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1. 发明授权

US4636333A Alkoxy-substituted polyhydroindan carboxaldehydes 失效
标题翻译：烷氧基取代的多羟基茚满羧醛
公开(公告)号：US4636333A
公开(公告)日：1987-01-13
申请号：US837386
申请日：1986-03-07
申请人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
发明人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
IPC分类号： C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0042 , C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523
摘要： Described is a mixture of polyhydroindan carboxaldehydes defined according to the structure: ##STR1## wherein R.sub.7 represents a moiety selected from the group consisting of methyl and isopropyl prepared by means of reacting bicyclopentadiene with a lower alkanol in the presence of a Lewis acid in order to form a mixture of compounds defined according to the structure: ##STR2## and then reacting the resulting ether with carbon monoxide and hydrogen in the presence of an "oxo" reaction catalyst.
摘要翻译：描述了根据以下结构定义的多羟基茚基甲醛的混合物：其中R 7表示选自甲基和异丙基的部分，其通过在路易斯酸存在下通过双环戊二烯与低级链烷醇反应制备，以便形成根据以下结构定义的化合物的混合物：，然后在“氧代”反应催化剂存在下，使所得的醚与一氧化碳和氢气反应。

2. 发明授权

US4554385A Tertiary hydroxyl carboxaldehydes, organoleptic uses thereof, and processes for producing same 失效
标题翻译：叔羟基醛，其感官用途及其制备方法
公开(公告)号：US4554385A
公开(公告)日：1985-11-19
申请号：US709916
申请日：1985-03-08
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： C07C47/36 , C07C47/19
CPC分类号： C07C47/36
摘要： Described are tertiary hydroxyl carboxaldehydes defined according to the generic structure: ##STR1## wherein the lines ##STR2## represent covalent carbon-carbon bonds when m does not=0; and wherein the lines ##STR3## do not represent any bonds when m=0; wherein R represents hydrogen or methyl; wherein p and q each represents 0 or 1 with the proviso that p=1 when q=0 and p=0 when q=1; wherein X and Z each represent one or more carbon atoms required to complete a bicyclo ring with the lines ##STR4## representing carbon-carbon bonds; wherein X and Z complete a phenyl moiety when the line ##STR5## represents no bond; wherein X and Z complete a cycloalkyl ring moiety with the lines ##STR6## represent carbon-carbon bonds and with the line ##STR7## representing no bond; and wherein when m is 0, X represents an alkylene moiety, processes for preparing same by means of reacting carbon monoxide and hydrogen with an unsaturated tertiary alcohol defined according to the structure: ##STR8## by means of an oxo reaction, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., cosmetic powders, perfumed polymers, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, face creams, and the like).
摘要翻译：描述的是根据通用结构定义的叔羟基醛：其中当m不为0时，线和 - - - - 和/或+ + + + +代表共价碳 - 碳键; 并且当m = 0时，线+ + + + +和 - - - - - 不表示任何键; 其中R表示氢或甲基; 其中p和q各自表示0或1，条件是当q = 0时p = 1，q = 1时p = 0; 其中X和Z各自表示一个或多个用代表碳 - 碳键的+ + + + +和 - 当线 - - - - 表示无键时，X和Z完全为苯基部分; 其中X和Z与所述线完成环烷基环部分，并且+ + + + +代表碳 - 碳键，并且具有不代表键的线 - - - - - 。并且其中当m为0时，X表示亚烷基部分，通过使一氧化碳和氢与根据以下结构定义的不饱和叔醇反应制备其方法：通过氧代反应，其用途在增加或增强香水组合物，古龙水和香水制品（例如，化妆品粉末，加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂，面霜和喜欢）。

3. 发明授权

US4540812A 2-Acetoxy-4-(2-bornyloxy) butane 失效
标题翻译： 2-乙酰氧基-4-（2-苄氧基）丁烷
公开(公告)号：US4540812A
公开(公告)日：1985-09-10
申请号：US578346
申请日：1984-02-09
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , C07C69/14
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277
摘要： Described is the 2-acetoxy-4-(2-bornyloxy) butane of our invention defined according to the structure: ##STR1## as well as methods for augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles by adding thereto an aroma augmenting or enhancing quantity of the 2-acetoxy-4-(2-bornyloxy) butane of our invention.
摘要翻译：描述了根据以下结构定义的本发明的2-乙酰氧基-4-（2-甲氧基）丁烷：＆lt; IMAGE＆gt;以及通过添加其来增强或增强消耗材料的香气的方法，包括香料，古龙水和香料制品香气增加或增加本发明的2-乙酰氧基-4-（2-甲氧基）丁烷。

4. 发明授权

US4539142A 4-(2-Bornyloxy)-2-butyn-1-ol and organoleptic uses thereof 失效
标题翻译： 4-（2-呋喃氧基）-2-丁炔-1-醇及其感官用途
公开(公告)号：US4539142A
公开(公告)日：1985-09-03
申请号：US604230
申请日：1984-04-26
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , A61K7/46 , C07C5/23
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C07C2102/42 , Y10S514/951
摘要： Described is the 4-(2-bornyloxy)-2-butyn-1-ol of our invention defined according to the structure: ##STR1## as well as methods for augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles by adding thereto an aroma augmenting or enhancing quantity of the 4-(2-bornyloxy)-2-butyn-1-ol of our invention.
摘要翻译：描述了根据以下结构定义的本发明的4-（2-开氧基）-2-丁炔-1-醇，以及用于增强或增强消耗材料的香气的方法，包括香料，古龙水和香料制品通过向其中加入增加或增加本发明的4-（2-甲氧基）-2-丁炔-1-醇的香味。

5. 发明授权

US4521634A Ether carbinols and process for preparing same 失效
标题翻译：醚甲醇及其制备方法
公开(公告)号：US4521634A
公开(公告)日：1985-06-04
申请号：US574150
申请日：1984-01-26
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , C07C43/188 , C07C41/06
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C07C2102/42
摘要： Described are ether carbinols defined according to the generic structure: ##STR1## wherein X.sub.1 represents a moiety selected from the group consisting of: ##STR2## and wherein Y.sub.1 represents C.sub.4 or C.sub.5 alkylene or C.sub.4 or C.sub.5 alkenylene or C.sub.4 or C.sub.5 alkynylene; processes for preparing such ether carbinols by means of first reacting allyl ethers with a mixture of carbon monoxide and hydrogen by means of an oxoreaction to produce ether carboxaldehydes and then reducing the thus formed ether carboxaldehydes to ether carbinols; or reacting camphene with appropriate diols; as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; and smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carbinols.Also described are two ether carboxaldehydes having one of the structures: ##STR3## processes for preparing such ether carboxaldehydes by means of reacting out an appropriate allyl ether with a mixture of carbon monoxide and hydrogen by means of an oxo-reaction as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carboxaldehydes.
摘要翻译：描述根据通用结构定义的醚甲醇：其中X 1表示选自下列的部分：其中Y 1表示C 4或C 5亚烷基或C 4或C 5亚链烯基或C 4或C 4 C5亚炔基; 通过首先使烯丙基醚与一氧化碳和氢气的混合物通过氧化反应制备这种醚甲醇的方法，以产生醚甲醛，然后将由此形成的醚甲醛还原成醚甲醇; 或使camp烯与适当的二醇反应; 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 并通过向其中加入香烟或味道来增加或增加如此生产的醚甲醇，从而吸烟烟草和烟草制品。还描述了具有以下结构之一的两种醚甲醛：通过使一种合适的烯丙基醚与一氧化碳和氢气的混合物通过氧代反应制备这种醚甲醛的方法以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 通过向其中加入香味或味道增加或增加如此制备的醚甲醛的量来吸烟烟草和烟草制品。

6. 发明授权

US4519943A 5-Alkoxybicyclo[2.2.1]heptane-2-oxypropane derivatives and uses thereof in augmenting or enhancing the aromas of perfume compositions, colognes and perfumed articles 失效
标题翻译： 5-烷氧基双环[2.2.1]庚烷-2-氧基丙烷衍生物及其用于增强或增强香料组合物，古龙水和香料的香味
公开(公告)号：US4519943A
公开(公告)日：1985-05-28
申请号：US535794
申请日：1983-09-26
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber , Patrick Whelan , Marie R. Hanna
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber , Patrick Whelan , Marie R. Hanna
IPC分类号： C07C43/196 , C07C45/49 , C07C47/198 , C11B9/00 , A61K7/46 , C07C35/24 , C07C47/34
CPC分类号： C11B9/0046 , C07C43/196 , C07C45/49 , C07C47/198
摘要： Described are 5-alkoxybicyclo[2.2.1]heptane-2-oxypropane derivatives defined according to the structure: ##STR1## (wherein R represents C.sub.1 -C.sub.3 alkyl and wherein Z represents one of the moieties, carbinol having the structure: ##STR2## or carboxaldehyde having the structure: ##STR3## and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes or perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders, hair preparations, perfumed polymers and the like).
摘要翻译：描述了根据以下结构定义的5-烷氧基双环[2.2.1]庚烷-2-氧代丙烷衍生物：其中R表示C1-C3烷基，其中Z表示其中一个部分，具有以下结构的甲醇：或具有以下结构的羧甲醛：其用于增强或增强香料组合物，古龙水或香水制品（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，化妆品粉末，头发制剂，加香聚合物等）。

7. 发明授权

US4751933A Use of hydroxybornyloxybutanes in augmenting or enhancing the aroma or taste of smoking tobacco articles and smoking tobacco compositions 失效
标题翻译：使用羟基苯氧基丁烷来增强或增强吸烟烟草制品和吸烟烟草组合物的香气或味道
公开(公告)号：US4751933A
公开(公告)日：1988-06-21
申请号：US2022
申请日：1987-01-09
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , A24B3/12
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277
摘要： Described are the uses of mixtures of hydroxybornyloxybutanes defined according to the generic structure: ##STR1## wherein in the mixture in each of the compounds one or R.sub.1 or R.sub.2 is methyl and the other of R.sub.1 or R.sub.2 is hydrogen in augmenting or enhancing the aroma or taste of smoking tobacco articles and smoking tobacco compositions.
摘要翻译：描述了根据通用结构定义的羟基乙氧基丁烷的混合物的用途：其中在每个化合物的混合物中，一个或R 1或R 2是甲基，R 1或R 2中的另一个是氢，以增强或增强香气或吸烟烟草制品和吸烟烟草组合物的味道。

8. 发明授权

US4622171A Polyhydroindan carboxaldehydes and uses thereof in augmenting or enhancing the aromas of perfume compositions, colognes and perfumed articles 失效
公开(公告)号：US4622171A
公开(公告)日：1986-11-11
申请号：US712164
申请日：1985-03-15
申请人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
发明人： Mark A. Sprecker , William L. Schreiber , Futoshi Fujioka , Richard M. Boden , Manfred H. Vock , Patrick Whelan , Marie R. Hanna
IPC分类号： C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0042 , C07C45/49 , C07C45/50 , C07C47/36 , C07C47/37 , C07C47/445 , C07C49/523
摘要： Described is the genus of polyhydroindan carboxaldehydes defined according to the structure: ##STR1## wherein each of the dashed lines represent carbon-carbon single bonds or carbon-carbon double bonds with the proviso that at least one of the dashed lines represents a carbon-carbon single bond; wherein one of R.sub.1, R.sub.2 and R.sub.3 is hydrogen or methyl and each of the other of R.sub.1, R.sub.2 and R.sub.3 represents hydrogen; wherein one of R.sub.4, R.sub.5 and R.sub.6 represents hydrogen or methyl and each of the other of R.sub.4, R.sub.5 and R.sub.6 represents hydrogen; wherein m is 0 or 1 and n is 0 or 1 and the sum of m+n=1; wherein X' represents one of the moieties: ##STR2## wherein R.sub.7 represents C.sub.1 -C.sub.3 alkyl or acetyl; and wherein R.sub.8 represents C.sub.1 -C.sub.3 alkyl, with the proviso that when X' is methylene having the structure: ##STR3## then m is 0 and n is 1 and with the further proviso that when n is 0, one of the dashed lines is a carbon-carbon double bond; and one of R.sub.1, R.sub.2 and R.sub.3 represents methyl and one of R.sub.4, R.sub.5, and R.sub.6 represents methyl, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, perfumed polymers and cosmetic powders). Also described is a process for preparing such polyhydroindan carboxaldehydes by reacting a tricyclic compound or mixture of compounds defined according to the structure: ##STR4## with carbon monoxide and hydrogen via an "oxo" reaction; wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are defined, supra; wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein X" represents one of the moieties: with the proviso that when X' is methylene having the structure: ##STR5## then the line:+++++is a double bond and when X' is not methylene having the structure: ##STR6## then the line:+++++is a carbon-carbon single bond.

9. 发明授权

US4620041A Ether carbinols 失效
标题翻译：乙醚甲醇
公开(公告)号：US4620041A
公开(公告)日：1986-10-28
申请号：US784618
申请日：1985-10-04
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C07C2102/42
摘要： Described are ether carbinols defined according to the generic structure: ##STR1## wherein X.sub.1 represents a moiety selected from the group consisting of: ##STR2## and wherein Y.sub.1 represents C.sub.4 or C.sub.5 alkylene; C.sub.4 or C.sub.5 alkenylene or C.sub.4 or C.sub.5 alkynylene; processes for preparing such ether carbinols by means of first reacting allyl ethers with a mixture or carbon monoxide and hydrogen by means of an oxo reaction to produce ether carboxaldehydes and then reducing the thus formed ether carboxaldehydes to ether carbinols; or reacting camphene with appropriate diols; as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; and smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carbinols.Also described are two ether carboxaldehydes having one of the structures: ##STR3## processes for preparing such ether carboxaldehydes by means of reacting out an appropriate allyl ether with a mixture of carbon monoxide and hydrogen by means of an oxo-reaction as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colgnes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carboxaldehydes.
摘要翻译：描述了根据通用结构定义的醚甲醇：其中X 1表示选自以下的部分：其中Y 1表示C 4或C 5亚烷基; C4或C5亚链烯基或C4或C5亚炔基; 通过首先使烯丙基醚与混合物或一氧化碳和氢气通过羰基反应反应生成醚甲醛，然后将由此形成的醚甲醛还原成醚甲醇来制备此类醚甲醇的方法; 或使camp烯与适当的二醇反应; 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 并通过向其中加入香烟或味道来增加或增加如此生产的醚甲醇，从而吸烟烟草和烟草制品。还描述了具有以下结构之一的两个醚甲醛：＆lt; IMAGE＆gt;和＆lt; IMAGE＆gt;用于通过使羰基合成的烯丙基醚与一氧化碳和氢的混合物通过氧代 - 以及用于增强或增强消耗材料的香气或味道的方法，包括香料，水泥和香料制品; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 通过向其中加入香味或味道增加或增加如此制备的醚甲醛的量来吸烟烟草和烟草制品。

10. 发明授权

US4608195A Preparing a tertiary hydroxyl carboxaldehyde containing perfume composition 失效
标题翻译：制备含羟基甲醛的香料组合物
公开(公告)号：US4608195A
公开(公告)日：1986-08-26
申请号：US768839
申请日：1985-08-23
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： C07C45/49 , C07C47/27 , C07C47/36 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0061 , C07C45/49 , C07C47/27 , C07C47/36
摘要： Described are tertiary hydroxyl carboxaldehydes defined according to the generic structure: ##STR1## wherein the lines ##STR2## represent covalent carbon-carbon bonds when m does not=0; and wherein the lines ##STR3## do not represent any bonds when m=0; wherein R represents hydrogen or methyl; wherein p and q each represents 0 or 1 with the proviso that p=1 when q=0 and p=0 when q=1; wherein X and Z each represent one or more carbon atoms required to complete a bicyclo ring with the lines ##STR4## representing carbon-carbon bonds; wherein X and Z complete a phenyl moiety when the line ##STR5## represents no bond; wherein X and Z complete a cycloalkyl ring moiety with the lines ##STR6## represent carbon-carbon bonds and with the line ##STR7## representing no bond; and wherein when m is 0, X represents an alkylene moiety, processes for preparing same by means of reacting carbon monoxide and hydrogen with an unsaturated tertiary alcohol defined according to the structure: ##STR8## by means of an oxo reaction, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., cosmetic powders, perfumed polymers solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, face creams, and the like).
摘要翻译：描述的是根据通用结构定义的叔羟基甲醛：其中当m不为0时，线* * * * *和 - - - - - 和/或+ + + + +代表共价碳 - 碳键 ; 并且当m = 0时，线+ + + + + * * * * *和 - - - - - 不表示任何键; 其中R表示氢或甲基; 其中p和q各自表示0或1，条件是当q = 0时p = 1，q = 1时p = 0; 其中X和Z各自表示一个或多个完成具有代表碳 - 碳键的线+ + + + + * * * * *和 - - - - 的双环的所需的碳原子。当线 - - - - 表示无键时，X和Z完全为苯基部分; 其中X和Z完全是环烷基环部分，其中线* * * *和+ + + +代表碳 - 碳键，并且线 - - - - - 不表示键; 并且其中当m为0时，X表示亚烷基部分，通过使一氧化碳和氢与根据以下结构定义的不饱和叔醇反应制备其方法：通过氧代反应，其用途在增加或增强香水组合物，古龙水和香水制品（例如，化妆品粉末，加香聚合物固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂，面霜等）的香气）。

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