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1. 发明授权

US5756595A Production of polysuccinimide in cyclic carbonate solvent 失效
标题翻译：在环状碳酸酯溶剂中生产聚琥珀酰亚胺
公开(公告)号：US5756595A
公开(公告)日：1998-05-26
申请号：US808467
申请日：1997-03-03
申请人： Grigory Ya Mazo , Daniel A. Batzel , James F. Kneller , Jacob Mazo
发明人： Grigory Ya Mazo , Daniel A. Batzel , James F. Kneller , Jacob Mazo
IPC分类号： C08G73/10
CPC分类号： C08G73/1092
摘要： A method for the preparation of a desired molecular weight polysuccinimide by the catalytic polymerization of aspartic acid in the presence of a cyclic carbonate solvent. Polysuccinimide of relatively high weight average molecular weight and high purity can be produced in relatively high yields while employing a relatively low catalyst loading.
摘要翻译：一种在环状碳酸酯溶剂存在下通过天冬氨酸的催化聚合制备所需分子量聚琥珀酰亚胺的方法。相对较高的重均分子量和高纯度的聚琥珀酰亚胺可以以较高的产率生产，同时采用较低的催化剂负载量。

2. 发明授权

US5939518A Polyaspartate (salt) by polymerizing aspartic acid and hydrolyzing 失效
标题翻译：聚天冬氨酸（盐）通过天冬氨酸的聚合和水解
公开(公告)号：US5939518A
公开(公告)日：1999-08-17
申请号：US84822
申请日：1998-05-26
申请人： Grigory Ya. Mazo , Daniel A. Batzel , James F. Kneller , Jacob Mazo
发明人： Grigory Ya. Mazo , Daniel A. Batzel , James F. Kneller , Jacob Mazo
IPC分类号： C08G73/10
CPC分类号： C08G73/1092
摘要： A method for the preparation of a desired molecular weight polysuccinimide by the catalytic polymerization of aspartic acid in the presence of a cyclic carbonate solvent. Polysuccinimide of relatively high weight average molecular weight and high purity can be produced in relatively high yields while employing a relatively low catalyst loading.
摘要翻译：一种在环状碳酸酯溶剂存在下通过天冬氨酸的催化聚合制备所需分子量聚琥珀酰亚胺的方法。相对较高的重均分子量和高纯度的聚琥珀酰亚胺可以以较高的产率生产，同时采用较低的催化剂负载量。

3. 发明授权

US06399715B2 Solution polymerizing aspartic acid and monomer to form succinimide copolymer 失效
标题翻译：溶液聚合天冬氨酸和单体形成琥珀酰亚胺共聚物
公开(公告)号：US06399715B2
公开(公告)日：2002-06-04
申请号：US09799230
申请日：2001-03-05
申请人： Grigory Ya. Mazo , Robert J. Ross , James F. Kneller , Jacob Mazo
发明人： Grigory Ya. Mazo , Robert J. Ross , James F. Kneller , Jacob Mazo
IPC分类号： C08G7310
CPC分类号： C08G73/1092
摘要： A method for the preparation of a succinimide copolymer by the catalytic co-polymerization of aspartic acid with a selected polyfunctional monomer in the presence of a cyclic carbonate solvent. Succinimide copolymers of relatively high weight average molecular weight and high purity can be produced in relatively high yields while employing a relatively low catalyst loading.
摘要翻译：一种通过在环状碳酸酯溶剂存在下天冬氨酸与所选择的多官能单体的催化共聚合制备琥珀酰亚胺共聚物的方法。相对高的重均分子量和高纯度的琥珀酰亚胺共聚物可以以相当高的产率生产，同时采用相对较低的催化剂负载量。

4. 发明授权

US06197897B1 Production of succinimide copolymers in cyclic carbonate solvent 失效
标题翻译：在环状碳酸酯溶剂中生产琥珀酰亚胺共聚物
公开(公告)号：US06197897B1
公开(公告)日：2001-03-06
申请号：US09357682
申请日：1999-07-20
申请人： Grigory Ya. Mazo , Robert J. Ross , James F. Kneller , Jacob Mazo
发明人： Grigory Ya. Mazo , Robert J. Ross , James F. Kneller , Jacob Mazo
IPC分类号： C08G7310
CPC分类号： C08G73/1092
摘要： A method for the preparation of a succinimide copolymer by the catalytic co-polymerization of aspartic acid with a selected polyfunctional monomer in the presence of a cyclic carbonate solvent. Succinimide copolymers of relatively high weight average molecular weight and high purity can be produced in relatively high yields while employing a relatively low catalyst loading.
摘要翻译：一种通过在环状碳酸酯溶剂存在下天冬氨酸与所选择的多官能单体的催化共聚合制备琥珀酰亚胺共聚物的方法。相对高的重均分子量和高纯度的琥珀酰亚胺共聚物可以以相当高的产率生产，同时采用相对较低的催化剂负载量。

5. 发明授权

US5939517A Production of succinimide copolymers in cyclic carbonate solvent 失效
标题翻译：在环状碳酸酯溶剂中生产琥珀酰亚胺共聚物
公开(公告)号：US5939517A
公开(公告)日：1999-08-17
申请号：US6255
申请日：1998-01-13
申请人： Grigory Ya. Mazo , Robert J. Ross , James F. Kneller , Jacob Mazo
发明人： Grigory Ya. Mazo , Robert J. Ross , James F. Kneller , Jacob Mazo
IPC分类号： C08G73/10 , C08G73/14 , C08G73/16
CPC分类号： C08G73/1092
摘要： A method for the preparation of a succinimide copolymer by the catalytic co-polymerization of aspartic acid with a selected polyfunctional monomer in the presence of a cyclic carbonate solvent. Succinimide copolymers of relatively high weight average molecular weight and high purity can be produced in relatively high yields while employing a relatively low catalyst loading.
摘要翻译：一种通过在环状碳酸酯溶剂存在下天冬氨酸与所选择的多官能单体的催化共聚合制备琥珀酰亚胺共聚物的方法。相对高的重均分子量和高纯度的琥珀酰亚胺共聚物可以以相当高的产率生产，同时采用相对较低的催化剂负载量。

6. 发明授权

US5508434A Production of a polysuccinimide and derivatives thereof in the presence of a sulfur-containing dehydrating agent 失效
标题翻译：在含硫脱水剂的存在下制备聚琥珀酰亚胺及其衍生物
公开(公告)号：US5508434A
公开(公告)日：1996-04-16
申请号：US313770
申请日：1994-09-28
申请人： Daniel A. Batzel , James F. Kneller , Abdul R. Y. Meah
发明人： Daniel A. Batzel , James F. Kneller , Abdul R. Y. Meah
IPC分类号： C08G69/10 , C08G73/10 , C07D207/40 , C07D207/325 , C07D403/06
CPC分类号： C08G73/1092 , C08G69/10
摘要： Polysuccinimide of varying molecular weight has been prepared by heat polymerization of aspartic acid in the presence of a sulfur-containing dehydrating agent employing a variety of reaction mixtures and reaction conditions. Sulfur trioxide and heat decomposable sulfur trioxide precursor dehydrating agents are preferred for this purpose. The presence of an acid scavenger within the reaction mixture is desirable and leads to a relatively higher molecular weight polysuccinimide, while the absence of an acid scavenger results in a relatively lower molecular weight polysuccinimide.
摘要翻译：通过使用各种反应混合物和反应条件的含硫脱水剂的存在下天冬氨酸的热聚合制备了不同分子量的聚琥珀酰亚胺。为此目的，优选三氧化硫和可热分解的三氧化硫前体脱水剂。反应混合物中存在酸清除剂是合乎需要的，并导致相对较高分子量的聚琥珀酰亚胺，而不存在酸清除剂导致相对较低分子量的聚琥珀酰亚胺。

7. 发明授权

US5478919A Aspartic acid copolymers and their preparation 失效
标题翻译：天冬氨酸共聚物及其制备方法
公开(公告)号：US5478919A
公开(公告)日：1995-12-26
申请号：US283268
申请日：1994-07-29
申请人： Larry P. Koskan , James F. Kneller , Daniel A. Batzel
发明人： Larry P. Koskan , James F. Kneller , Daniel A. Batzel
IPC分类号： C08G69/10 , C08G73/10 , C08G69/48
CPC分类号： C08G69/10 , C08G73/1092
摘要： Aspartic acid precursors such as mono and diammonium maleate, maleamic acid, ammonium maleamate, ammonium malate and mixtures of these and other precursors are copolycondensed thermally with a variety of mono, di and multifunctional monomers containing amino, hydroxyl and carboxyl functional groups. The resulting condensation copolymers and terpolymers contain succinimide units derived from aspartic acid precursors, condensed with other functional group monomers usually though amide and ester linkages. Hydrolysis of the polysuccinimide copolymers and terpolymers with alkali, alkaline earth and ammonium hydroxide produces aspartic acid copolymer and terpolymer salts.
摘要翻译：天冬氨酸前体如马来酸单和二铵，马来酰胺酸，马来酸铵，马来酸铵，这些和其它前体的混合物与含有氨基，羟基和羧基官能团的各种单，二和多官能单体共缩聚。所得的缩合共聚物和三元共聚物含有衍生自天冬氨酸前体的琥珀酰亚胺单元，其通常通过酰胺和酯键与其它官能团单体缩合。聚琥珀酰亚胺共聚物和三元共聚物与碱金属，碱土金属和氢氧化铵的水解产生天冬氨酸共聚物和三元共聚物盐。

8. 再颁专利

USRE36234E Aspartic acid copolymers and their preparation 失效
标题翻译：天冬氨酸共聚物及其制备方法
公开(公告)号：USRE36234E
公开(公告)日：1999-06-22
申请号：US995444
申请日：1997-12-22
申请人： Larry P. Koskan , James F. Kneller , Daniel A. Batzel
发明人： Larry P. Koskan , James F. Kneller , Daniel A. Batzel
IPC分类号： C08G69/10 , C08G73/10 , C08G69/48
CPC分类号： C08G69/10 , C08G73/1092
摘要： Aspartic acid precursors such as mono and diammonium maleate, maleamic acid, ammonium maleamate, ammonium malate and mixtures of these and other precursors are copolycondensed thermally with a variety of mono, di and multifunctional monomers containing amino, hydroxyl and carboxyl functional groups. The resulting condensation copolymers and terpolymers contain succinimide units derived from aspartic acid precursors, condensed with other functional group monomers usually .�.though.!. .Iadd.through .Iaddend.amide and ester linkages. Hydrolysis of the polysuccinimide copolymers and terpolymers with alkali, alkaline earth and ammonium hydroxide produces aspartic acid copolymer and terpolymer salts.
摘要翻译：天冬氨酸前体如马来酸单和二铵，马来酰胺酸，马来酸铵，马来酸铵，这些和其它前体的混合物与含有氨基，羟基和羧基官能团的各种单，二和多官能单体共缩聚。所得的缩合共聚物和三元共聚物含有衍生自天冬氨酸前体的琥珀酰亚胺单元，其与通常通过酰胺和酯键的其它官能团单体缩合。聚琥珀酰亚胺共聚物和三元共聚物与碱金属，碱土金属和氢氧化铵的水解产生天冬氨酸共聚物和三元共聚物盐。

9. 发明授权

US5085794A Oligomer containing phosphinate compositions and their method of manufacture 失效
标题翻译：含有次膦酸盐组合物的低聚物及其制备方法
公开(公告)号：US5085794A
公开(公告)日：1992-02-04
申请号：US514444
申请日：1990-04-25
申请人： James F. Kneller , Vytas Narutis , Barbara E. Fair , Donald A. Johnson
发明人： James F. Kneller , Vytas Narutis , Barbara E. Fair , Donald A. Johnson
IPC分类号： C02F5/14
CPC分类号： C02F5/145 , C02F5/14
摘要： A phosphinate containing composition which has as its major ingredient more than 32 mole percent of a phosphinicosuccinic acid oligomer having the probable structural formula: ##STR1## M is H, Na, K, NH.sub.4, or mixtures thereof; and m and n are either 0 or a small whole number with the proviso that either m or n is a small whole number and the sum of m plus n is greater than 2.
摘要翻译：含有次膦酸盐的组合物，其主要成分为具有32摩尔％以下具有可能结构式的次膦酸琥珀酸低聚物：H，Na，K，NH 4或其混合物; 并且m和n为0或小整数，条件是m或n为小整数，m + n的和大于2。

10. 发明授权

US5018577A Phosphinate inhibitor for scale squeeze applications 失效
标题翻译：用于鳞片挤压应用的磷酸盐抑制剂
公开(公告)号：US5018577A
公开(公告)日：1991-05-28
申请号：US561854
申请日：1990-08-02
申请人： Jerry E. Pardue , James F. Kneller
发明人： Jerry E. Pardue , James F. Kneller
IPC分类号： C02F5/14 , C07F9/30 , C09K8/528
CPC分类号： C09K8/528 , C02F5/14 , C07F9/301 , Y10S507/927
摘要： A squeeze treatment for preventing scale utilizes as the scale inhibitor a predominantly phosphinate containing composition comprising:______________________________________ Mole Percent - Ingredients Less Than ______________________________________ A. Monosodium phosphinicobis - 22 (succinic acid) B. Monosodium phosphinico- 26 succinic acid C. Sodium phosphonosuccinic acid 12 D. Sodium phosphate 5 E. Sodium phosphite 6 F. Sodium hypophosphite, and 6 G. A phosphinicosuccinic acid oligomer having the probable structural formula: ##STR1## ______________________________________ wherein G exceeds 25 mole percent, M is H, Na, K, NH.sub.4, amine salts and mixtures thereof and m and n are either 0 or a small whole number with the proviso that either m or n is a small whole number and the sum of m plus n is greater than 2.
摘要翻译：用于防止垢的挤压处理用作阻垢剂，主要是含磷酸盐的组合物，其包含： - 摩尔百分数 - 小于-A的成分。次膦酸二钠22 - （琥珀酸）-B。次膦酸二钠26-琥珀酸-C。次膦酸琥珀酸钠12-D。磷酸钠5 -E。亚磷酸钠6 -F。次磷酸钠和6 -G。具有可能结构式的次膦酸琥珀酸低聚物：其中G超过25摩尔％，M为H，Na，K，NH 4，胺盐及其混合物，m和n为0或小整数数字，条件是m或n是小整数，m + n的和大于2。

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