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1. 发明授权

US5598005A Non-destructive method for determining the extent of cure of a polymerizing material and the solidification of a thermoplastic polymer based on wavelength shift of fluroescence 失效
标题翻译：用于确定聚合材料的固化程度和基于荧光波长漂移的热塑性聚合物固化的非破坏性方法
公开(公告)号：US5598005A
公开(公告)日：1997-01-28
申请号：US389823
申请日：1995-02-15
申请人： Francis W. Wang , Robert E. Lowry , King-Fu Lin
发明人： Francis W. Wang , Robert E. Lowry , King-Fu Lin
IPC分类号： A61F2/46 , G01N21/64 , G01N33/44
CPC分类号： G01N21/648 , A61B17/8836 , G01N21/64 , A61B2017/883 , G01N33/44
摘要： The change in the peak fluorescence wavelength of a small amount of a fluorescent compound, i.e., a fluorophore, which has been dissolved in a polymerizing material or a thermoplastic polymer is used to determine the extent of cure or solidification, respectively. The measured wavelength-shift can either be compared with a previously determined correlation to obtain an absolute value for the extent of cure, or can be utilized to compare or maintain an acceptable extent of cure throughout a manufacturing or a clinical process. Similarly, in the processing of a thermoplastic polymer by injection molding, the measured wavelength shift can either be compared with a previously determined correlation to obtain an absolute value for the temperature of the polymer, or can be utilized to adjust the injection molding cycle so that the mold is opened at the optimum times. The fluorophores used in the method are preferably selected from a class of fluorophores comprising alpha, omega substituted linear alkenes having an electron accepting group attached at the alpha position and an electron donating group attached at the omega position.
摘要翻译：使用溶解在聚合材料或热塑性聚合物中的少量荧光化合物即荧光团的峰值荧光波长的变化来分别确定固化或固化的程度。测量的波长漂移可以与先前确定的相关性进行比较，以获得固化程度的绝对值，或者可以用于在整个制造或临床过程中比较或维持可接受的固化程度。类似地，在通过注射成型处理热塑性聚合物时，将测量的波长偏移与先前确定的相关性进行比较以获得聚合物温度的绝对值，或者可用于调节注射成型周期，使得模具在最佳时间打开。在该方法中使用的荧光团优选选自一类荧光团，其包括在α位置附有电子接受基团的α，ω-取代的线性烯烃和连接在ω位置的给电子基团。

2. 发明授权

US5151748A Optical sensor for the measurement of molecular orientation and viscosity of polymeric materials based on fluorescence radiation 失效
标题翻译：用于测量基于荧光辐射的聚合物材料的分子取向和粘度的光学传感器
公开(公告)号：US5151748A
公开(公告)日：1992-09-29
申请号：US563762
申请日：1990-08-07
申请人： Anthony J. Bur , Robert E. Lowry , Steven C. Roth , Charles L. Thomas , Francis W. Wang
发明人： Anthony J. Bur , Robert E. Lowry , Steven C. Roth , Charles L. Thomas , Francis W. Wang
IPC分类号： G01N1/30 , G01N11/00 , G01N21/64 , G01N33/44
CPC分类号： G01N21/6445 , G01N11/00 , G01N1/30 , G01N2021/6439 , G01N33/44
摘要： A method of measuring fluid properties of a polymer melt, undergoing shear and/or extensional flow which utilizes fluorescent anisotropy. The method utilizes a polymeric chromophore which includes a bifunctional anthracene that is covalently bonded to polybutadiene. The invention also involves an optical probe which is designed to be inserted into existing temperature and/or pressure probe ports in processing equipment. The probe includes a rotatable polarizer and emission collection fibers.
摘要翻译：测量聚合物熔体的流体性质的方法，其经历使用荧光各向异性的剪切和/或拉伸流动。该方法使用包含共价键合到聚丁二烯的双功能蒽的聚合物发色团。本发明还涉及一种光学探针，其被设计成插入到处理设备中的现有温度和/或压力探测端口中。探头包括可旋转的偏振器和排出物收集纤维。

3. 发明授权

US5384079A Method for detecting thermodynamic phase transitions during polymer injection molding 失效
标题翻译：聚合物注射成型过程中热力学相变的检测方法
公开(公告)号：US5384079A
公开(公告)日：1995-01-24
申请号：US1728
申请日：1993-01-06
申请人： Anthony J. Bur , Francis W. Wang , Charles L. Thomas , Joseph L. Rose
发明人： Anthony J. Bur , Francis W. Wang , Charles L. Thomas , Joseph L. Rose
IPC分类号： B29C45/76 , G01N21/64
CPC分类号： G01N21/643 , B29C45/76
摘要： A method is provided for measuring the onset of polymer solidification, i phase transitions from liquid to crystal or liquid to glass, during injection molding to detect characteristic fluorescence radiation from a dye which has been doped into the polymer at very low concentration. The method involves the use of a calibration relationship between the fluorescence intensity and temperature of the doped polymer in order to determine distinct features which characterize the onset of solidification.
摘要翻译：提供了一种用于测量聚合物固化的开始的方法，即在注射模塑期间从液体到晶体或液体到玻璃的相变，以检测以非常低的浓度掺杂到聚合物中的染料的特征性荧光辐射。该方法涉及使用掺杂聚合物的荧光强度和温度之间的校准关系，以确定表征固化开始的不同特征。

4. 发明申请

US20090096133A1 MICROPATTERNING OF BIOLOGICAL MOLECULES USING LASER ABLATION 有权
标题翻译：使用激光消除微生物生物分子的微波
公开(公告)号：US20090096133A1
公开(公告)日：2009-04-16
申请号：US12249824
申请日：2008-10-10
申请人： Andrew D. Doyle , Kenneth M. Yamada , Francis W. Wang
发明人： Andrew D. Doyle , Kenneth M. Yamada , Francis W. Wang
IPC分类号： B29C59/16
CPC分类号： B29C59/16 , B01J2219/00441 , B01J2219/00527 , B01J2219/00596 , B01J2219/00605 , B01J2219/00612 , B01J2219/00617 , B01J2219/00619 , B01J2219/00637 , B01J2219/00639 , B01J2219/00722 , B01J2219/00725 , B01J2219/0074 , B01J2219/00743 , B29C2059/023 , B29C2791/009 , B29K2995/0092
摘要： The present invention employs the natural hydrophilic properties of a macromolecular film such as a hydrogel and in combination with localized photo-ablation of monolayers created with the hydrogel using multi-photon laser excitation, provides a stampless, versatile method of micropattern fabrication.
摘要翻译：本发明采用大分子膜如水凝胶的天然亲水性质，并结合使用多光子激光激发由水凝胶产生的单层局部光消融，提供了一种无模式，通用的微图案制作方法。

5. 发明授权

US08048641B2 Micropatterning of biological molecules using laser ablation 有权
标题翻译：使用激光消融的生物分子的微图案化
公开(公告)号：US08048641B2
公开(公告)日：2011-11-01
申请号：US12249824
申请日：2008-10-10
申请人： Andrew D. Doyle , Kenneth M. Yamada , Francis W. Wang
发明人： Andrew D. Doyle , Kenneth M. Yamada , Francis W. Wang
IPC分类号： G01N31/00 , G01N33/53
CPC分类号： B29C59/16 , B01J2219/00441 , B01J2219/00527 , B01J2219/00596 , B01J2219/00605 , B01J2219/00612 , B01J2219/00617 , B01J2219/00619 , B01J2219/00637 , B01J2219/00639 , B01J2219/00722 , B01J2219/00725 , B01J2219/0074 , B01J2219/00743 , B29C2059/023 , B29C2791/009 , B29K2995/0092
摘要： The present invention employs the natural hydrophilic properties of a macromolecular film such as a hydrogel and in combination with localized photo-ablation of monolayers created with the hydrogel using multi-photon laser excitation, provides a stampless, versatile method of micropattern fabrication.
摘要翻译：本发明采用大分子膜如水凝胶的天然亲水性质，并结合使用多光子激光激发由水凝胶产生的单层局部光消融，提供了一种无模式，通用的微图案制作方法。

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