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1. 发明授权

US5106906A Process for the production of finely dispersed polymer mixtures 失效
标题翻译：生产精细分散聚合物混合物的方法
公开(公告)号：US5106906A
公开(公告)日：1992-04-21
申请号：US411082
申请日：1989-09-22
申请人： Erich Meier , Hanns-Ingolf Paul , Rudiger Plaetschke , Gunther Weymanns
发明人： Erich Meier , Hanns-Ingolf Paul , Rudiger Plaetschke , Gunther Weymanns
IPC分类号： B01F3/08 , B01F3/18 , B01F3/20 , B29B7/82 , B29B7/86 , B29B13/00 , B29B13/02 , C08J3/00
CPC分类号： B29B7/82 , B01F3/0803 , B29B13/00 , B29B13/022 , C08J3/005 , B01F2003/0064 , B01F2003/0892 , Y02P20/544
摘要： 37 Highly dispersed mixtures of at least two polymers which are not completely miscible in the melt under customary conditions are produced by melting the polymers used in the presence of supercritical gases or mixtures of gases, intensively thoroughly mixing the molten polymers for long enough until the viscosity of the melt has diminished by at least 10%, subsequently cooling the polymer melt with further thorough mixing, until the viscosity of the melt has at least reached the original value again and then depressurizing the polymer melt. The highly dispersed mixtures produced in this way can be processed in the customary manner into mouldings.
摘要翻译：通常在超临界气体或气体混合物的存在下熔化聚合物，使熔融聚合物充分混合足够长的时间，直到粘度达到最高，从而产生在常规条件下不完全混溶在熔体中的至少两种聚合物的高分散混合物的熔体已经减少至少10％，随后进一步充分混合冷却聚合物熔体，直到熔体的粘度至少达到原始值，然后使聚合物熔体减压。以这种方式生产的高度分散的混合物可以以常规方式加工成模制品。

2. 发明授权

US09512240B2 Process for the production of water and solvent-free polymers 有权
标题翻译：生产水和无溶剂聚合物的方法
公开(公告)号：US09512240B2
公开(公告)日：2016-12-06
申请号：US13063227
申请日：2009-09-17
申请人： Jörg Kirchhoff , Werner Bäcker , Rolf Feller , Paul Wagner , John Lovegrove , Hanns-Ingolf Paul
发明人： Jörg Kirchhoff , Werner Bäcker , Rolf Feller , Paul Wagner , John Lovegrove , Hanns-Ingolf Paul
IPC分类号： B29C47/76 , C08C2/00 , C01B5/00 , C08F6/00 , B29C47/36 , B29C47/38 , B29C47/60 , B29C47/62 , B29B7/74
CPC分类号： C08C2/00 , B29B7/7485 , B29C47/364 , B29C47/38 , B29C47/6056 , B29C47/62 , C01B5/00 , C08F6/003 , C08L23/283
摘要： The present invention relates to water and solvent-free polymers, in particular water and solvent-free synthetic rubber products like non-halogenated and halogenated butyl rubber products as well as a process for the production thereof. The invention further relates to a device suitable to accomplish said process.
摘要翻译：本发明涉及无水和无溶剂的聚合物，特别是无水和无溶剂的合成橡胶产品，如非卤化和卤化丁基橡胶产品，以及其生产方法。本发明还涉及适合于完成所述过程的装置。

3. 发明授权

US08975361B2 Process for the production of water and solvent-free polymers 有权
标题翻译：生产水和无溶剂聚合物的方法
公开(公告)号：US08975361B2
公开(公告)日：2015-03-10
申请号：US13635781
申请日：2011-03-23
申请人： Wolfgang Krumbe , Rolf Feller , Paul Wagner , Hanns-Ingolf Paul , Martin Siebuerger , Heike Kloppenburg , Alicia Le-Sattler , John Lovegrove
发明人： Wolfgang Krumbe , Rolf Feller , Paul Wagner , Hanns-Ingolf Paul , Martin Siebuerger , Heike Kloppenburg , Alicia Le-Sattler , John Lovegrove
IPC分类号： C08G63/02 , C08L9/00 , C08F6/10 , C08F6/12 , C08C2/00 , C08G64/00
CPC分类号： C08F6/10 , C08C2/00 , C08F6/12 , C08L9/00
摘要： The present invention relates to water and solvent-free polymers, in particular water and solvent-free synthetic rubber products like styrene butadiene rubber products and butadiene rubber products as well as a process for the production thereof. The invention further relates to a device suitable to accomplish said process.
摘要翻译：本发明涉及无水和无溶剂的聚合物，特别是无溶剂的合成橡胶产品，如丁苯橡胶产品和丁二烯橡胶产品，以及其生产方法。本发明还涉及适合于完成所述过程的装置。

4. 发明申请

US20140309362A1 PROCESS FOR PRODUCING BROMINATED BUTYL RUBBER 有权
标题翻译：生产丁二烯橡胶的方法
公开(公告)号：US20140309362A1
公开(公告)日：2014-10-16
申请号：US14233548
申请日：2012-07-17
申请人： Ricarda Leiberich , Joachim Ritter , Hanns-Ingolf Paul , Udo Wiesner , Holger Luesgen
发明人： Ricarda Leiberich , Joachim Ritter , Hanns-Ingolf Paul , Udo Wiesner , Holger Luesgen
IPC分类号： C08K5/01 , C09J11/06 , C09D7/12
CPC分类号： C08K5/01 , C08F8/22 , C09D7/63 , C09D115/02 , C09J11/06 , C09J115/02 , C08F210/12
摘要： The invention relates to an energy efficient, environmentally favourable process for the preparation of brominated butyl rubbers, that uses a bromination agent and a oxidizing agent in order to enhance the utilization of bromine contained in the bromination agent. In a preferred embodiment a common medium for both solution polymerization and subsequent bromination of the rubber is employed.
摘要翻译：本发明涉及使用溴化剂和氧化剂制备溴化丁基橡胶的能量有效，环境友好的方法，以便增强溴化剂中所含的溴的利用。在优选的实施方案中，采用用于溶液聚合和随后的橡胶溴化的常用介质。

5. 发明申请

US20140058050A1 ACTIVITY MONITORING AND POLYMERIZATION PROCESS CONTROL 有权
标题翻译：活动监测和聚合过程控制
公开(公告)号：US20140058050A1
公开(公告)日：2014-02-27
申请号：US13878255
申请日：2011-09-23
申请人： Ursula Tracht , Ricarda Leiberich , Michael Berger , Hanns-Ingolf Paul , Udo Wiesner
发明人： Ursula Tracht , Ricarda Leiberich , Michael Berger , Hanns-Ingolf Paul , Udo Wiesner
IPC分类号： C08F236/08
CPC分类号： C08F236/08 , B01J19/0033 , B01J19/18 , B01J2219/00164 , B01J2219/00186 , B01J2219/00198 , B01J2219/00209 , B01J2219/00231 , C08F210/12 , C08F2400/02 , C08F2/00
摘要： The present invention relates to a method to control a liquid feed stream carried out by measuring at least one spectrum of the liquid feed stream comprising an initiator or catalyst, determining its activity using a predictive model on the basis of said spectrum and adjusting the feed streams and/or the preparation conditions of the feed stream comprising the initiators or catalysts in order to attain or maintain a desired level of total activity. In a further aspect the invention relates to a controlled process for the preparation of polymers in a polymerization reactor by contacting liquid feed streams comprising monomers and initiators or catalysts, whereby the control of the feed streams entering the polymerization reactor and/or the initiator or catalyst preparation is carried out by measuring at least one spectrum of the liquid feed stream comprising an initiator or catalyst, determining its activity using a predictive model on the basis of said spectrum and adjusting the feed streams and/or the preparation conditions of the feed stream comprising the initiators or catalysts in order to attain or maintain a desired level of total activity within the polymerization reactor. More particularly, the invention relates to a method for controlling the activity of aluminium containing initiators in a process for the co-polymerisation of isolefins and multiolefins, in particular isobutylene and isoprene. The present invention further to device and a chemical plant suitable to operate said process.
摘要翻译：本发明涉及一种控制液体进料流的方法，所述方法是通过测量包含引发剂或催化剂的至少一个光谱的液体进料物流，使用基于所述光谱的预测模型确定其活性并调节进料流和/或包含引发剂或催化剂的进料流的制备条件以获得或保持期望的总活性水平。在另一方面，本发明涉及通过使包含单体和引发剂或催化剂的液体进料流接触而在聚合反应器中制备聚合物的受控方法，由此控制进入聚合反应器和/或引发剂或催化剂的进料流通过测量包含引发剂或催化剂的液体进料流的至少一个谱线，基于所述光谱使用预测模型确定其活性并调节进料流和/或进料流的制备条件来进行制备，所述进料流和/ 引发剂或催化剂，以获得或保持聚合反应器内所需的总活性水平。更具体地说，本发明涉及在异烯烃和多烯烃，特别是异丁烯和异戊二烯的共聚合方法中控制含铝引发剂的活性的方法。本发明还涉及适用于操作所述方法的装置和化学设备。

6. 发明申请

US20140039142A1 EXTRUDER WITH INTEGRATED DIE PLATE AND METHOD FOR DEGASING POLYMER MIXTURES 有权
标题翻译：具有整体式切片机的挤出机和用于降低聚合物混合物的方法
公开(公告)号：US20140039142A1
公开(公告)日：2014-02-06
申请号：US13811330
申请日：2011-07-22
申请人： Hanns-Ingolf Paul , Udo Wiesner , Jörg Kirchhoff , Thomas König , Klemens Kohlgrüber
发明人： Hanns-Ingolf Paul , Udo Wiesner , Jörg Kirchhoff , Thomas König , Klemens Kohlgrüber
IPC分类号： B29B7/84
CPC分类号： B29B7/845 , B29C47/0009 , B29C47/0871 , B29C47/1063 , B29C47/40 , B29C47/404 , B29C47/6031 , B29C47/6056 , B29C47/6062 , B29C47/62 , B29C47/762 , B29C47/763 , B29C47/767 , B29K2023/083 , B29K2023/22 , B29K2105/0005
摘要： The invention is directed to an extruder (10), particularly for extruding a synthetic rubber product, which comprises a barrel (24), one or several extruder elements (12, 14), particularly one or several extruder screws and/or a kneader elements (14), arranged inside the barrel (24) for conveying the product, optionally an inlet port for feeding a stripping agent into the barrel (24) and an outlet port for removing volatile compounds from the product and, where applicable, the stripping agent. According to the invention a perforated die plate (26) is fixed to the barrel (24) in flow direction before the outlet port. Since the die plate (26) is not fixed to the extruder elements (12, 14) but to the barrel (24) a circumferential clearance between the die plate (26) and the barrel (24) is prevented so that no extruded material is passing the die plate (26) radially outside. Parts of the extruded material comprising a low surface area to volume ratio are prevented so that the evaporation of volatile compounds is facilitated.
摘要翻译：本发明涉及挤出机（10），特别是用于挤出合成橡胶产品，其包括桶（24），一个或多个挤出机元件（12,14），特别是一个或多个挤出机螺杆和/或捏合元件（14），布置在所述筒体（24）内用于输送所述产品，任选地用于将汽提剂进料到所述筒体（24）中的入口和用于从所述产品中除去挥发性化合物的出口端口，以及在适用的情况下，所述汽提剂。根据本发明，穿孔模板（26）在出口之前沿流动方向固定到筒体（24）。由于模板（26）不固定到挤出机元件（12,14）而是固定到筒体（24）上，因此防止了模板（26）和筒体（24）之间的周向间隙，使得不挤出材料径向地穿过模板（26）。防止包含低表面积与体积比的挤出材料的部分，从而促进挥发性化合物的蒸发。

7. 发明授权

US06307028B1 Chromatographic method for high yield purification and viral inactivation of antibodies 有权
标题翻译：用于高产率纯化和病毒灭活抗体的色谱法
公开(公告)号：US06307028B1
公开(公告)日：2001-10-23
申请号：US09270724
申请日：1999-03-17
申请人： Wytold Lebing , Patricia Alred , Douglas C. Lee , Hanns-Ingolf Paul
发明人： Wytold Lebing , Patricia Alred , Douglas C. Lee , Hanns-Ingolf Paul
IPC分类号： C07K136
CPC分类号： A61L2/0088 , A61L2/18 , A61L2/23 , C07K16/065
摘要： An improved process for the purification of antibodies from human plasma or other sources is disclosed. The process involves suspension of the antibodies at pH 3.8 to 4.5 followed by addition of caprylic acid and a pH shift to pH 5.0 to 5.2. A precipitate of contaminating proteins, lipids and caprylate forms and is removed, while the majority of the antibodies remain in solution. Sodium caprylate is again added to a final concentration of not less than about 15 mM. This solution is incubated for 1 hour at 25° C. to effect viral inactivation. A precipitate (mainly caprylate) is removed and the clear solution is diluted with purified water to reduce ionic strength. Anion exchange chromatography using two different resins is utilized to obtain an exceptionally pure IgG with subclass distribution similar to the starting distribution. The method maximizes yield and produces a gamma globulin with greater than 99% purity. The resin columns used to obtain a high yield of IgG, retain IgM and IgA, respectively. IgA and IgM may be eluted in high yield and purity.
摘要翻译：公开了一种用于从人血浆或其他来源纯化抗体的改进方法。该方法包括将抗体在pH 3.8至4.5下悬浮，然后加入辛酸，并将pH转变至pH5.5至5.2。污染蛋白质，脂质和辛酸盐形式的沉淀物被除去，而大多数抗体保留在溶液中。再加入辛酸钠，终浓度不低于约15mM。将该溶液在25℃孵育1小时以进行病毒灭活。除去沉淀物（主要是辛酸盐），并用净化水稀释澄清溶液以降低离子强度。使用两种不同树脂的阴离子交换色谱法获得特异纯的IgG，其亚类分布类似于起始分布。该方法使产量最大化，产生纯度高于99％的γ球蛋白。用于获得高产量的IgG的树脂柱分别保留IgM和IgA。可以以高产率和纯度洗脱IgA和IgM。

8. 发明授权

US5229486A Process for isolating polymers from their solvents using liquids containing carbon dioxide 失效
标题翻译：使用含有二氧化碳的液体从其溶剂中分离聚合物的方法
公开(公告)号：US5229486A
公开(公告)日：1993-07-20
申请号：US805424
申请日：1991-12-11
申请人： Hanns-Ingolf Paul , Rolf Treckmann , Gunther Weymans , Jurgen Kirsch , Jurgen Heuser , Klaus Elgeti
发明人： Hanns-Ingolf Paul , Rolf Treckmann , Gunther Weymans , Jurgen Kirsch , Jurgen Heuser , Klaus Elgeti
IPC分类号： C08G63/89 , C08G64/40 , C08G85/00 , C08J3/00 , C08J3/14
CPC分类号： C08G85/00 , C08G63/89 , C08G64/403
摘要： A process for isolating polymers from their solvents by addition of fluids containing carbon dioxide at temperatures of 30.degree. to 280.degree. C. and under pressures of 1 to 1,000 bar is disclosed. The process is characterized in that the concentration of the polymers in their solvents is between 5% and 80% by weight and the fluid containing carbon dioxide consists of at least 50% by weight carbon dioxide.
摘要翻译：公开了一种通过在30℃至280℃的温度和1至1,000巴的压力下加入含有二氧化碳的流体从其溶剂中分离聚合物的方法。该方法的特征在于聚合物在其溶剂中的浓度为5重量％至80重量％，含有二氧化碳的流体由至少50重量％的二氧化碳组成。

9. 发明授权

US09273154B2 Process for production of halobutyl ionomers 有权
标题翻译：卤代丁基离聚物的制备方法
公开(公告)号：US09273154B2
公开(公告)日：2016-03-01
申请号：US13522757
申请日：2011-01-17
申请人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
发明人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
IPC分类号： C08F8/22 , C08C19/24 , C08F8/30 , C08C19/14 , C08C19/22 , C08F2/06 , C08F8/32 , C08F8/40 , C08F210/12
CPC分类号： C08C19/24 , C08C19/14 , C08C19/22 , C08F2/06 , C08F8/22 , C08F8/30 , C08F8/32 , C08F8/40 , C08F210/12 , C08F236/08
摘要： The invention relates to an energy efficient, environmentally favorable process for the preparation of butyl ionomers that uses a common medium for both solution polymerization and subsequent bromination of butyl rubber. More particularly, the invention relates to a process that employs a common aliphatic medium for both solution polymerization and bromination of butyl rubber in the presence of a brominating agent and optionally for subsequent reaction with at least one nitrogen and/or phosphorus based nucleophile.
摘要翻译：本发明涉及用于制备丁基离聚物的能量效率高，环境友好的方法，该方法使用普通介质进行溶液聚合和随后溴化丁基橡胶。更具体地说，本发明涉及一种在溴化剂存在下使用普通脂肪族介质进行丁基橡胶的溶液聚合和溴化的方法，并且任选地随后与至少一种基于氮和/或磷的亲核试剂反应。

10. 发明授权

US09062185B2 Process for production of polymer nanocomposites 有权
标题翻译：生产聚合物纳米复合材料的方法
公开(公告)号：US09062185B2
公开(公告)日：2015-06-23
申请号：US13522760
申请日：2011-01-17
申请人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
发明人： Carsten Kreuder , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Dana Adkinson , Phil Magill
IPC分类号： C08L9/00 , B60C1/00 , B82Y30/00 , C08J5/00 , C08F210/12
CPC分类号： C08L9/00 , B60C1/00 , B82Y30/00 , C08F8/22 , C08F8/40 , C08F8/44 , C08F210/12 , C08J5/005 , C08J2323/28 , C08J2323/36 , Y02T10/862 , C08F236/08 , C08F2500/21
摘要： The invention relates to a processes for preparing nanocomposites comprising rubber ionomers which were prepared by an energy efficient, environmentally favorable process that uses a common medium for solution polymerization, bromination of rubber and optionally subsequent polymer nanocomposite formation. Polymer nanocomposites according to the present invention exhibit high oxygen impermeability.
摘要翻译：本发明涉及一种制备纳米复合材料的方法，其包括橡胶离聚物，其通过使用普通介质进行溶液聚合，溴化橡胶和任选的后续聚合物纳米复合材料形成的能量有效的，环境友好的方法制备。根据本发明的聚合物纳米复合材料显示出高的不透气性。

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