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1. 发明授权

US06919418B2 Approach to reduce cyclics formation in 3-CIPA based polyetherimide polymers 有权
标题翻译：减少3-CIPA聚醚酰亚胺聚合物中周期形成的方法
公开(公告)号：US06919418B2
公开(公告)日：2005-07-19
申请号：US10647679
申请日：2003-08-25
申请人： Farid Fouad Khouri , Daniel Joseph Brunelle , Donald Scott Johnson
发明人： Farid Fouad Khouri , Daniel Joseph Brunelle , Donald Scott Johnson
IPC分类号： C07D209/48 , C08G73/12 , C08G73/10 , C07D209/00 , C08G65/40 , C08G69/26
CPC分类号： C07D209/48 , C08G73/12 , C08G73/124
摘要： Methods of reducing the amount of undesirable cyclic oligomer by-products in the production of polyetherimides are disclosed. The resulting polyetherimides have enhanced thermomechanical properties.
摘要翻译：公开了减少聚醚酰亚胺生产中不期望的环状低聚物副产物量的方法。得到的聚醚酰亚胺具有增强的热机械性能。

2. 发明授权

US07714095B2 Phase transfer catalyzed method for preparation of polyetherimides 有权
标题翻译：相转移催化聚醚酰亚胺的制备方法
公开(公告)号：US07714095B2
公开(公告)日：2010-05-11
申请号：US11363681
申请日：2006-02-28
申请人： Daniel Joseph Brunelle , Havva Yagci Acar , Farid Fouad Khouri , Thomas Link Guggenheim , David Winfield Woodruff , Norman Enoch Johnson
发明人： Daniel Joseph Brunelle , Havva Yagci Acar , Farid Fouad Khouri , Thomas Link Guggenheim , David Winfield Woodruff , Norman Enoch Johnson
IPC分类号： C08G73/00 , C08G73/10 , C08G8/02 , C08G14/00
CPC分类号： C08G73/12 , C08G73/121 , C08G73/124
摘要： Polyether polymers, such as polyetherimides, are prepared by the reaction of a dihydroxy-substituted aromatic hydrocarbon alkali metal salt, such as bisphenol A disodium salt, with a bis(N-(chlorophthalimido))aromatic compound, such as 1,3- and/or 1,4-bis(N-(4-chlorophthalimido))benzene, in a solvent such as o-dichlorobenzene and in the presence of a phase transfer catalyst such as a hexaalkylguanidinium chloride. Several embodiments may be employed to improve the method. They comprise employing substantially dry reagents, employing a high solids level in solvent, beginning with an excess of bis(N-(chlorophthalimido))-aromatic compound and incrementally adding alkali metal salt, employing alkali metal salt of small particle size, and using reagents of high purity.
摘要翻译：聚醚聚合物如聚醚酰亚胺通过二羟基取代的芳族烃碱金属盐如双酚A二钠盐与双（N-（氯代邻苯二甲酰亚胺基））芳族化合物如1,3-和 /或1,4-双（N-（4-氯邻苯二甲酰亚氨基））苯，在溶剂如邻二氯苯中，并在相转移催化剂如六烷基氯化the存在下进行。可以采用几个实施例来改进该方法。它们包括使用基本上干的试剂，在溶剂中使用高固体含量，从过量的双（N-（氯代邻苯二甲酰亚胺基）） - 芳族化合物开始，并逐渐加入碱金属盐，使用小粒径的碱金属盐，并使用试剂的高纯度。

3. 发明授权

US07273919B1 High heat polyethersulfone compositions 有权
标题翻译：高热聚醚砜组合物
公开(公告)号：US07273919B1
公开(公告)日：2007-09-25
申请号：US11286181
申请日：2005-11-21
申请人： Daniel Steiger , Farid Fouad Khouri , Daniel Joseph Brunelle , Amy Beth Koren
发明人： Daniel Steiger , Farid Fouad Khouri , Daniel Joseph Brunelle , Amy Beth Koren
IPC分类号： C08G75/00 , C08G61/02 , C08G65/38 , C08G65/40
CPC分类号： C08G75/23
摘要： High heat polyethersulfone compositions are provided which possess unexpectedly high glass transition temperatures. The polyethersulfone compositions comprise structural units derived from phthalimide bisphenols such as 3,3-bis(4 -hydroxyphenyl)-N-phenylphthalimide, and structural units derived from at least one biphenyl-bissulfone such as 4,4′-bis((4-chlorophenyl)sulfonyl)-1,1′-biphenyl. The novel polyethersulfone compositions may further comprise structural units derived from one or more biphenols such as 4,4′-biphenol, bisphenols such as BPA, or other electrophilic sulfone monomers, such as bis(4-chlorophenyl)sulfone. In one embodiment, the polyethersulfone composition of the present invention comprises structural groups derived exclusively from 3,3-bis(4-hydroxyphenyl)-N-phenylphthalimide, and 4,4′-bis((4-chlorophenyl)sulfonyl)-1,1′-biphenyl and exhibits a single glass transition of greater than 300° C.
摘要翻译：提供了具有出人意料的高玻璃化转变温度的高热聚醚砜组合物。聚醚砜组合物包含衍生自邻苯二甲酰亚胺双酚的结构单元，例如3,3-双（4-羟基苯基）-N-苯基邻苯二甲酰亚胺，以及衍生自至少一种联苯基 - 砜的结构单元，例如4,4'-双（（4- 氯苯基）磺酰基）-1,1'-联苯。新型聚醚砜组合物还可以包含衍生自一种或多种双酚的结构单元，例如4,4'-联苯酚，双酚如BPA或其它亲电子砜单体如双（4-氯苯基）砜。在一个实施方案中，本发明的聚醚砜组合物包含仅由3,3-双（4-羟基苯基）-N-苯基邻苯二甲酰亚胺衍生的结构基团和4,4'-双（（4-氯苯基）磺酰基） 1'-联苯并且表现出大于300℃的单一玻璃化转变。

4. 发明授权

US07115785B2 Method for making salts hydroxy-substituted hydrocarbons 有权
标题翻译：盐的制备方法羟基取代的烃
公开(公告)号：US07115785B2
公开(公告)日：2006-10-03
申请号：US10647890
申请日：2003-08-25
申请人： Thomas Link Guggenheim , Daniel Joseph Brunelle , David Winfield Woodruff , Lee Harris Bergman , Norman Enoch Johnson , Matthew Hal Littlejohn , Farid Fouad Khouri
发明人： Thomas Link Guggenheim , Daniel Joseph Brunelle , David Winfield Woodruff , Lee Harris Bergman , Norman Enoch Johnson , Matthew Hal Littlejohn , Farid Fouad Khouri
IPC分类号： C07C37/68 , C07C39/16
CPC分类号： C07C37/70 , C07C37/66 , C07C39/235
摘要： Disclosed is a method for preparing an alkali metal salt of a hydroxy-substituted hydrocarbon which comprises the steps of (i) contacting in solvent media at least one hydroxy-substituted hydrocarbon with a base comprising an alkali metal cation; and (ii) devolatilizing the solvent media comprising alkali metal salt by adding or spraying the solvent media into a substantially water-immiscible organic solvent, said solvent being at a temperature greater than the boiling point of solvent media at the prevailing pressure. In one embodiment the solvent media comprises water, and optionally at least one water-soluble protic organic solvent.
摘要翻译：公开了一种制备羟基取代烃的碱金属盐的方法，其包括以下步骤：（i）在溶剂介质中使至少一种羟基取代的烃与包含碱金属阳离子的碱接触; 和（ii）通过将溶剂介质加入或喷雾到基本上与水不混溶的有机溶剂中来使包含碱金属盐的溶剂介质脱挥发分，所述溶剂的温度大于溶剂介质在当前压力下的沸点。在一个实施方案中，溶剂介质包含水和任选的至少一种水溶性质子有机溶剂。

5. 发明授权

US06849706B1 Copolyetherimides 有权
标题翻译：共聚酰亚胺
公开(公告)号：US06849706B1
公开(公告)日：2005-02-01
申请号：US10647888
申请日：2003-08-25
申请人： Daniel Joseph Brunelle , Havva Yagci Acar , Farid Fouad Khouri , William David Richards
发明人： Daniel Joseph Brunelle , Havva Yagci Acar , Farid Fouad Khouri , William David Richards
IPC分类号： C08G73/12 , C08G73/00
CPC分类号： C08G73/123 , C08G73/124 , C08G73/125
摘要： Copolyetherimides comprise phthalimide structural units comprising both 3- and 4-linkages, wherein the designations 3-linkage and 4-linkage refer to the isomeric positions on the phthalimide ring in the totality of phthalimide-comprising structural units in the copolymer. The products have excellent properties, including high glass transition and heat distortion temperatures, high ductility and good melt flow properties, and low polydispersity.
摘要翻译：共聚酰亚胺包括包含3-和4-键的邻苯二甲酰亚胺结构单元，其中3-键和4-键的名称是指共聚物中邻苯二甲酰亚胺包含的结构单元总共在邻苯二甲酰亚胺环上的异构位置。该产品具有优异的性能，包括高玻璃化转变和热变形温度，高延展性和良好的熔体流动性能，以及低的多分散性。

6. 发明授权

US07902316B2 Polyethersulfone composition, method of making and articles therefrom 有权
标题翻译：聚醚砜组合物，制造方法和制品
公开(公告)号：US07902316B2
公开(公告)日：2011-03-08
申请号：US11388710
申请日：2006-03-24
申请人： Donald Scott Johnson , Daniel Steiger , Daniel Joseph Brunelle , Sean Elliot Armstrong
发明人： Donald Scott Johnson , Daniel Steiger , Daniel Joseph Brunelle , Sean Elliot Armstrong
IPC分类号： C08G75/23 , C08G75/00 , C08G75/20
CPC分类号： C08G65/40 , C08G75/23 , C08L71/10 , C08L81/06
摘要： A polyethersulfone composition is disclosed which comprises structural units derived from bisphenol-A and 4,4′-biphenol, the structural units derived from 4,4′-biphenol being present in an amount corresponding to greater than 65 mole percent based on total moles of structural units derived from diphenolic monomers, wherein the polyethersulfone has a weight average molecular weight (Mw) of at least 54,000 grams per mole as measured by gel permeation chromatography. The polyethersulfone compositions of the invention display outstanding impact strength as measured using ASTM D256. Surprisingly, the polyethersulfone compositions of the invention show enhanced impact strength relative to known polyethersulfones such as RADEL R, a commercially available polyethersulfone engineering thermoplastic comprised of structural units derived from a dihalodiarylsulfone and 4,4′-biphenol and having a Notched Izod impact strength of about 700 Joules per meter.
摘要翻译：公开了一种聚醚砜组合物，其包含衍生自双酚A和4,4'-联苯酚的结构单元，衍生自4,4'-联苯酚的结构单元的存在量相当于基于总共摩尔数衍生自二元酚单体的结构单元，其中聚醚砜的重均分子量（Mw）通过凝胶渗透色谱法测定为至少54,000克/摩尔。本发明的聚醚砜组合物显示出优异的冲击强度，使用ASTM D256测量。令人惊奇的是，本发明的聚醚砜组合物相对于已知的聚醚砜如RADEL R显示出增强的冲击强度，RADEL R是由二卤代芳基砜和4,4'-联苯酚衍生的结构单元的市售聚醚砜工程热塑性塑料，其具有缺口伊佐德冲击强度约700焦耳/米。

7. 发明授权

US07705190B2 Method of making an aromatic polyether composition using phosphazenium salt phase transfer catalysts 失效
标题翻译：使用磷腈鎓盐相转移催化剂制备芳族聚醚组合物的方法
公开(公告)号：US07705190B2
公开(公告)日：2010-04-27
申请号：US11651167
申请日：2007-01-09
申请人： Daniel Joseph Brunelle
发明人： Daniel Joseph Brunelle
IPC分类号： C07C41/00
CPC分类号： B01J31/0239 , B01J31/0265 , B01J31/0268 , B01J2231/14 , B01J2231/40 , B01J2531/98 , C07C41/16 , C07C315/04 , C07F9/067 , C08G65/4087 , C08G79/025 , C07C317/22 , C07C43/29
摘要： A method for carrying out a chemical reaction between at least two reactants occupying separate phases within a multiphase reaction mixture has been discovered in which at least one phosphazenium salt is employed as a phase transfer catalyst. The remarkable utility of phosphazenium salts as phase transfer catalysts is illustrated by the preparation of aromatic ethers. The phosphazenium salt phase transfer catalysts are shown to be especially useful in the preparation of aromatic polyethers such as polyether sulfones.
摘要翻译：已经发现在多相反应混合物中在至少两种占据分离相的反应物之间进行化学反应的方法，其中使用至少一种磷氮烯基鏻盐作为相转移催化剂。通过制备芳族醚来说明磷氮烯基鏻盐作为相转移催化剂的显着效用。显示磷氮烯基鏻盐相转移催化剂特别可用于制备芳族聚醚如聚醚砜。

8. 发明申请

US20080269396A1 TELECHELIC POLYESTER/POLYCARBONATE/ORGANOCLAY NANOCOMPOSITES, AND RELATED METHODS AND ARTICLES 有权
标题翻译：电话聚酯/聚碳酸酯/有机硅纳米复合材料及相关方法和文章
公开(公告)号：US20080269396A1
公开(公告)日：2008-10-30
申请号：US11966051
申请日：2007-12-28
申请人： Sreepdaraj Karanam , Robert Lee Sherman , Ganesh Kannan , Steven James Montgomery , Daniel Joseph Brunelle , Enrico Binassi
发明人： Sreepdaraj Karanam , Robert Lee Sherman , Ganesh Kannan , Steven James Montgomery , Daniel Joseph Brunelle , Enrico Binassi
IPC分类号： C08K3/34
CPC分类号： C08L69/00 , C08K3/346 , C08K9/04 , C08L21/00 , C08L51/00 , C08L55/02 , C08L67/02 , C08L2666/02
摘要： A composition comprises, based on the total weight of the composition, from 30 to 50 weight percent of an ionomeric telechelic polyalkylene ester comprising from 0.05 to 5 mole percent of sulfonate end groups; from 50 to 70 weight percent of a polycarbonate; from 0.1 to 10 weight percent of an organoclay; and from 2 to 12 weight percent of an impact modifier.
摘要翻译：组合物基于组合物的总重量包含30至50重量％的包含0.05至5摩尔％磺酸酯端基的离聚物遥爪聚亚烷基酯; 50-70重量％的聚碳酸酯; 0.1至10重量％的有机粘土; 和2至12重量％的抗冲改性剂。

9. 发明授权

US07381331B2 Hydrophilic membrane and associated method 失效
标题翻译：亲水膜及相关方法
公开(公告)号：US07381331B2
公开(公告)日：2008-06-03
申请号：US11241227
申请日：2005-09-30
申请人： Hieu Minh Duong , Hongyi Zhou , Rainer Koeniger , Daniel Joseph Brunelle , Daniel Robert Olson , Karmin Lorraine Olson
发明人： Hieu Minh Duong , Hongyi Zhou , Rainer Koeniger , Daniel Joseph Brunelle , Daniel Robert Olson , Karmin Lorraine Olson
IPC分类号： B01D39/00 , B01D39/14 , B01D71/14 , B01D29/00 , B01D63/00
CPC分类号： B01D67/0088 , B01D67/0093 , B01D71/36 , B01D71/38 , B01D71/44 , B01D2323/02 , B01D2323/30 , B01D2323/32 , B01D2325/36 , H01M8/1027 , H01M8/103 , H01M8/1053 , H01M8/1058 , H01M8/1081 , H01M10/0565 , H01M2300/0082 , Y02P70/56
摘要： A membrane is provided, which may include a microporous base membrane; and a cross-linkable coating disposed on a surface of the membrane. The coating may include polyvinyl nucleophilic polymer and a urethane or a blocked isocyanate. The coating may be cross-linked. Also provided is a method of making the membrane.
摘要翻译：提供膜，其可以包括微孔基膜; 以及设置在膜的表面上的可交联涂层。涂层可以包括聚乙烯基亲核聚合物和聚氨酯或封端的异氰酸酯。涂层可以是交联的。还提供了制造膜的方法。

10. 发明授权

US06828410B2 Method for preparing poly(cyclohexane-1,4-dicarboxylate)s from cyclohexane-1,4-dicarboxylic acid, and composition 有权
标题翻译：由环己烷-1,4-二羧酸制备聚（环己烷-1,4-二羧酸酯）的方法及其组合物
公开(公告)号：US06828410B2
公开(公告)日：2004-12-07
申请号：US10192579
申请日：2002-07-10
申请人： Daniel Joseph Brunelle , Corrado Berti , Annamaria Celli , Martino Colonna , Maurizio Fiorini , Elisabetta Marianucci , Massimo Messori , Francesco Pilati , Laura Sisti , Paola Marchese
发明人： Daniel Joseph Brunelle , Corrado Berti , Annamaria Celli , Martino Colonna , Maurizio Fiorini , Elisabetta Marianucci , Massimo Messori , Francesco Pilati , Laura Sisti , Paola Marchese
IPC分类号： C08G6300
CPC分类号： C08G63/199 , C08G63/78 , C08G63/82
摘要： Poly(1,4-cyclohexanedicarboxylate)s, especially poly(1,4-cyclohexanedimethylene-1,4-cyclohexanedicarboxylate), are prepared from at least one relatively non-volatile diol, such as 1,4-cyclohexanedimethanol, and cyclohexane-1,4-dicarboxylic acid by an esterification process in the presence of a catalyst, at a maximum temperature of about 260°. In one embodiment the procedure employs a two-step process, the second of which may be performed in the melt or in the solid state. A volatile diol such as ethylene glycol may also be present.
摘要翻译：聚（1,4-环己烷二羧酸酯），特别是聚（1,4-环己烷二亚甲基-1,4-环己烷二羧酸酯），由至少一种相对不挥发的二醇如1,4-环己烷二甲醇和环己烷-1 在催化剂存在下，通过酯化方法，在约260℃的最高温度下进行。在一个实施方案中，该方法采用两步法，其中第二步可以在熔体中或在固态下进行。也可以存在挥发性二醇如乙二醇。

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