最后，本发明是利用X射线无定形过干的碱金属硅酸盐的作为具有助洗剂作用，在固体洗涤剂和清洁剂的面积的混合物高吸收能力用于可流动助剂和有用的材料的多官能混合物组分。

7. 发明申请

WO1994020187A1 IMPROVED DISTILLATIVE SEPARATION PROCESS BY STEAMING FOR MIXTURES OF MULTIPLE SUBSTANCES 审中-公开
标题翻译：改进方法蒸汽更多燃料混合物在蒸馏分离
公开(公告)号：WO1994020187A1
公开(公告)日：1994-09-15
申请号：PCT/EP1994000563
申请日：1994-02-25
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , RÄHSE, Wilfried , FUES, Johann, Friedrich , PAATZ, Kathleen , SCHECK, Hans , KOZMA, Jozsef , WIEDEMEYER, Rolf
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： B01D01/18
CPC分类号： C11B3/14 , B01D3/38 , C07B63/00
摘要： A process is disclosed for intensifying and/or accelerating the distillative separation of mixtures of multiple substances by using a steam flow (5, 7) which allows the steam-volatile parts of the substances to be removed more easily (steaming). The process is characterized in that the substances to be separated (4, 19, 1), which are fluid in processing conditions, are steamed in a finely pulverized form. Preferably, steam which is overheated at the working pressure is used in particularly at least partially as propellant gas for vaporizing the liquid phases to be purified. The substances to be processed are pulverized by means of this propellant gas in pulverizing nozzles for multiple substances. This process may have a wide range of applications, by simply adapting its parameters, in particular temperature and working pressure.

8. 发明申请

WO1994011486A1 PROCESS FOR THE EASIER PURIFICATION OF VALUABLE MATERIALS AND/OR THEIR MIXTURES IN THE FIELD OF WETTING, WASHING AND/OR CLEANING AGENTS AND RELATED SUBSTANCES 审中-公开
标题翻译：用于清洁便利上有价值的物质和/或再生混合从POWER，洗涤和/或清洗剂的方法技术领域和相关材料VALUE
公开(公告)号：WO1994011486A1
公开(公告)日：1994-05-26
申请号：PCT/EP1993003047
申请日：1993-11-02
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , RÄHSE, Wilfried , FUES, Johann, Friedrich , SCHMID, Karl-Heinz , PAATZ, Kathleen
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： C11D11/02
CPC分类号： C07C303/44 , C11D11/02 , C07C309/08
摘要： The invention relates to a process for improving the degree of purity and especially the quality of colour and odour in valuable materials and mixtures in the field of wetting, washing and/or cleaning agents. In the process, a substance containing impurities and especially water-vapour volatile impurities is treated in finely divided form with superheated steam in the region of normal pressure in which bleaching agents may be used together with the substance for colour enhancement. In a special embodiment, the invention relates to the use of the process for drying aqueous preparations of valuable materials and/or their mixtures in the field of wetting, washing and/or cleaning agents in the spray region and/or eddy layer with the addition of superheated steam as the drying gas for the simultaneous cleaning of a substance contaminated especially with water-vapour-volatile impurities. This cleaning can be combined with an oxidising or reducing bleach dissolved at the same time in the substance to obtain brightly coloured valuable materials or their mixtures. If desired, traces of ozone may be added to the superheated steam.

9. 发明申请

WO1995014519A1 PROCESS FOR PRODUCING ANHYDROUS POURABLE SUGAR TENSIDE POWDERS 审中-公开
标题翻译：法产水免费，自由流动的ZUCKERTENSIDPULVER
公开(公告)号：WO1995014519A1
公开(公告)日：1995-06-01
申请号：PCT/EP1994003855
申请日：1994-11-22
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , RÄHSE, Wilfried , PAATZ, Kathleen , BREITZKE, Willi , SEIPEL, Werner , TESMANN, Holger , SCHMID, Karl-Heinz , FABRY, Bernd
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： B01D01/18
CPC分类号： C11D11/0082 , A61K8/42 , A61K8/604 , A61Q11/00 , A61Q19/10 , B01F17/0085 , C07C233/18 , C07C233/20 , C11D1/146 , C11D1/525 , C11D1/662 , C11D1/835 , C11D1/86
摘要： Anhydrous pourable sugar tenside powders are obtained by the treatment of aqueous preparations containing (a1) alkyl and/or alkenyl oligoglycosides and/or (a2) fatty acid-N-alkylpolyhydroxyalkylamides with superheated steam at a temperature of 100-225 DEG C and removal of the dried product. The products thus obtained have excellent smell and taste characteristics and can be used in the production of surface active substances such as toothpastes and synthetic soaps.
摘要翻译：无水，自由流动的Zuckertensidpulver通过在范围100-225℃的过热蒸汽和在一定温度下处理含有含水制剂（A1）烷基和/或烯基低聚糖苷和/或（a2）脂肪酸N-烷基多羟基酰胺来获得干燥的材料被分离。该产品具有优良的感官品质和适于生产表面活性剂，特别是牙膏和合成洗涤剂皂。

10. 发明申请

WO1995002031A1 COATED ENZYME COMPOSITION FOR WASHING AND CLEANING PRODUCTS 审中-公开
标题翻译： COATED酶制剂用于洗涤和清洁剂
公开(公告)号：WO1995002031A1
公开(公告)日：1995-01-19
申请号：PCT/EP1994002079
申请日：1994-06-27
申请人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN , PAATZ, Kathleen , RÄHSE, Wilfried , PICHLER, Werner , KÜHNE, Norbert , UPADEK, Horst
发明人： HENKEL KOMMANDITGESELLSCHAFT AUF AKTIEN
IPC分类号： C11D03/386
CPC分类号： C12N9/98 , C11D3/38672 , C11D17/0039 , C12N11/04
摘要： In order to obtain dust-free enzyme granulates, a coating system is required which counteracts the destruction of the surface of the granulate when uniformly applied on an enzyme-containing granulate, increases the storage stability of the enzyme by protectively coating the whole granulate, allows any existent natural coloration of the uncoated enzyme granulate to be masked and eliminates any disturbing odours of the uncoated granulate. For that purpose, an enzyme granulate is prepared which comprises enzyme and an inorganic and/or organic excipient, as well as a uniform outer pigment-containing coating layer made of a coating system which contains 30 to 50 % by weight finely powdered inorganic pigment, 45 to 60 % by weight of an alcohol solid at room temperature and with a fusion point in the 45 DEG C to 65 DEG C range, up to 15 % by weight of an emulsifier for the alcohol, up to 5 % by weight of a dispersing agent for the pigment and up to 3 % by weight water.
摘要翻译：无尘酶颗粒的包装系统必须要开发的，与稳定的工作抵消上的颗粒的表层破坏的颗粒含酶，酶的贮藏稳定性提高了整个颗粒的保护涂层，未涂覆的酶颗粒的任何固有颜色的覆盖允许的和可能干扰气味无涂层颗粒消除。这是通过提供含酶和无机和/或有机载体物质和含有.- 30％（重量）的涂层体系的均匀外含颜料的涂层的酶颗粒基本上达到〜50％（重量）细碎的无机颜料，45重量％至 60重量固体在室温下的％，具有范围从45℃至65℃的熔点，高达15重量％的乳化剂为醇，至多5重量％的分散剂用于颜料和至多醇 3包括重量％的水。

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