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1. 发明授权

US07026506B2 Method for producing acrylic acid by heterogeneously catalyzed gas-phase oxidation of propene with molecular oxygen in a reaction zone 失效
标题翻译：通过在反应区中用分子氧异丙烯催化丙烯气相氧化丙烯来制备丙烯酸的方法
公开(公告)号：US07026506B2
公开(公告)日：2006-04-11
申请号：US10474202
申请日：2002-04-12
申请人： Frieder Borgmeier , Jochen Petzoldt , Hartmut Hibst , Andreas Tenten
发明人： Frieder Borgmeier , Jochen Petzoldt , Hartmut Hibst , Andreas Tenten
IPC分类号： C07C51/16
CPC分类号： C07C45/33 , B01J23/002 , B01J23/28 , B01J27/0576 , B01J37/0232 , C07C45/35 , C07C47/22
摘要： In a process for the preparation of acrylic acid by heterogeneously catalyzed gas-phase oxidation of propene with molecular oxygen in a reaction zone, the catalytically active material is a multimetal oxide which contains the elements Mo, V, Te and/or Sb and has a specific structure.
摘要翻译：在通过在反应区中用分子氧进行非均相催化丙烯气相氧化丙烯酸的方法中，催化活性材料是多元氧化物，其含有元素Mo，V，Te和/或Sb，并具有具体结构。

2. 发明申请

US20090234159A1 PREPARATION OF CATALYTICALLY ACTIVE MULTIELEMENT OXIDE MATERIALS WHICH CONTAIN AT LEAST ONE OF THE ELEMENTS NB AND W AND THE ELEMENTS MO, V AND CU 有权
标题翻译：含有至少一个元素NB和W以及元素MO，V和CU的催化活性多元素氧化物材料的制备
公开(公告)号：US20090234159A1
公开(公告)日：2009-09-17
申请号：US12401349
申请日：2009-03-10
申请人： Martin DIETERLE , Hartmut Hibst , Wolfgang Juergen Popel , Jochen Petzoldt , Klaus Joachim Muller-Engel
发明人： Martin DIETERLE , Hartmut Hibst , Wolfgang Juergen Popel , Jochen Petzoldt , Klaus Joachim Muller-Engel
IPC分类号： C07C51/235 , C07C51/215
CPC分类号： B01J23/002 , B01J23/8877 , B01J23/8885 , B01J35/0006 , B01J37/08 , B01J2523/00 , C07C51/215 , C07C51/235 , C07C57/04 , B01J2523/17 , B01J2523/68 , B01J2523/69
摘要： A process for making acrylic acid from acrolein; a process for making methacrylic acid from methacrolein; and a process for making acrylic acid from propane.
摘要翻译：丙烯醛制造丙烯酸的方法; 从甲基丙烯醛制造甲基丙烯酸的方法; 以及由丙烷制造丙烯酸的方法。

3. 发明授权

US07524792B2 Preparation of catalytically active multielement oxide materials which contain at least one of the elements Nb and W and the elements Mo, V and Cu 有权
标题翻译：制备催化活性多元素氧化物材料，其含有元素Nb和W中的至少一种元素Mo，V和Cu
公开(公告)号：US07524792B2
公开(公告)日：2009-04-28
申请号：US10840745
申请日：2004-05-07
申请人： Martin Dieterle , Hartmut Hibst , Wolfgang Juergen Poepel , Jochen Petzoldt , Klaus Joachim Mueller-Engel
发明人： Martin Dieterle , Hartmut Hibst , Wolfgang Juergen Poepel , Jochen Petzoldt , Klaus Joachim Mueller-Engel
IPC分类号： B01J23/00
CPC分类号： B01J23/002 , B01J23/8877 , B01J23/8885 , B01J35/0006 , B01J37/08 , B01J2523/00 , C07C51/215 , C07C51/235 , C07C57/04 , B01J2523/17 , B01J2523/68 , B01J2523/69
摘要： Catalytically active multielement oxide materials which contain at least one of the elements Nb and W and the elements Mo, V and Cu are prepared by a process in which an intimate dry blend containing ammonium ions is prepared and said dry blend is subjected to a thermal treatment in an atmosphere having a low molecular oxygen content at elevated temperatures, a portion of the ammonium ions contained in the intimate dry blend being decomposed with liberation of ammonia and the oxygen content of the thermal treatment atmosphere being increased in the course of the thermal treatment.
摘要翻译：含有至少一种元素Nb和W以及元素Mo，V和Cu的催化活性多元素氧化物材料通过其中制备含有铵离子的紧密干混合物并对所述干混合物进行热处理的方法制备在升高的温度下具有低分子氧含量的气氛中，紧密干燥混合物中所含的一部分铵离子被氨释放分解，热处理气氛的氧含量在热处理过程中增加。

4. 发明授权

US07667073B2 Preparation of catalytically active multielement oxide materials which contain at least one of the elements Nb and W and the elements Mo, V and Cu 有权
标题翻译：制备催化活性多元素氧化物材料，其含有元素Nb和W中的至少一种元素Mo，V和Cu
公开(公告)号：US07667073B2
公开(公告)日：2010-02-23
申请号：US12401349
申请日：2009-03-10
申请人： Martin Dieterle , Hartmut Hibst , Wolfgang Juergen Popel , Jochen Petzoldt , Klaus Joachim Mueller-Engel
发明人： Martin Dieterle , Hartmut Hibst , Wolfgang Juergen Popel , Jochen Petzoldt , Klaus Joachim Mueller-Engel
IPC分类号： C07C51/235 , C07C51/215 , B01J23/00
CPC分类号： B01J23/002 , B01J23/8877 , B01J23/8885 , B01J35/0006 , B01J37/08 , B01J2523/00 , C07C51/215 , C07C51/235 , C07C57/04 , B01J2523/17 , B01J2523/68 , B01J2523/69
摘要： A process for making acrylic acid from acrolein; a process for making methacrylic acid from methacrolein; and a process for making acrylic acid from propane.
摘要翻译：丙烯醛制备丙烯酸的方法; 从甲基丙烯醛制造甲基丙烯酸的方法; 以及由丙烷制造丙烯酸的方法。

5. 发明申请

US20120077977A1 PROCESS FOR PREPARING (METH)ACRYLIC ESTERS OF N,N-SUBSTITUTED AMINO ALCOHOLS 审中-公开
标题翻译：制备N，N-取代氨基醇的（甲基）丙烯酸酯的方法
公开(公告)号：US20120077977A1
公开(公告)日：2012-03-29
申请号：US13236893
申请日：2011-09-20
申请人： Virginie Bette , Hermann Bergmann , Jochen Petzoldt , Frank Höfer
发明人： Virginie Bette , Hermann Bergmann , Jochen Petzoldt , Frank Höfer
IPC分类号： C07C67/02 , C07D295/185 , C07D295/15
CPC分类号： C07D295/088
摘要： The present invention relates to a process for preparing (meth)acrylic esters (F) of N,N-substituted amino alcohols, by transesterifying N,N-substituted amino alcohols (I) in which Y and Z are each independently C1-C20-alkyl, C3-C15-cycloalkyl, aryl, or Y and Z together with the nitrogen atom connecting them form a 5- to 9-membered saturated heterocyclic radical which optionally has oxygen, sulfur, nitrogen or C1-C4-alkyl-substituted nitrogen as a further heteroatom, and X is C2-C20-alkylene which may be interrupted by 1 to 10 nonadjacent oxy groups and/or unsubstituted or methoxy-substituted C1-C4-alkylimino groups, or a C3-C15-cycloalkylene, with at least one (meth)acrylic ester (D) in the presence of at least one heterogeneous catalyst (K), wherein the heterogeneous catalyst (K) is used without any further solvent and the content of polymerization inhibitors in the reaction mixture is
摘要翻译：本发明涉及一种制备N，N-取代氨基醇的（甲基）丙烯酸酯（F）的方法，其中N，N-取代的氨基醇（I），其中Y和Z各自独立地为C 1 -C 20 - 烷基，C 3 -C 15 - 环烷基，芳基或Y和Z与连接它们的氮原子一起形成5-至9-元饱和杂环基，其任选具有氧，硫，氮或C 1 -C 4 - 烷基取代的氮作为另外的杂原子，X是可被1-10个不相邻的氧基和/或未被取代的或甲氧基取代的C 1 -C 4烷基亚氨基或C 3 -C 15 - 亚环烷基间隔的C 2 -C 20亚烷基，其中至少有一个（甲基）丙烯酸酯（D）在至少一种非均相催化剂（K）的存在下使用，其中非均相催化剂（K）不使用任何其它溶剂而使用，反应混合物中的聚合抑制剂的含量<450ppm，和涉及使用N，N-取代的氨基醇的（甲基）丙烯酸酯（F）。

6. 发明申请

US20100274042A1 PROCESS FOR PREPARING (METH)ACRYLIC ESTERS OF ALCOHOLS COMPRISING POLYALKOXY GROUPS 审中-公开
标题翻译：制备包含聚烷氧基团的醇的丙烯酸酯的方法
公开(公告)号：US20100274042A1
公开(公告)日：2010-10-28
申请号：US12764349
申请日：2010-04-21
申请人： Virginie BETTE , Jochen Petzoldt , Hermann Bergmann
发明人： Virginie BETTE , Jochen Petzoldt , Hermann Bergmann
IPC分类号： C07C67/02
CPC分类号： C07C67/03 , C08G65/3322 , C08L71/02 , C08L2205/05 , C07C69/54 , C08L2666/04
摘要： A process for preparing (meth)acrylic esters (E) of alcohols (A) comprising polyalkoxy groups, in which alcohols (A) which comprise polyalkoxy groups and are of the formula (I) RO—[(CH2)mO]n—H (I) in which m is an integer from 1 to 10, n is an integer from 1 to 100 and R is a straight-chain saturated or unsaturated alcohol having 1 to 30 carbon atoms, are transesterified with at least one (meth) acrylic ester (D) in the presence of at least one inorganic salt (S).
摘要翻译：一种制备包含聚烷氧基的（甲基）丙烯酸酯（E）的方法，其中包含聚烷氧基并且具有式（I）的醇（A）RO - [（CH 2）m O] n -H （I）其中m是1至10的整数，n是1至100的整数，R是具有1至30个碳原子的直链饱和或不饱和醇，与至少一种（甲基）丙烯酸酯酯（D）在至少一种无机盐（S）的存在下反应。

7. 发明申请

US20100069660A1 PROCESS FOR PRODUCING GEOMETRIC SHAPED CATALYST BODIES 有权
标题翻译：生产几何形状催化剂体的方法
公开(公告)号：US20100069660A1
公开(公告)日：2010-03-18
申请号：US12557021
申请日：2009-09-10
申请人： Andreas Raichle , Catharina Horstmann , Frank Rosowski , Klaus Joachim Müller-Engel , Jochen Petzoldt , Ulrich Cremer
发明人： Andreas Raichle , Catharina Horstmann , Frank Rosowski , Klaus Joachim Müller-Engel , Jochen Petzoldt , Ulrich Cremer
IPC分类号： B01J21/06 , C07C45/27 , C07C255/00
CPC分类号： C07C51/252 , B01J23/002 , B01J23/8885 , B01J35/0006 , B01J35/023 , B01J37/0036 , B01J37/0221 , B01J37/34 , B01J2523/00 , C07C45/35 , C07C45/37 , C07C253/26 , Y02P20/52 , C07C47/22 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , C07C255/08
摘要： A process for producing geometric shaped catalyst bodies K whose active material is a multielement oxide of stoichiometry [BiaZ1bOx]p[BicMo12FedZ2eZ3fZ4gZ5hZ6iOy]1, in which a finely divided oxide BiaZ1bOx and, formed from element sources, a finely divided mixture of stoichiometry BicMo12FedZ2eZ3fZ4gZ5hZ6i are mixed in a ratio of p:1, this mixture is used to form shaped bodies and these are treated thermally, where 0
摘要翻译：用于生产几何形状的催化剂体K的方法，其活性材料是化学计量的多元素氧化物[BicMo12FedZ2eZ3fZ4gZ5hZ6iOy] 1，其中细分的氧化物BiaZ1bOx和由元素源形成的细分的化学计量比BicMo 12 FedZ 2eZ 3 fZ 4 gZ 5hZ 6i的混合物混合以p：1的比例，将该混合物用于形成成形体，并将它们热处理，其中0

8. 发明申请

US20080269521A1 PROCESS FOR STARTING-UP A HETEROGENEOUSLY CATALYZED PARTIAL GAS PHASE OXIDATION OF ACROLEIN TO ACRYLIC ACID OR OF METHACROLEIN TO METHACRYLIC ACID 有权
标题翻译：将异丙烯酸异丙酯与甲基丙烯酸异丙酯气相氧化反应进行甲基丙烯酸的方法
公开(公告)号：US20080269521A1
公开(公告)日：2008-10-30
申请号：US12107420
申请日：2008-04-22
申请人： Ulrich HAMMON , Thorsten Friese , Jochen Petzoldt , Klaus Joachim Muller-Engel , Ulrich Cremer , Andreas Raichle
发明人： Ulrich HAMMON , Thorsten Friese , Jochen Petzoldt , Klaus Joachim Muller-Engel , Ulrich Cremer , Andreas Raichle
IPC分类号： C07C51/235
CPC分类号： B01J8/067 , B01J23/002 , B01J23/8885 , B01J27/199 , B01J35/0006 , B01J2208/00212 , B01J2208/00221 , B01J2208/00513 , B01J2208/025 , B01J2219/30207 , B01J2219/30215 , B01J2523/00 , C07C51/235 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , B01J2523/17 , B01J2523/55 , B01J2523/15 , B01J2523/51 , B01J2523/53 , B01J2523/62
摘要： A process for starting-up a heterogeneously catalyzed partial gas phase oxidation of acrolein to acrylic acid or of methacrolein to methacrylic acid over a fixed catalyst bed disposed in a tube bundle reactor cooled by a heat exchange medium, wherein the temperature of the heat exchange medium is ≧290° C. and the temperature of that reactor plate surface which faces the reaction gas entry mixture and the temperature of the reaction gas entry mixture itself are ≦285° C.
摘要翻译：一种在由热交换介质冷却的管束反应器中的固定催化剂床上启动丙烯醛异丙烯醛至丙烯醛或甲基丙烯醛至甲基丙烯酸的非均相催化部分气相氧化方法，其中热交换介质的温度 > 290℃，反应器板表面的面对反应气体进入混合物的温度和反应气体进入混合物本身的温度<285℃。

9. 发明授权

US07129195B2 Heterogenically catalysed gas-phase partial oxidation method for precursor compounds of (meth)acrylic acid 失效
标题翻译：（甲基）丙烯酸前体化合物的异相催化气相部分氧化法
公开(公告)号：US07129195B2
公开(公告)日：2006-10-31
申请号：US10466244
申请日：2002-01-12
申请人： Raimund Felder , Signe Unverricht , Heiko Arnold , Jochen Petzoldt
发明人： Raimund Felder , Signe Unverricht , Heiko Arnold , Jochen Petzoldt
IPC分类号： B01J23/00 , B01J21/00
CPC分类号： C07C51/235 , B01J19/30 , B01J23/28 , B01J23/31 , B01J23/8876 , B01J23/8877 , B01J35/002 , B01J35/026 , B01J2219/30223 , B01J2219/30242 , B01J2219/30475 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： The invention relates to a method for the heterogenically catalyed gas-phase partial oxidation of precursor compounds of (meth)acrylic acid in a fixed catalyst bed, containing as the catalyst an activated mass of mixed oxide, shaped to form a geometric body. Said geometric body is a geometric base body, into whose surface a cavity is incorporated.
摘要翻译：本发明涉及在固定催化剂床中异构催化气相部分氧化前体化合物（甲基）丙烯酸的方法，该方法含有形成几何体的成形为混合氧化物的活化物质作为催化剂。所述几何体是几何基体，其表面中并入有空腔。

10. 发明授权

US07115776B2 Heterogeneously catalyzed gas-phase partial oxidation of at least one organic compound 有权
标题翻译：至少一种有机化合物的异相催化气相部分氧化
公开(公告)号：US07115776B2
公开(公告)日：2006-10-03
申请号：US10460153
申请日：2003-06-13
申请人： Ulrich Hammon , Jochen Petzoldt , Klaus Joachim Müller-Engel , Martin Dieterle
发明人： Ulrich Hammon , Jochen Petzoldt , Klaus Joachim Müller-Engel , Martin Dieterle
IPC分类号： C07C51/16
CPC分类号： C07C51/252 , B01J8/003 , B01J8/008 , B01J8/067 , B01J23/002 , B01J2208/00707 , B01J2208/00752 , B01J2208/00761 , B01J2523/00 , C07C51/215 , C07C57/04 , B01J2523/12 , B01J2523/13
摘要： A process for the heterogeneously catalyzed gas-phase partial oxidation of an organic compound over a fixed catalyst bed present in a fixed-bed reactor having a plurality of catalyst tubes, in which the reduction of the quality of the catalyst load with increasing duration of operation is restored by a partial catalyst change, is described.
摘要翻译：存在于具有多个催化剂管的固定床反应器中的固定催化剂床上的有机化合物的非均相催化气相部分氧化的方法，其中随着操作持续时间的延长，催化剂负载的质量降低被部分催化剂改变所恢复。

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