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1. 发明授权

US5252309A Azine synthesis in the absence of CO.sub.2 失效
标题翻译：在不存在二氧化碳的情况下合成Azine
公开(公告)号：US5252309A
公开(公告)日：1993-10-12
申请号：US897830
申请日：1992-06-12
申请人： Gerard Krempf , Bertrand Collier , Pierre Tellier , Jean-Pierre Schirmann
发明人： Gerard Krempf , Bertrand Collier , Pierre Tellier , Jean-Pierre Schirmann
IPC分类号： C07B61/00 , C07C249/00 , C07C249/16 , C07C251/88 , C01B21/16 , C07C241/00 , C07C241/02
CPC分类号： C07C249/00 , Y02P20/582
摘要： Azines, well suited for hydrolysis into hydrazine, are prepared in high yields by reacting ammonia, aqueous hydrogen peroxide and a carbonyl compound reactant in the presence of a catalytically effective amount of a catalyst medium therefor, i.e., an aqueous solution of ammonium acetate and acetamide or of acetamide and acetic acid, but in the absence of CO.sub.2.
摘要翻译：通过在催化有效量的催化剂介质，即乙酸铵和乙酰胺的水溶液存在下，使氨，过氧化氢水溶液和羰基化合物反应物反应，以高产率制备非常适合水解成肼的氮杂环丁烷或乙酰胺和乙酸，但在不存在CO 2的情况下。

2. 发明授权

US5393508A Vaporization of solutions of hydrazine hydrate 失效
标题翻译：水合肼溶液的蒸发
公开(公告)号：US5393508A
公开(公告)日：1995-02-28
申请号：US118775
申请日：1993-09-10
申请人： Gerard Krempf , Bertrand Collier , Pierre Tellier , Jean-Pierre Pleuvry
发明人： Gerard Krempf , Bertrand Collier , Pierre Tellier , Jean-Pierre Pleuvry
IPC分类号： C01B21/16 , F28F21/08
CPC分类号： F28F21/082 , C01B21/16 , Y10S203/06
摘要： Solutions of hydrazine hydrate are vaporized, without any concomitant decomposition thereof, by heating such solutions, in the liquid phase, under conditions as to effect the decompression or volatilization thereof; this process is particularly applicable for the vaporization of that hydrazine hydrate solution contained in the reboiler of a column wherein the hydrolysis of an azine R.sub.1 R.sub.2 C.dbd.N-N.dbd.CR.sub.1 R.sub.2 is carried out, with recovery of hydrazine hydrate at the base of the column and of a ketone, R.sub.1 R.sub.2 C.dbd.O, at the column head.
摘要翻译：通过在液相中加热这些溶液，在其减压或挥发的条件下，将水合肼溶液蒸发而不伴随其分解; 该方法特别适用于在塔的再沸器中蒸发含水合肼的水合物溶液，其中进行吖嗪R1R2C = NN = CR1R2is的水解，同时回收塔底部的水合肼和酮， R1R2C = O，在柱头。

3. 发明申请

US20110021849A1 Process For The Preparation of Fluorinated Compounds 有权
标题翻译：氟化合物的制备方法
公开(公告)号：US20110021849A1
公开(公告)日：2011-01-27
申请号：US12842737
申请日：2010-07-23
申请人： Karine Avril , Bertrand Collier
发明人： Karine Avril , Bertrand Collier
IPC分类号： C07C21/18 , C07C17/38 , C07C17/383
CPC分类号： C07C21/18 , C07C17/25 , C07C17/354 , C07C17/383 , C07C19/08
摘要： A subject-matter of the invention is a process for the preparation of 2,3,3,3-tetrafluoro-1-propene comprising the following stages: (i) hydrogenation of hexafluoropropylene to give 1,1,1,2,3,3-hexafluoropropane; (ii) dehydrofluorination of the 1,1,1,2,3,3-hexafluoropropane obtained in the preceding stage to give 1,2,3,3,3-pentafluoro-1-propene; (iii) hydrogenation of the 1,2,3,3,3-pentafluoro-1-propene obtained in the preceding stage to give 1,1,1,2,3-pentafluoropropane; (iv) purification of the 1,1,1,2,3-pentafluoropropane obtained in the preceding stage; and (v) dehydrofluorination of the 1,1,1,2,3-pentafluoropropane obtained in the preceding stage to give 2,3,3,3-tetrafluoro-1-propene; and (vi) purification of the 2,3,3,3-tetrafluoro-1-propene of the preceding stage.
摘要翻译：本发明的主题是制备2,3,3,3-四氟-1-丙烯的方法，包括以下步骤：（i）六氟丙烯的氢化，得到1,1,1,2,3， 3-六氟丙烷; （ii）前段得到的1,1,1,2,3,3-六氟丙烷的脱氟化氢，得到1,2,3,3,3-五氟-1-丙烯; （iii）在前一阶段获得的1,2,3,3,3-五氟-1-丙烯的氢化，得到1,1,1,2,3-五氟丙烷; （iv）前一阶段获得的1,1,1,2,3-五氟丙烷的纯化; 和（v）前一阶段获得的1,1,1,2,3-五氟丙烷的脱氟化氢，得到2,3,3,3-四氟-1-丙烯; 和（vi）前一阶段的2,3,3,3-四氟-1-丙烯的纯化。

4. 发明授权

US09346723B2 Method for producing 2,3,3,3-tetrafluoropropene 有权
标题翻译：制备2,3,3,3-四氟丙烯的方法
公开(公告)号：US09346723B2
公开(公告)日：2016-05-24
申请号：US14376190
申请日：2013-01-11
申请人： Dominique Deur-Bert , Bertrand Collier , Laurent Wendlinger
发明人： Dominique Deur-Bert , Bertrand Collier , Laurent Wendlinger
IPC分类号： C07C17/20 , C07C17/25 , C07C17/38 , C07C17/383 , F25J1/00
CPC分类号： C07C17/20 , C07C17/206 , C07C17/25 , C07C17/38 , C07C17/383 , F25J1/0022 , F25J3/04412 , C07C21/18
摘要： The invention concerns a method for producing 2,3,3,3-tetrafluoropropene comprising: a fluoridation reaction of a halopropane and/or halopropene into 2,3,3,3-tetrafluoropropene by means of hydrogen fluoride; the recovery of a gas stream resulting from the reaction; the cooling and partial condensation of the gas stream resulting from the reaction into a partially condensed stream; the separation of the partially condensed stream into a gas fraction and a liquid fraction; the compression of the gas fraction into a compressed gas fraction; the compression of the liquid fraction into a compressed liquid fraction; the distillation of the compressed gas fraction and compressed liquid fraction in order to provide a stream of 2,3,3,3-tetrafluoropropene, a stream of hydrochloric acid, and a stream of unreacted hydrogen fluoride. The invention also concerns an installation suitable for implementing said method.
摘要翻译：本发明涉及一种生产2,3,3,3-四氟丙烯的方法，包括：通过氟化氢将卤代丙烷和/或卤代丙烯氟化反应成2,3,3,3-四氟丙烯; 回收由反应产生的气流; 将由反应产生的气流冷却和部分冷凝成部分冷凝的流; 将部分冷凝的流分离成气体馏分和液体馏分; 将气体馏分压缩成压缩气体馏分; 将液体馏分压缩成压缩液体馏分; 蒸馏压缩气体馏分和压缩液体馏分以提供2,3,3,3-四氟丙烯的流，盐酸流和未反应的氟化氢气流。本发明还涉及适于实现所述方法的安装。

5. 发明授权

US08269052B2 Method for producing pentafluoroethane 有权
标题翻译：五氟乙烷生产方法
公开(公告)号：US08269052B2
公开(公告)日：2012-09-18
申请号：US12302645
申请日：2007-05-09
申请人： Bertrand Collier , Géraldine Cavallini , Béatrice Boussand
发明人： Bertrand Collier , Géraldine Cavallini , Béatrice Boussand
IPC分类号： C07C17/00 , C07C17/38
CPC分类号： C07C19/08 , C07C17/206 , C07C17/21 , Y02P20/582
摘要： The invention relates to a method for producing pentafluoroethane, and especially to a method comprising (i) a step during which perchloroethylene and optionally 2,2-dichloro-1,1,1-trifluoroethane and/or 2-chloro-1,1,1,2-tetrafluoroethane react(s) with hydrofluoric acid in a gaseous phase in the presence of a catalyst in an adiabatic multi-stage reactor, and optionally (ii) a step of separating the flow produced in step (i) in order to obtain a fraction of light products and a fraction of heavy products.
摘要翻译：本发明涉及一种生产五氟乙烷的方法，特别涉及一种方法，其包括（i）全氯乙烯和任选的2,2-二氯-1,1,1-三氟乙烷和/或2-氯-1,1，在绝热多级反应器中，在催化剂存在下，1,2-二氟乙烷与氢氟酸在气相中反应，和任选地（ii）分离步骤（i）中产生的流以便获得一小部分轻质产品和一部分重质产品。

6. 发明申请

US20100280292A1 METHOD OF RECOVERING HYDROFLUORIC ACID 审中-公开
标题翻译：回收氢氟酸的方法
公开(公告)号：US20100280292A1
公开(公告)日：2010-11-04
申请号：US12305875
申请日：2007-05-21
申请人： Bertrand Collier
发明人： Bertrand Collier
IPC分类号： C07C19/08
CPC分类号： C01B7/196 , B01D53/002 , B01D2257/2047 , C01B7/195 , Y02C20/30
摘要： The present invention relates to a process for producing pentafluoroethane. More particularly, the subject of the invention is a continuous process for producing pentafluoroethane comprising (i) a step of fluorinating perchloroethylene (PER) with hydrofluoric acid, in the gas phase, in the presence of a catalyst, (ii) a step of separating the products issuing from step (i) in order to give a fraction of light products and a fraction of heavy products, comprising hydrofluoric acid, unreacted perchloroethylene and under-fluorinated products, and (iii) a step of pretreating the fraction of heavy products before recycling to step (i).
摘要翻译：本发明涉及一种生产五氟乙烷的方法。更具体地，本发明的主题是生产五氟乙烷的连续方法，其包括（i）在气相中，在催化剂存在下，用氢氟酸氟化全氯乙烯（PER）的步骤，（ii）分离步骤从步骤（i）中发出的产品，以产生一小部分轻质产品和一部分重质产品，其中包括氢氟酸，未反应的全氯乙烯和未完全氟化的产物，以及（iii）预处理重质产物部分的步骤回收到步骤（i）。

7. 发明授权

US09334208B2 Process for the preparation of 2,3,3,3 tetrafluoropropene 有权
标题翻译：制备2,3,3,3-四氟丙烯的方法
公开(公告)号：US09334208B2
公开(公告)日：2016-05-10
申请号：US14363918
申请日：2011-12-14
申请人： Dominique Deur-Bert , Bertrand Collier , Laurent Wendlinger
发明人： Dominique Deur-Bert , Bertrand Collier , Laurent Wendlinger
IPC分类号： C07C17/25 , C07C17/20 , C07C17/38 , C07C17/383 , C01B7/19 , B01J37/12 , B01J37/24 , B01J37/26 , B01J23/26 , B01J23/86 , B01J27/132
CPC分类号： C07C17/25 , B01J23/26 , B01J23/866 , B01J27/132 , B01J37/12 , B01J37/24 , B01J37/26 , C01B7/191 , C07C17/206 , C07C17/38 , C07C17/383 , C07C19/08 , C07C21/18
摘要： The present invention provides a process for preparing 2,3,3,3-tetrafluoropropene from 1,1,1,2,3-pentachloropropane and/or 1,1,2,2,3-pentachloropropane, comprising the following steps: (a) catalytic reaction of 1,1,1,2,3-pentachloropropane and/or 1,1,2,2,3-pentachloropropane with HF into a reaction mixture comprising HCl, 2-chloro-3,3,3-trifluoropropene, 2,3,3,3-tetrafluoropropene, unreacted HF, and optionally 1,1,1,2,2-pentafluoropropane; (b) separating the reaction mixture into a first stream comprising HCl and 2,3,3,3-tetrafluoropropene and a second stream comprising HF, 2-chloro-3,3,3-trifluoropropene and optionally 1,1,1,2,2-pentafluoropropane; (c) catalytic reaction of the second stream into a reaction mixture comprising 2,3,3,3-tetrafluoropropene, HCl, unreacted 2-chloro-3,3,3-trifluoropropene, unreacted HF and optionally 1,1,1,2,2-pentafluoropropane and (d) feeding the reaction mixture of step (c) directly without separation to step (a).
摘要翻译：本发明提供从1,1,1,2,3-五氯丙烷和/或1,1,2,2,3-五氯丙烷制备2,3,3,3-四氟丙烯的方法，包括以下步骤：（ a）1,1,1,2,3-五氯丙烷和/或1,1,2,2,3-五氯丙烷与HF的催化反应进入包含HCl，2-氯-3,3,3-三氟丙烯的反应混合物，2,3,3,3-四氟丙烯，未反应的HF和任选的1,1,1,2,2-五氟丙烷; （b）将反应混合物分离成包含HCl和2,3,3,3-四氟丙烯的第一料流和包含HF，2-氯-3,3,3-三氟丙烯和任选的1,1,1,2 ，2-五氟丙烷; （c）将第二流催化反应成包含2,3,3,3-四氟丙烯，HCl，未反应的2-氯-3,3,3-三氟丙烯，未反应的HF和任选的1,1,1,2 （d）直接进料步骤（c）的反应混合物而不分离步骤（a）。

8. 发明授权

US09266799B2 Method for separating and recovering 2,3,3,3-tetrafluoropropene and hydrofluoric acid 有权
标题翻译： 2,3,3,3-四氟丙烯和氢氟酸的分离和回收方法
公开(公告)号：US09266799B2
公开(公告)日：2016-02-23
申请号：US14131036
申请日：2012-06-14
申请人： Dominique Deur-Bert , Bertrand Collier
发明人： Dominique Deur-Bert , Bertrand Collier
IPC分类号： C07C17/38 , C07C21/18 , C07C17/42 , C07C17/25 , C07C17/20 , C01B7/19 , C07C17/35
CPC分类号： C07C17/42 , C01B7/195 , C07C17/20 , C07C17/206 , C07C17/25 , C07C17/35 , C07C17/38 , C07C17/383 , C07C21/18
摘要： The present invention relates to a method for separating a composition containing 2,3,3,3-tetrafluoropropene and hydrofluoric acid, and for recovering the thus-separated 2,3,3,3-tetrafluoropropene and hydrofluoric acid. The invention also relates to a method for manufacturing and purifying 2,3,3,3-tetrafluoropropene using a hydrofluorination reaction of the saturated or unsaturated compound having three carbon atoms and including at least one chlorine atom in the presence of a fluorination catalyst.
摘要翻译：本发明涉及分离含有2,3,3,3-四氟丙烯和氢氟酸的组合物的方法，并用于回收这样分离的2,3,3,3-四氟丙烯和氢氟酸。本发明还涉及在氟化催化剂的存在下，使用具有三个碳原子的饱和或不饱和化合物并且包含至少一个氯原子的氢氟化反应制备和纯化2,3,3,3-四氟丙烯的方法。

9. 发明申请

US20150080619A1 Method for Producing 2,3,3,3-Tetrafluoropropene 有权
标题翻译：生产2,3,3,3-四氟丙烯的方法
公开(公告)号：US20150080619A1
公开(公告)日：2015-03-19
申请号：US14376190
申请日：2013-01-11
申请人： Dominique Deur-Bert , Bertrand Collier , Laurent Wendlinger
发明人： Dominique Deur-Bert , Bertrand Collier , Laurent Wendlinger
IPC分类号： C07C17/20 , F25J1/00
CPC分类号： C07C17/20 , C07C17/206 , C07C17/25 , C07C17/38 , C07C17/383 , F25J1/0022 , F25J3/04412 , C07C21/18
摘要： The invention concerns a method for producing 2,3,3,3-tetrafluoropropene comprising: a fluoridation reaction of a halopropane and/or halopropene into 2,3,3,3-tetrafluoropropene by means of hydrogen fluoride; the recovery of a gas stream resulting from the reaction; the cooling and partial condensation of the gas stream resulting from the reaction into a partially condensed stream; the separation of the partially condensed stream into a gas fraction and a liquid fraction; the compression of the gas fraction into a compressed gas fraction; the compression of the liquid fraction into a compressed liquid fraction; the distillation of the compressed gas fraction and compressed liquid fraction in order to provide a stream of 2,3,3,3-tetrafluoropropene, a stream of hydrochloric acid, and a stream of unreacted hydrogen fluoride. The invention also concerns an installation suitable for implementing said method.
摘要翻译：本发明涉及一种生产2,3,3,3-四氟丙烯的方法，包括：通过氟化氢将卤代丙烷和/或卤代丙烯氟化反应成2,3,3,3-四氟丙烯; 回收由反应产生的气流; 将由反应产生的气流冷却和部分冷凝成部分冷凝的流; 将部分冷凝的流分离成气体馏分和液体馏分; 将气体馏分压缩成压缩气体馏分; 将液体馏分压缩成压缩液体馏分; 蒸馏压缩气体馏分和压缩液体馏分以提供2,3,3,3-四氟丙烯的流，盐酸流和未反应的氟化氢气流。本发明还涉及适于实现所述方法的安装。

10. 发明申请

US20140296585A1 Method for Separating and Recovering 2,3,3,3-tetrafluoropropene and Hydrofluoric Acid 有权
标题翻译：分离和回收2,3,3,3-四氟丙烯和氢氟酸的方法
公开(公告)号：US20140296585A1
公开(公告)日：2014-10-02
申请号：US14131036
申请日：2012-06-14
申请人： Dominique Deur-Bert , Bertrand Collier
发明人： Dominique Deur-Bert , Bertrand Collier
IPC分类号： C07C17/42 , C07C17/35 , C07C17/25
CPC分类号： C07C17/42 , C01B7/195 , C07C17/20 , C07C17/206 , C07C17/25 , C07C17/35 , C07C17/38 , C07C17/383 , C07C21/18
摘要： The present invention relates to a method for separating a composition containing 2,3,3,3-tetrafluoropropene and hydrofluoric acid, and for recovering the thus-separated 2,3,3,3-tetrafluoropropene and hydrofluoric acid. The invention also relates to a method for manufacturing and purifying 2,3,3,3-tetrafluoropropene using a hydrofluorination reaction of the saturated or unsaturated compound having three carbon atoms and including at least one chlorine atom in the presence of a fluorination catalyst.
摘要翻译：本发明涉及分离含有2,3,3,3-四氟丙烯和氢氟酸的组合物的方法，并用于回收这样分离的2,3,3,3-四氟丙烯和氢氟酸。本发明还涉及在氟化催化剂的存在下，使用具有三个碳原子的饱和或不饱和化合物并且包含至少一个氯原子的氢氟化反应制备和纯化2,3,3,3-四氟丙烯的方法。

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