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1. 发明申请

WO2006127223A1 IMPACT-MODIFIED MOLDING COMPOSITION AND METHOD 审中-公开
标题翻译：冲击改性成型组合物和方法
公开(公告)号：WO2006127223A1
公开(公告)日：2006-11-30
申请号：PCT/US2006/016988
申请日：2006-05-03
申请人： GENERAL ELECTRIC COMPANY , DHAWAN, Sandeep , BERZINIS, Albin, Peter , KALYANARAMAN, Viswanathan
发明人： DHAWAN, Sandeep , BERZINIS, Albin, Peter , KALYANARAMAN, Viswanathan
IPC分类号： C08F291/02 , C08F265/04 , C08F285/00
CPC分类号： C08F285/00
摘要： A method is disclosed for preparing an acrylic-styrene-acrylonitrile (ASA) resin, which comprises the steps of: (a) polymerizing a mixture comprising at least one acrylate monomer and at least one crosslinking agent to form a rubber substrate, followed by (b) polymerizing a mixture of monomers in the presence of the rubber substrate, at least one of which monomers is selected from the group consisting of vinyl aromatic monomers and at least one of which monomers is selected from the group consisting of monoethylenically unsaturated nitrile monomers, and optionally followed by (c) polymerizing one or more monomers in at least one subsequent stage in the presence of the rubber substrate from (b), wherein the one or more monomers comprise at least one monomer selected from the group consisting of (C 1 -C 12 ) alkyl- and aryl-(meth)acrylate monomers; wherein the amount of unreacted crosslinking agent remaining in the rubber substrate before step (b) is less than 5.6 micromoles per gram based on the dry weight of the rubber substrate. The invention also relates to a molding composition comprising an ASA resin comprising an elastomeric phase derived from a rubber substrate comprising structural units derived from at least one crosslinking agent; wherein the rubber substrate comprises less than 5.6 micromoles of unreacted crosslinking agent per gram of rubber substrate based on dry weight of the rubber substrate. Articles comprising said ASA resin and/or made from said molding composition are also disclosed.
摘要翻译：公开了一种用于制备丙烯酸 - 苯乙烯 - 丙烯腈（ASA）树脂的方法，其包括以下步骤：（a）使包含至少一种丙烯酸酯单体和至少一种交联剂的混合物聚合以形成橡胶基材，然后（ b）在橡胶基质的存在下聚合单体的混合物，其中至少一种单体选自乙烯基芳族单体，并且其中至少一种单体选自单烯属不饱和腈单体，（c）在（b）中在橡胶基质存在下的至少一个后续阶段中聚合一种或多种单体，其中所述一种或多种单体包含至少一种选自（C 1〜（甲基）丙烯酸烷基酯和/或（甲基）丙烯酸酯单体; 其中在步骤（b）之前残留在橡胶基材中的未反应交联剂的量相对于橡胶基材的干重小于5.6微摩尔/克。本发明还涉及包含ASA树脂的模塑组合物，其包含衍生自橡胶基质的弹性体相，其包含衍生自至少一种交联剂的结构单元; 其中所述橡胶基材基于所述橡胶基材的干重，每克橡胶基材包含小于5.6微摩尔的未反应交联剂。还公开了包含所述ASA树脂和/或由所述模塑组合物制成的制品。

2. 发明申请

WO2021055267A1 METHOD OF PREPARING POLYMER PARTICLES AND POLYMER PARTICLES PREPARED THEREBY 审中-公开
公开(公告)号：WO2021055267A1
公开(公告)日：2021-03-25
申请号：PCT/US2020/050635
申请日：2020-09-14
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , KALYANARAMAN, Viswanathan
发明人： KALYANARAMAN, Viswanathan
IPC分类号： C08J3/14
摘要： Fine polymer particles are prepared by dissolving a polycarbonate, a poly(arylene ether), or a poly(arylene ether sulfone), each in a specific solvent, to form a slurry, heating the slurry to a temperature greater than the solvent boiling point to form a homogeneous solution, cooling the solution to form a dispersion of fine particles, and isolating the fine particles. A volume-based distribution of the isolated fine particles has a median equivalent spherical diameter less than or equal to 125 micrometers.

3. 发明申请

WO2017165805A1 COMPOSITE ARTICLE FROM REACTIVE PRECURSOR MATERIAL 审中-公开
标题翻译：来自反应前驱体材料的复合制品
公开(公告)号：WO2017165805A1
公开(公告)日：2017-09-28
申请号：PCT/US2017/024080
申请日：2017-03-24
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , GENG, Eddie Kebin , ZUBER, Peter James , KALYANARAMAN, Viswanathan , TEUTSCH, Erich Otto
发明人： GENG, Eddie Kebin , ZUBER, Peter James , KALYANARAMAN, Viswanathan , TEUTSCH, Erich Otto
IPC分类号： C08G73/10 , C08J5/24
摘要： A method comprises preparing or receiving a polyetherimide precursor solution including (i) a solvent comprising water, aliphatic alcohol, or a mixture thereof;(ii) an amine additive comprising a secondary or tertiary amine; and (iii) a polyetherimide precursor dissolved and dissociated in the solvent. The method further comprises at least partially coating or impregnating one or more reinforcement structures with the polyetherimide precursor solution and polymerizing the one or more polyetherimide precursor reagents to form a polyetherimide matrix such that the one or more reinforcement structures are at least partially embedded in the polyetherimide matrix to provide a composite article.
摘要翻译：一种方法包括制备或接收聚醚酰亚胺前体溶液，所述聚醚酰亚胺前体溶液包含（i）包含水，脂族醇或其混合物的溶剂;（ii）包含仲胺或叔胺的胺添加剂; 和（iii）在溶剂中溶解和离解的聚醚酰亚胺前体。该方法进一步包括用聚醚酰亚胺前体溶液至少部分地涂布或浸渍一种或多种增强结构，并使一种或多种聚醚酰亚胺前体试剂聚合以形成聚醚酰亚胺基质，使得一种或多种增强结构至少部分地嵌入聚醚酰亚胺矩阵来提供复合文章。

4. 发明申请

WO2018026806A1 METHOD FOR THE MANUFACTURE OF A POLY(IMIDE) PREPOLYMER POWDER AND VARNISH, POLY(IMIDE) PREPOLYMER POWDER AND VARNISH PREPARED THEREBY, AND POLY(IMIDE) PREPARED THEREFROM 审中-公开
标题翻译：制备聚（酰亚胺）预聚物粉末和清漆，聚（酰亚胺）预聚物粉末和由其制备的清漆以及由其制备的聚（酰亚胺）的方法
公开(公告)号：WO2018026806A1
公开(公告)日：2018-02-08
申请号：PCT/US2017/044884
申请日：2017-08-01
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , KALYANARAMAN, Viswanathan
发明人： KALYANARAMAN, Viswanathan , YAMAGUCHI, Norimitsu
IPC分类号： C08G73/10
CPC分类号： C08G73/1032 , C08G73/1028 , C08G73/1046 , C08J5/24
摘要： A method for manufacturing a poly(imide) prepolymer powder includes combining a bisanhydride powder or organic diamine and a solvent comprising an alcohol, a water-soluble ketone or water to form a mixture, adding an organic diamine or bisanhydride powder to the mixture to form a poly(imide) prepolymer, and removing the solvent to provide the poly(imide) prepolymer powder. A method for manufacturing a poly(imide) prepolymer varnish includes combining a bisanhydride powder or organic diamine and a solvent comprising an alcohol, a water-soluble ketone or water to form a mixture, and adding an organic diamine or bisanhydride powder to the mixture to form a poly(imide) prepolymer. The method of manufacturing the varnish further includes at least one of adding an effective amount of a secondary or tertiary amine to solubilize the poly(imide) prepolymer powder, heating the mixture to a temperature effective to provide the varnish, or agitating the mixture to provide the varnish. The poly(imide) prepolymer powder and varnish can have a residual organic diamine content of less than or equal to 1000 ppm. A poly(imide) polymer prepared from the prepolymer powder or varnish is also disclosed.
摘要翻译：用于制造聚（酰亚胺）预聚物粉末的方法包括将二酸酐粉末或有机二胺与包含醇，水溶性酮或水的溶剂混合以形成混合物，将有机二胺或二氢化铝粉末混合以形成聚（酰亚胺）预聚物，并除去溶剂以提供聚（酰亚胺）预聚物粉末。制备聚酰亚胺预聚物清漆的方法包括将二酸酐粉末或有机二胺与包含醇，水溶性酮或水的溶剂混合以形成混合物，并将有机二胺或二酐粉末加入到混合物中形成聚（酰亚胺）预聚物。制造清漆的方法进一步包括添加有效量的仲或叔胺以溶解聚（酰亚胺）预聚物粉末，将混合物加热至有效提供清漆的温度或搅拌混合物以提供清漆。聚（酰亚胺）预聚物粉末和清漆可具有小于或等于1000ppm的残余有机二胺含量。还公开了由预聚物粉末或清漆制备的聚（酰亚胺）聚合物。

5. 发明申请

WO2016111911A1 REACTIVE FRIABLE POLYIMIDE AND METHOD OF MAKING 审中-公开
标题翻译：反应性聚合物及其制备方法
公开(公告)号：WO2016111911A1
公开(公告)日：2016-07-14
申请号：PCT/US2016/012015
申请日：2016-01-04
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , KALYANARAMAN, Viswanathan
发明人： KALYANARAMAN, Viswanathan , TOPLE, Nitin Vilas
IPC分类号： C08G73/10
CPC分类号： C08G73/1053 , C08G73/1078 , C08J3/12 , C08J2379/08 , C08L33/14 , C08L63/00 , C08L79/08
摘要： Disclosed herein is a friable polyimide powder having a weight average molecular weight, as determined by gel permeation chromatography (GPC) using polystyrene standards, of less than or equal to 24,500 Daltons and a reactive aromatic amine end group concentration greater than or equal to 3 mole percent, wherein 90 weight percent of the powder particles are reducible to less than or equal to 75 micrometers by mechanical grinding. Also disclosed is a method of making the friable polyimide powder, a processed polyimide resulting from the friable polyimide powder and compositions comprising the processed polyimide.
摘要翻译：本文公开了具有重均分子量的易碎聚酰亚胺粉末，其通过使用聚苯乙烯标准物的凝胶渗透色谱（GPC）测定的小于或等于24,500道尔顿和反应性芳族胺末端基团浓度大于或等于3摩尔的百分比，其中90重量％的粉末颗粒通过机械研磨可还原成小于或等于75微米。还公开了制造易碎聚酰亚胺粉末的方法，由易碎聚酰亚胺粉末得到的加工聚酰亚胺和包含加工聚酰亚胺的组合物。

6. 发明申请

WO2016109343A1 POLYIMIDE-FORMING COMPOSITIONS, METHODS OF MANUFACTURE, AND ARTICLES PREPARED THEREFROM 审中-公开
标题翻译：聚酰亚胺成分组合物，制备方法和制备的制品
公开(公告)号：WO2016109343A1
公开(公告)日：2016-07-07
申请号：PCT/US2015/067392
申请日：2015-12-22
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , KALYANARAMAN, Viswanathan
发明人： KALYANARAMAN, Viswanathan
IPC分类号： C09D179/08 , C08G73/10
CPC分类号： C08G73/1028 , B29B11/14 , B29K2079/085 , B29K2896/02 , B29K2896/04 , C08J7/14 , C08K5/0008 , C09D179/085
摘要： A polyimide-forming composition includes a particulate polyimide precursor composition having an average particle size of 0.1 to 100 micrometers wherein the polyimide precursor composition comprises a substituted or unsubstituted C 4-40 bisanhydride, and a substituted or unsubstituted divalent C 1-20 diamine; an aqueous carrier; and a surfactant. A method of manufacturing an article including a polyimide includes the steps of forming a preform comprising the polyimide-forming composition; and heating the preform at a temperature and for a period of time effective to imidize the polyimide precursor composition and form the polyimide. An article prepared by the method, and a layer or coating including a polyimide and a surfactant are also described.
摘要翻译：聚酰亚胺形成组合物包括平均粒度为0.1至100微米的颗粒状聚酰亚胺前体组合物，其中聚酰亚胺前体组合物包含取代或未取代的C 4-40双酸酐，以及取代或未取代的二价C 1-20二胺; 水性载体; 和表面活性剂。制造包含聚酰亚胺的制品的方法包括以下步骤：形成包含聚酰亚胺形成组合物的预成型体; 并在一定温度下加热预制件，并且有效地使酰亚胺化聚酰亚胺前体组合物形成聚酰亚胺。还描述了通过该方法制备的制品和包含聚酰亚胺和表面活性剂的层或涂层。

7. 发明申请

WO2018106525A1 PROCESS FOR THE MANUFACTURE OF THERMOPLASTIC POLYMER PARTICLES, THERMOPLASTIC POLYMER PARTICLES MADE THEREBY, AND ARTICLES MADE THEREFROM 审中-公开
公开(公告)号：WO2018106525A1
公开(公告)日：2018-06-14
申请号：PCT/US2017/064138
申请日：2017-12-01
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , KALYANARAMAN, Viswanathan
发明人： KALYANARAMAN, Viswanathan , PRICE, Brian
IPC分类号： C08J3/14
摘要： A process for the manufacture of thermoplastic polymer particles in a yield of greater than 70% is described. The process includes dissolving a thermoplastic polymer in an organic solvent capable of dissolving the polymer to form a solution, emulsifying the solution by combining the solution with water and a surfactant to form an emulsion, removing the organic solvent to form a slurry, and recovering thermoplastic polymer particles having a diameter of less than 150 micrometers and in a yield of greater than 70%. The water is present in the emulsion in an amount of 5 to less than 50 weight percent. The thermoplastic polymer particles exhibit a combination of size characteristics. Thermoplastic polymer particles and articles prepared therefrom are also described.

8. 发明申请

WO2017004140A1 PROCESS OF MAKING POLYIMIDE MICRONIZED PARTICLES, PARTICLES FORMED THEREFROM, AND ARTICLES PREPARED THEREFROM 审中-公开
标题翻译：制备聚酰胺微粒的方法，其形成的颗粒及其制备的制品
公开(公告)号：WO2017004140A1
公开(公告)日：2017-01-05
申请号：PCT/US2016/039994
申请日：2016-06-29
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , KALYANARAMAN, Viswanathan
发明人： KALYANARAMAN, Viswanathan , DESHPANDE, Hareesh Shamrao , MORALI, Ekrem Mehmet
IPC分类号： C08J3/07 , C09D179/08 , C08K5/42
CPC分类号： C08J3/14 , B01D21/262 , B01D33/64 , C08G73/1053 , C08G73/106 , C08G73/1064 , C08G73/1071 , C08J3/07 , C08J2379/08 , C09D179/08 , C09J179/08
摘要： A method of manufacturing polyimide particles, including: combining a polyimide solution including a polyimide and an organic solvent with an aqueous solution including water in the presence of an emulsifying surfactant at a shear rate from 1,000 to 3,000 revolutions per minute, from 1,000 to 2,500 revolutions per minute, or from 1,500 to less than 2,500 revolutions per minute to form an emulsion; removing the organic solvent to form an aqueous polymer dispersion including polyimide particles; and recovering the polyimide particles, which have a spherical morphology, and a volume based D10 diameter from 3 to 50 micrometers, preferably from 3 to 45 micrometers and a volume based D90 diameter from 3 to 80 micrometers, from 3 to 75 micrometers, or from 3 to 45 micrometers and a volume based D100 diameter from 3 to 100 micrometers, from 3 to 75 micrometers, or from 10 to 75 micrometers.
摘要翻译：一种制造聚酰亚胺颗粒的方法，包括：在1000至3000转/分钟的剪切速率下，在乳化表面活性剂存在下，将包含聚酰亚胺和有机溶剂的聚酰亚胺溶液与包含水的水溶液组合在一起，为1,000至2500转或1500至小于2500转/分钟以形成乳液; 除去有机溶剂以形成包含聚酰亚胺颗粒的聚合物水分散体; 并回收具有球形形态的聚酰亚胺颗粒，体积基于D10直径为3至50微米，优选3至45微米，体积基于D90直径为3至80微米，3至75微米，或从 3至45微米，体积基于D100直径为3至100微米，3至75微米，或10至75微米。

9. 发明申请

WO2016134126A1 POLY(AMIC ACID) SYNTHESIS AND CONVERSION TO HIGH MOLECULAR WEIGHT POLYIMIDE 审中-公开
标题翻译： POLY（AMIC ACID）合成和转化为高分子量聚酰胺
公开(公告)号：WO2016134126A1
公开(公告)日：2016-08-25
申请号：PCT/US2016/018435
申请日：2016-02-18
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , KALYANARAMAN, Viswanathan
发明人： KALYANARAMAN, Viswanathan
IPC分类号： C08G73/10 , C09D179/08
CPC分类号： C08G73/1032 , C08G73/1017 , C09D179/08
摘要： A process is disclosed for synthesis of a poly(amic acid), including reacting a dianhydride and a diamine in the presence of a tertiary amine, tertiary ammonium salt, tertiary ammonium hydroxide, secondary amine, secondary ammonium salt, secondary ammonium hydroxide, quaternary ammonium salt, quaternary ammonium hydroxide, ammonium hydroxide, or a combination comprising at least one of the foregoing, in water, at a temperature of 60C to 180C, or 60C to 100C, or 100C to 180C, under an inert atmosphere, with agitation, to produce an aqueous poly(amic acid).
摘要翻译：公开了用于合成聚（酰胺酸）的方法，包括在叔胺，叔铵盐，氢氧化铵，仲胺，仲铵盐，仲氢氧化铵，季铵盐的存在下使二酐和二胺反应盐，季铵氢氧化物，氢氧化铵或包含至少一种前述物质的组合，在水中，在60℃至180℃，或60℃至100℃或100℃至180℃的温度下，在惰性气氛下搅拌，至产生聚（酰胺酸）水溶液。

10. 发明申请

WO2014151481A1 PROCESS OF MAKING WATER DISPERSED POLYETHERIMIDE MICRONIZED PARTICLES AND PROCESS OF COATING AND FURTHER FORMING OF THESE PARTICLES PRODUCTS MADE THEREFROM 审中-公开
标题翻译：制备水分散聚乙二醇微球颗粒的方法及其制备方法和进一步形成这些颗粒的产品
公开(公告)号：WO2014151481A1
公开(公告)日：2014-09-25
申请号：PCT/US2014/025824
申请日：2014-03-13
申请人： SABIC INNOVATIVE PLASTICS IP B.V. , KALYANARAMAN, Viswanathan
发明人： KALYANARAMAN, Viswanathan
IPC分类号： C09D5/02 , C09D7/12 , C09D179/08 , C09D181/06
CPC分类号： C09D7/63 , C08G73/1046 , C08L79/08 , C09D5/027 , C09D7/69 , C09D179/08 , Y10T428/31623 , Y10T428/31681 , Y10T428/31721
摘要： Processes involving wetting fibers with an aqueous dispersion of micronized thermoplastic powders; processes for producing an aqueous dispersion of micronized thermoplastic powders; processes of chemically surface crosslinking micronized particles; and articles of produced therefrom.
摘要翻译：涉及用微粉化热塑性粉末的水性分散体润湿纤维的方法; 制备微粉化热塑性粉末的水性分散体的方法; 化学表面交联微粉化过程; 和由此产生的物品。

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