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1. 发明授权

US06399715B2 Solution polymerizing aspartic acid and monomer to form succinimide copolymer 失效
标题翻译：溶液聚合天冬氨酸和单体形成琥珀酰亚胺共聚物
公开(公告)号：US06399715B2
公开(公告)日：2002-06-04
申请号：US09799230
申请日：2001-03-05
申请人： Grigory Ya. Mazo , Robert J. Ross , James F. Kneller , Jacob Mazo
发明人： Grigory Ya. Mazo , Robert J. Ross , James F. Kneller , Jacob Mazo
IPC分类号： C08G7310
CPC分类号： C08G73/1092
摘要： A method for the preparation of a succinimide copolymer by the catalytic co-polymerization of aspartic acid with a selected polyfunctional monomer in the presence of a cyclic carbonate solvent. Succinimide copolymers of relatively high weight average molecular weight and high purity can be produced in relatively high yields while employing a relatively low catalyst loading.
摘要翻译：一种通过在环状碳酸酯溶剂存在下天冬氨酸与所选择的多官能单体的催化共聚合制备琥珀酰亚胺共聚物的方法。相对高的重均分子量和高纯度的琥珀酰亚胺共聚物可以以相当高的产率生产，同时采用相对较低的催化剂负载量。

2. 发明授权

US4923634A Cooling water corrosion inhibition method 失效
标题翻译：冷却水腐蚀抑制方法
公开(公告)号：US4923634A
公开(公告)日：1990-05-08
申请号：US155393
申请日：1988-02-12
申请人： John E. Hoots , Donald A. Johnson , Dodd W. Fong , James F. Kneller
发明人： John E. Hoots , Donald A. Johnson , Dodd W. Fong , James F. Kneller
IPC分类号： C23F11/08
CPC分类号： C23F11/08
摘要： A method for inhibiting corrosion in industrial cooling waters which contain hardness and a pH of at least 6.5, by dosing the water with a composition which comprises a water-soluble inorganic phosphate capable of inhibiting corrosion in an aqueous alkaline environment and a hydrocarbon polymer containing an N-substituted acrylamide polymers with an amide structure as follows: ##STR1## where R.sub.2 is hydrogen or methyl, where R.sub.1 is a hydrogen or an alkyl and R is alkylene or phenylene, and X is sulfonate, (poly)hydroxyl, (poly)carboxyl or carbonyl, and combinations thereof; or containing derivatized maleic anhydride homo-, co- and terpolymers having N-substituted maleamic acid units, N-substituted maleimide units and maleic acid (and salts) units having a structure as follows: ##STR2## where R.sub.1, R.sub.2 and R.sub.3 are each independently chosen from the group consisting of hydrogen, hydroxyl, carboxyalkyl, carboxyamide, phenyl, substituted phenyl, linear or branched alkyl of from one to ten carbon atoms,and substituted alkyl of from one to ten carbon atoms, where the substituent is phosphonic acid; phosphinic acid; phosphate ester; sulfonic acid; sulfate ester, carboxyamide, (poly)carboxy and (poly)hydroxy, alkoxy and carboxylate ester groups; and combinations thereof.
摘要翻译：一种通过用含有能够在碱性水溶液中抑制腐蚀的水溶性无机磷酸盐的组合物给予水，并且含有至少为6.5的烃聚合物的含有硬度和pH至少为6.5的工业冷却水中的腐蚀的方法具有酰胺结构的N-取代丙烯酰胺聚合物如下：其中R 2是氢或甲基，其中R 1是氢或烷基，R是亚烷基或亚苯基，X是磺酸根，（多）羟基，（聚）羧基或羰基，及其组合; 或含有具有N-取代的马来酰胺酸单元，N-取代的马来酰亚胺单元和具有如下结构的马来酸（和盐）单元的衍生化马来酸酐均聚物，共聚物和三元共聚物：其中R 1，R 2和R 3各自为独立地选自氢，羟基，羧基烷基，羧基酰胺，苯基，取代的苯基，1至10个碳原子的直链或支链烷基和1至10个碳原子的取代烷基，其中取代基是膦酸; 次膦酸磷酸酯; 磺酸硫酸酯，羧酰胺，（多）羧基和（多）羟基，烷氧基和羧酸酯基团; 及其组合。

3. 发明授权

US4913824A Anionic polymers containing N-vinyl-pyrrolidone or other vinyl amides as scale inhibitors for preventing or reducing calcium phosphate and other scales 失效
标题翻译：含有N-乙烯基 - 吡咯烷酮或其它乙烯基酰胺的阴离子聚合物作为防止或减少磷酸钙和其它垢的阻垢剂
公开(公告)号：US4913824A
公开(公告)日：1990-04-03
申请号：US253355
申请日：1988-09-29
申请人： James F. Kneller
发明人： James F. Kneller
IPC分类号： C02F5/12
CPC分类号： C02F5/12
摘要： A method of inhibiting scale, generally and specifically and preferably calcium phosphate and calcium carbonate scale, which is found on metal surfaces in contact with industrial cooling waters, boiler waters, oil well drilling waters, and evaporated sea water, which comprises treating the water present in such systems with a few ppm of a water-soluble anionic co- or terpolymer of N-vinyl-2-pyrrolidone (NVP) or vinyl amide. The preferred anionic comonomers are either acrylic or methacrylic acid.
摘要翻译：一种在工业冷却水，锅炉水，油井钻井水和蒸发的海水接触的金属表面上发现的一般和特别地，特别地，优选磷酸钙和碳酸钙垢的垢的方法，其包括处理存在的水在具有几ppm的N-乙烯基-2-吡咯烷酮（NVP）或乙烯基酰胺的水溶性阴离子共聚物或三元共聚物的这种体系中。优选的阴离子共聚单体是丙烯酸或甲基丙烯酸。

4. 发明授权

US4711726A Carboxylate N-vinylamide copolymers for internal scale control and passivation in high pressure boiler systems 失效
标题翻译：羧酸盐N-乙烯基酰胺共聚物用于高压锅炉系统中的内部尺度控制和钝化
公开(公告)号：US4711726A
公开(公告)日：1987-12-08
申请号：US947060
申请日：1986-12-29
申请人： Claudia C. Pierce , Robert S. Robinson , James F. Kneller
发明人： Claudia C. Pierce , Robert S. Robinson , James F. Kneller
IPC分类号： C02F5/12 , C23F11/173
CPC分类号： C23F11/173 , C02F5/12
摘要： Copolymers of acrylic or methacrylic acid with certain N-vinyl amides are excellent treating agents to prevent scale and corrosion caused by boiler waters in contact with heat transfer surfaces.
摘要翻译：丙烯酸或甲基丙烯酸与某些N-乙烯基酰胺的共聚物是防止与传热表面接触的锅炉水引起的垢和腐蚀的优良处理剂。

5. 发明授权

US4604211A Acrylic acid-sodium vinylsulfonate-vinyl acetate terpolymer and use thereof as a dispersant 失效
标题翻译：丙烯酸 - 乙烯基磺酸钠 - 乙酸乙烯酯三元共聚物及其作为分散剂的用途
公开(公告)号：US4604211A
公开(公告)日：1986-08-05
申请号：US696227
申请日：1985-01-29
申请人： James F. Kneller , John R. Hurlock
发明人： James F. Kneller , John R. Hurlock
IPC分类号： C02F5/10 , C23F11/173
CPC分类号： C23F11/173 , C02F5/10
摘要： Terpolymers of acrylic acid, sodium vinylsulfonate and vinyl acetate are disclosed. These materials are effective dispersants for industrial water systems.
摘要翻译：公开了丙烯酸，乙烯基磺酸钠和乙酸乙烯酯的三元共聚物。这些材料是工业用水系统的有效分散剂。

6. 发明授权

US5508434A Production of a polysuccinimide and derivatives thereof in the presence of a sulfur-containing dehydrating agent 失效
标题翻译：在含硫脱水剂的存在下制备聚琥珀酰亚胺及其衍生物
公开(公告)号：US5508434A
公开(公告)日：1996-04-16
申请号：US313770
申请日：1994-09-28
申请人： Daniel A. Batzel , James F. Kneller , Abdul R. Y. Meah
发明人： Daniel A. Batzel , James F. Kneller , Abdul R. Y. Meah
IPC分类号： C08G69/10 , C08G73/10 , C07D207/40 , C07D207/325 , C07D403/06
CPC分类号： C08G73/1092 , C08G69/10
摘要： Polysuccinimide of varying molecular weight has been prepared by heat polymerization of aspartic acid in the presence of a sulfur-containing dehydrating agent employing a variety of reaction mixtures and reaction conditions. Sulfur trioxide and heat decomposable sulfur trioxide precursor dehydrating agents are preferred for this purpose. The presence of an acid scavenger within the reaction mixture is desirable and leads to a relatively higher molecular weight polysuccinimide, while the absence of an acid scavenger results in a relatively lower molecular weight polysuccinimide.
摘要翻译：通过使用各种反应混合物和反应条件的含硫脱水剂的存在下天冬氨酸的热聚合制备了不同分子量的聚琥珀酰亚胺。为此目的，优选三氧化硫和可热分解的三氧化硫前体脱水剂。反应混合物中存在酸清除剂是合乎需要的，并导致相对较高分子量的聚琥珀酰亚胺，而不存在酸清除剂导致相对较低分子量的聚琥珀酰亚胺。

7. 发明授权

US5085794A Oligomer containing phosphinate compositions and their method of manufacture 失效
标题翻译：含有次膦酸盐组合物的低聚物及其制备方法
公开(公告)号：US5085794A
公开(公告)日：1992-02-04
申请号：US514444
申请日：1990-04-25
申请人： James F. Kneller , Vytas Narutis , Barbara E. Fair , Donald A. Johnson
发明人： James F. Kneller , Vytas Narutis , Barbara E. Fair , Donald A. Johnson
IPC分类号： C02F5/14
CPC分类号： C02F5/145 , C02F5/14
摘要： A phosphinate containing composition which has as its major ingredient more than 32 mole percent of a phosphinicosuccinic acid oligomer having the probable structural formula: ##STR1## M is H, Na, K, NH.sub.4, or mixtures thereof; and m and n are either 0 or a small whole number with the proviso that either m or n is a small whole number and the sum of m plus n is greater than 2.
摘要翻译：含有次膦酸盐的组合物，其主要成分为具有32摩尔％以下具有可能结构式的次膦酸琥珀酸低聚物：H，Na，K，NH 4或其混合物; 并且m和n为0或小整数，条件是m或n为小整数，m + n的和大于2。

8. 发明授权

US5018577A Phosphinate inhibitor for scale squeeze applications 失效
标题翻译：用于鳞片挤压应用的磷酸盐抑制剂
公开(公告)号：US5018577A
公开(公告)日：1991-05-28
申请号：US561854
申请日：1990-08-02
申请人： Jerry E. Pardue , James F. Kneller
发明人： Jerry E. Pardue , James F. Kneller
IPC分类号： C02F5/14 , C07F9/30 , C09K8/528
CPC分类号： C09K8/528 , C02F5/14 , C07F9/301 , Y10S507/927
摘要： A squeeze treatment for preventing scale utilizes as the scale inhibitor a predominantly phosphinate containing composition comprising:______________________________________ Mole Percent - Ingredients Less Than ______________________________________ A. Monosodium phosphinicobis - 22 (succinic acid) B. Monosodium phosphinico- 26 succinic acid C. Sodium phosphonosuccinic acid 12 D. Sodium phosphate 5 E. Sodium phosphite 6 F. Sodium hypophosphite, and 6 G. A phosphinicosuccinic acid oligomer having the probable structural formula: ##STR1## ______________________________________ wherein G exceeds 25 mole percent, M is H, Na, K, NH.sub.4, amine salts and mixtures thereof and m and n are either 0 or a small whole number with the proviso that either m or n is a small whole number and the sum of m plus n is greater than 2.
摘要翻译：用于防止垢的挤压处理用作阻垢剂，主要是含磷酸盐的组合物，其包含： - 摩尔百分数 - 小于-A的成分。次膦酸二钠22 - （琥珀酸）-B。次膦酸二钠26-琥珀酸-C。次膦酸琥珀酸钠12-D。磷酸钠5 -E。亚磷酸钠6 -F。次磷酸钠和6 -G。具有可能结构式的次膦酸琥珀酸低聚物：其中G超过25摩尔％，M为H，Na，K，NH 4，胺盐及其混合物，m和n为0或小整数数字，条件是m或n是小整数，m + n的和大于2。

9. 发明授权

US5939518A Polyaspartate (salt) by polymerizing aspartic acid and hydrolyzing 失效
标题翻译：聚天冬氨酸（盐）通过天冬氨酸的聚合和水解
公开(公告)号：US5939518A
公开(公告)日：1999-08-17
申请号：US84822
申请日：1998-05-26
申请人： Grigory Ya. Mazo , Daniel A. Batzel , James F. Kneller , Jacob Mazo
发明人： Grigory Ya. Mazo , Daniel A. Batzel , James F. Kneller , Jacob Mazo
IPC分类号： C08G73/10
CPC分类号： C08G73/1092
摘要： A method for the preparation of a desired molecular weight polysuccinimide by the catalytic polymerization of aspartic acid in the presence of a cyclic carbonate solvent. Polysuccinimide of relatively high weight average molecular weight and high purity can be produced in relatively high yields while employing a relatively low catalyst loading.
摘要翻译：一种在环状碳酸酯溶剂存在下通过天冬氨酸的催化聚合制备所需分子量聚琥珀酰亚胺的方法。相对较高的重均分子量和高纯度的聚琥珀酰亚胺可以以较高的产率生产，同时采用较低的催化剂负载量。

10. 再颁专利

USRE36234E Aspartic acid copolymers and their preparation 失效
标题翻译：天冬氨酸共聚物及其制备方法
公开(公告)号：USRE36234E
公开(公告)日：1999-06-22
申请号：US995444
申请日：1997-12-22
申请人： Larry P. Koskan , James F. Kneller , Daniel A. Batzel
发明人： Larry P. Koskan , James F. Kneller , Daniel A. Batzel
IPC分类号： C08G69/10 , C08G73/10 , C08G69/48
CPC分类号： C08G69/10 , C08G73/1092
摘要： Aspartic acid precursors such as mono and diammonium maleate, maleamic acid, ammonium maleamate, ammonium malate and mixtures of these and other precursors are copolycondensed thermally with a variety of mono, di and multifunctional monomers containing amino, hydroxyl and carboxyl functional groups. The resulting condensation copolymers and terpolymers contain succinimide units derived from aspartic acid precursors, condensed with other functional group monomers usually .�.though.!. .Iadd.through .Iaddend.amide and ester linkages. Hydrolysis of the polysuccinimide copolymers and terpolymers with alkali, alkaline earth and ammonium hydroxide produces aspartic acid copolymer and terpolymer salts.
摘要翻译：天冬氨酸前体如马来酸单和二铵，马来酰胺酸，马来酸铵，马来酸铵，这些和其它前体的混合物与含有氨基，羟基和羧基官能团的各种单，二和多官能单体共缩聚。所得的缩合共聚物和三元共聚物含有衍生自天冬氨酸前体的琥珀酰亚胺单元，其与通常通过酰胺和酯键的其它官能团单体缩合。聚琥珀酰亚胺共聚物和三元共聚物与碱金属，碱土金属和氢氧化铵的水解产生天冬氨酸共聚物和三元共聚物盐。

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