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1. 发明授权

US06565978B1 Multi-component composite coating composition and coated substrate 失效
标题翻译：多组分复合涂料组合物和涂层基材
公开(公告)号：US06565978B1
公开(公告)日：2003-05-20
申请号：US09250529
申请日：1999-02-16
申请人： Edward S. Pagac , Daniel E. Rardon , Shanti Swarup
发明人： Edward S. Pagac , Daniel E. Rardon , Shanti Swarup
IPC分类号： B32B2726
CPC分类号： B05D7/53 , C08F283/006 , C08F283/02 , C08F283/04 , C08F283/06 , C08F290/062 , C08G18/6229 , C09D4/00 , C09D4/06 , C09D5/027 , C09D151/08 , C09D167/06 , C09D167/08 , C09D171/02 , C09D175/04 , C09D177/00 , Y10T428/31504 , Y10T428/31551 , Y10T428/31554 , Y10T428/31562 , Y10T428/31565 , Y10T428/31576 , Y10T428/31725 , Y10T428/31736 , Y10T428/31743 , Y10T428/31786 , Y10T428/31855 , Y10T428/31928 , C08L2666/02 , C08L2666/04 , C08L2666/18 , C08F220/18 , C08F220/28 , C08L2666/16
摘要： A multi-component composite coating composition is provided which includes a basecoat deposited from an aqueous basecoat film-forming composition and a transparent topcoat applied over the basecoat. The basecoat film-forming composition includes at least one crosslinkable film-forming resin and at least one amphiphilic alcohol having the structural formula: HO—R, wherein R includes a linear hydrocarbon segment having at least seven contiguous carbon atoms. The amphiphilic alcohol is present in an amount ranging from about 0.01 to about 50 weight percent based upon total amount of resin solids of the basecoat film-forming composition. A coated substrate is also provided.
摘要翻译：提供了一种多组分复合涂料组合物，其包括从底漆成膜组合物沉积的底涂层和涂覆在底涂层上的透明面漆。底涂层成膜组合物包括至少一种可交联成膜树脂和至少一种具有以下结构式的两亲醇：HO-R，其中R包括具有至少七个连续碳原子的直链烃链段。基于底漆成膜组合物的树脂固体的总量，两亲性醇的存在量为约0.01至约50重量％。还提供涂覆的基底。

2. 发明授权

US06582822B2 Multi-component composite coating composition and coated substrate 失效
公开(公告)号：US06582822B2
公开(公告)日：2003-06-24
申请号：US09925670
申请日：2001-08-09
申请人： Dennis L. Faler , Djurdjica Glas , Hans-Dieter Hille , Michael Jäger , Walter Metzger , Kurt G. Olson , Edward S. Pagac , Daniel E. Rardon , Shanti Swarup
发明人： Dennis L. Faler , Djurdjica Glas , Hans-Dieter Hille , Michael Jäger , Walter Metzger , Kurt G. Olson , Edward S. Pagac , Daniel E. Rardon , Shanti Swarup
IPC分类号： B32B904
CPC分类号： B05D7/53 , C08F283/006 , C08F283/02 , C08F283/04 , C08F283/06 , C08F290/062 , C08G18/6229 , C09D4/00 , C09D4/06 , C09D5/027 , C09D151/08 , C09D167/06 , C09D167/08 , C09D171/02 , C09D175/04 , C09D177/00 , Y10T428/31504 , Y10T428/31551 , Y10T428/31554 , Y10T428/31562 , Y10T428/31565 , Y10T428/31576 , Y10T428/31725 , Y10T428/31736 , Y10T428/31743 , Y10T428/31786 , Y10T428/31855 , Y10T428/31928 , C08L2666/02 , C08L2666/04 , C08L2666/18 , C08F220/18 , C08F220/28 , C08L2666/16
摘要： An aqueous coating composition is provided which includes crosslinkable film-forming resin and about 0.01 to about 25 weight percent on a basis of total resin solids of an amphiphilic adjuvant having an acid value of less than 30, a water-soluble polar end including at least one terminal hydroxyl group and a water-insoluble hydrocarbon end including at least seven contiguous carbon atoms. The coating composition is useful as a monocoat or primer, basecoat or clearcoat in a multi-component composite coating composition for automotive applications.

3. 发明授权

US06291564B1 Aqueous coating compositions, coated substrate and method related thereto 失效
标题翻译：水性涂料组合物，涂布基材及其相关方法
公开(公告)号：US06291564B1
公开(公告)日：2001-09-18
申请号：US09250671
申请日：1999-02-16
申请人： Dennis L. Faler , Djurdjica Glas , Hans-Dieter Hille , Michael Jäger , Walter Metzger , Kurt G. Olson , Edward S. Pagac , Daniel E. Rardon , Shanti Swarup
发明人： Dennis L. Faler , Djurdjica Glas , Hans-Dieter Hille , Michael Jäger , Walter Metzger , Kurt G. Olson , Edward S. Pagac , Daniel E. Rardon , Shanti Swarup
IPC分类号： C08J300
CPC分类号： B05D7/53 , C08F283/006 , C08F283/02 , C08F283/04 , C08F283/06 , C08F290/062 , C08G18/6229 , C09D4/00 , C09D4/06 , C09D5/027 , C09D151/08 , C09D167/06 , C09D167/08 , C09D171/02 , C09D175/04 , C09D177/00 , Y10T428/31504 , Y10T428/31551 , Y10T428/31554 , Y10T428/31562 , Y10T428/31565 , Y10T428/31576 , Y10T428/31725 , Y10T428/31736 , Y10T428/31743 , Y10T428/31786 , Y10T428/31855 , Y10T428/31928 , C08L2666/02 , C08L2666/04 , C08L2666/18 , C08F220/18 , C08F220/28 , C08L2666/16
摘要： An aqueous coating composition is provided which includes crosslinkable film-forming resin and about 0.01 to about 25 weight percent on a basis of total resin solids of an amphiphilic adjuvant having an acid value of less than 30, a water-soluble polar end including at least one terminal hydroxyl group and a water-insoluble hydrocarbon end including at least seven contiguous carbon atoms. The coating composition is useful as a monocoat or primer, basecoat or clearcoat in a multi-component composite coating composition for automotive applications.
摘要翻译：提供一种水性涂料组合物，其包含可交联成膜树脂，基于酸值小于30的两亲佐剂的总树脂固体为约0.01至约25重量％，水溶性极性末端至少包括一个末端羟基和包含至少七个连续碳原子的水不溶性烃末端。涂料组合物可用作汽车应用的多组分复合涂料组合物中的单壳或底漆，底涂层或透明涂层。

4. 发明授权

US07001952B2 Coating compositions containing polyurethane dispersions and highly crosslinked polymer particles 有权
公开(公告)号：US07001952B2
公开(公告)日：2006-02-21
申请号：US10126903
申请日：2002-04-19
申请人： Dennis L. Faler , Karen A. Barkac , M. Frank Haley , Deena M. McHenry , Edward S. Pagac , Shanti Swarup , Cathy A. Taylor , Elizabeth A. Zezinka
发明人： Dennis L. Faler , Karen A. Barkac , M. Frank Haley , Deena M. McHenry , Edward S. Pagac , Shanti Swarup , Cathy A. Taylor , Elizabeth A. Zezinka
IPC分类号： C08F12/34
CPC分类号： C09D175/04 , C08G18/0823 , C08G18/0866 , C08G18/4288 , C08G18/4854 , C08G18/672 , C08G18/765 , Y10T428/31551 , Y10T428/31554 , Y10T428/31605 , C08G18/6692 , C08G18/6659
摘要： An aqueous polyurethane dispersion and thermosetting compositions containing them. The aqueous polyurethane dispersion includes an aqueous medium with dispersed polyurethane-acrylate particles, which include the reaction product obtained by polymerizing a pre-emulsion formed from hydrophobic polymerizable ethylenically unsaturated monomers, a crosslinking monomer, and an active hydrogen-containing polyurethane acrylate prepolymer, which is a reaction product obtained by reacting a polyol, a polymerizable, ethylenically unsaturated monomer containing at least one hydroxyl group, a compound that includes an alkyl group having at least one hydroxyl group and optionally a carboxylic acid group, and a polyisocyanate. The prepolymer includes at least 30 percent by weight of polyurethane acrylate prepolymers with at least one terminal ethylenic unsaturation at one end of the molecule, and at least one active hydrogen-containing group at the opposite end; and at least 10 percent by weight of prepolymers having at least one terminal ethylenic unsaturation at each end of the molecule.

5. 发明申请

US20080138639A1 POLYETHER CARBAMATE COMPOUNDS, COMPOSITIONS CONTAINING SUCH COMPOUNDS, AND METHODS RELATED THERETO 审中-公开
标题翻译：聚碳酸酯化合物，包含这些化合物的组合物及其相关方法
公开(公告)号：US20080138639A1
公开(公告)日：2008-06-12
申请号：US11837029
申请日：2007-08-10
申请人： Shanti Swarup , Michael P. Hart , Christiana Yichun Jia , Edward S. Pagac , Cathy A. Taylor , Elizabeth A. Zezinka
发明人： Shanti Swarup , Michael P. Hart , Christiana Yichun Jia , Edward S. Pagac , Cathy A. Taylor , Elizabeth A. Zezinka
IPC分类号： B32B27/08
CPC分类号： C08G18/672 , C08G18/5045 , C08G65/331 , C08G65/33344 , C08G71/04 , C09D175/16 , C09D201/025 , Y10T428/31855 , C08G18/42
摘要： The present invention provides a reaction product having polyether carbamate groups formed from (A) polyoxyalkylene amine, and (B) cyclic carbonate, in an equivalents ratio ranging from 1:0.5 to 1:1.5. Further provided is a process for preparing the aforementioned reaction product. The present invention also is directed to an improved curable coating composition including (1) a reactive functional group-containing polymer, and (2) a curing agent having functional groups reactive with the functional groups of (1), the improvement being the inclusion in the coating composition the reaction product. Multilayer composite coatings including a first coating layer formed from the curable coating composition and a second coating layer over the curable coating composition are also provided, as well as coated substrates.
摘要翻译：本发明提供具有由（A）聚氧化亚烷基胺和（B）环状碳酸酯形成的聚醚氨基甲酸酯基团的反应产物，其当量比为1:0.5至1:1.5。还提供了制备上述反应产物的方法。本发明还涉及一种改进的可固化涂料组合物，其包括（1）含反应性官能团的聚合物，和（2）具有与（1）的官能团反应的官能团的固化剂，其改进在于涂料组合物为反应产物。还提供了包括由可固化涂料组合物形成的第一涂层和可固化涂料组合物上的第二涂层的多层复合涂层以及涂覆的基材。

6. 发明授权

US06762240B2 Highly crosslinked polymer particles and coating compositions containing the same 有权
标题翻译：高度交联的聚合物颗粒和含有它的涂料组合物
公开(公告)号：US06762240B2
公开(公告)日：2004-07-13
申请号：US10126137
申请日：2002-04-19
申请人： Shanti Swarup , Brian Endlich , M. Frank Haley , Charles M. Kania , Kurt G. Olson , Edward S. Pagac , Kaliappa G. Ragunathan
发明人： Shanti Swarup , Brian Endlich , M. Frank Haley , Charles M. Kania , Kurt G. Olson , Edward S. Pagac , Kaliappa G. Ragunathan
IPC分类号： C08F21604
CPC分类号： C08F2/24 , C09D7/65
摘要： A latex emulsion that includes crosslinked polymeric microparticles dispersed in an aqueous continuous phase. The microparticles are prepared from a monomer mix of a crosslinking monomer, a monomer having hydrophilic functional groups, and one or more other monomers. Also disclosed is a thermosetting composition that includes a first reactant that has reactive functional groups; a curing agent that has at least two functional groups reactive with the functional groups of the first reactant; and the latex emulsion of crosslinked polymeric microparticles dispersed in an aqueous continuous phase. The thermosetting composition may be used to coat a substrate. The coating may be a multi-layer composite coating that includes a base coat layer deposited from a pigmented film-forming base coat composition containing the thermosetting composition; and a substantially pigment free top coat layer deposited over a portion of the base coat layer from a substantially pigment free top coat composition.
摘要翻译：包含分散在水相连续相中的交联聚合物微粒的胶乳乳液。微粒由交联单体，具有亲水性官能团的单体和一种或多种其它单体的单体混合物制备。还公开了一种热固性组合物，其包括具有反应性官能团的第一反应物; 具有至少两个与第一反应物的官能团反应的官能团的固化剂; 和分散在水性连续相中的交联聚合物微粒的胶乳乳液。热固性组合物可用于涂覆基材。涂层可以是多层复合涂层，其包括由含有热固性组合物的着色成膜底涂层组合物沉积的底涂层; 以及从基本上不含颜料的面漆组合物沉积在基底涂层的一部分上的基本上无颜料的顶涂层。

7. 发明授权

US07288595B2 Polyether carbamate compounds, compositions containing such compounds, and methods related thereto 有权
标题翻译：聚醚氨基甲酸酯化合物，含有这些化合物的组合物及其相关方法
公开(公告)号：US07288595B2
公开(公告)日：2007-10-30
申请号：US10949637
申请日：2004-09-24
申请人： Shanti Swarup , Michael P. Hart , Christiana Yichun Jia , Edward S. Pagac , Cathy A. Taylor , Elizabeth A. Zezinka
发明人： Shanti Swarup , Michael P. Hart , Christiana Yichun Jia , Edward S. Pagac , Cathy A. Taylor , Elizabeth A. Zezinka
IPC分类号： C08L61/00 , C08L63/00 , C08L67/00 , C08L71/00 , C08L75/04
CPC分类号： C08G18/672 , C08G18/5045 , C08G65/331 , C08G65/33344 , C08G71/04 , C09D175/16 , C09D201/025 , Y10T428/31855 , C08G18/42
摘要： The present invention provides a reaction product having polyether carbamate groups formed from (A) polyoxyalkylene amine, and (B) cyclic carbonate, in an equivalents ratio ranging from 1:0.5 to 1:1.5. Further provided is a process for preparing the aforementioned reaction product. The present invention also is directed to an improved curable coating composition including (1) a reactive functional group-containing polymer, and (2) a curing agent having functional groups reactive with the functional groups of (1), the improvement being the inclusion in the coating composition the reaction product. Multilayer composite coatings including a first coating layer formed from the curable coating composition and a second coating layer over the curable coating composition are also provided, as well as coated substrates.
摘要翻译：本发明提供具有由（A）聚氧化亚烷基胺和（B）环状碳酸酯形成的聚醚氨基甲酸酯基团的反应产物，其当量比为1:0.5至1:1.5。还提供了制备上述反应产物的方法。本发明还涉及一种改进的可固化涂料组合物，其包括（1）含反应性官能团的聚合物，和（2）具有与（1）的官能团反应的官能团的固化剂，其改进在于涂料组合物为反应产物。还提供了包括由可固化涂料组合物形成的第一涂层和可固化涂料组合物上的第二涂层的多层复合涂层以及涂覆的基材。

8. 发明申请

US20120142817A1 ONE COMPONENT EPOXY STRUCTURAL ADHESIVE COMPOSITION PREPARED FROM RENEWABLE RESOURCES 有权
标题翻译：可再生资源制备的一种组分环氧结构粘合剂组合物
公开(公告)号：US20120142817A1
公开(公告)日：2012-06-07
申请号：US12958460
申请日：2010-12-02
申请人： Shanti Swarup , Masayuki Nakajima , Umesh C. Desai , Tien-Chieh Chao , Charles M. Kania , Britt Minch
发明人： Shanti Swarup , Masayuki Nakajima , Umesh C. Desai , Tien-Chieh Chao , Charles M. Kania , Britt Minch
IPC分类号： C08L33/20 , C08L63/00
CPC分类号： C08G59/4021 , C08G59/4261 , C08G59/50 , C09J163/00
摘要： Curable, one-package, stable adhesive compositions are provided comprising: (a) a resin component comprising a polyepoxide, (b) a polyamine having at least two primary amine, secondary amine, and/or ketimine functional groups; and (c) a curing component comprising dicyandiamide and an accelerator. At least a portion of the polyepoxide in the resin component is reacted with carboxy-terminated butadiene acrylonitrile polymer. The accelerator comprises a reaction product comprising a renewable polyol, a diisocyanate, and a dialkyl monoamine containing alkyl groups with at least two carbon atoms each. The compositions are suitable for use as adhesive compositions over a wide temperature range.
摘要翻译：提供了可固化的单包装稳定的粘合剂组合物，其包含：（a）包含聚环氧化物的树脂组分，（b）具有至少两个伯胺，仲胺和/或酮亚胺官能团的多胺; 和（c）包含双氰胺和促进剂的固化组分。树脂组分中的至少一部分聚环氧化物与羧基封端的丁二烯丙烯腈聚合物反应。促进剂包括包含可再生多元醇，二异氰酸酯和含有至少两个碳原子的烷基的二烷基单胺的反应产物。该组合物适用于宽温度范围内的粘合剂组合物。

9. 发明授权

US08153708B2 Process for forming a waterborne composite polyurethane/acrylic polymer dispersion 有权
标题翻译：形成水性复合聚氨酯/丙烯酸聚合物分散体的方法
公开(公告)号：US08153708B2
公开(公告)日：2012-04-10
申请号：US12752372
申请日：2010-04-01
申请人： Shanti Swarup
发明人： Shanti Swarup
IPC分类号： C08J3/00
CPC分类号： C08G18/0823 , C08G18/2825 , C08G18/4063 , C08G18/4238 , C08G18/6229
摘要： The present invention provides a process for forming a waterborne composite polyurethane/acrylic polymer dispersion without the use of N-methyl pyrrolidone. The process includes polymerizing a reaction mixture of polyisocyanate, polyol, and a hydroxyl and carboxylic acid functional reactant in an organic solvent medium of alkyl carbonate, then adding ethylenically unsaturated monomers and inverting the mixture into an aqueous medium. Addition polymerization is performed to yield a waterborne composite polyurethane/acrylic polymer dispersion, and any remaining alkyl carbonate is hydrolyzed. The resulting aqueous polymer dispersions are environmentally friendly and are suitable for use in coating compositions that conventionally contained similar dispersions prepared in the presence of N-methyl pyrrolidone. Comparable physical properties are observed.
摘要翻译：本发明提供了不使用N-甲基吡咯烷酮形成水性复合聚氨酯/丙烯酸类聚合物分散体的方法。该方法包括将多异氰酸酯，多元醇和羟基和羧酸官能反应物的反应混合物聚合在碳酸烷基酯的有机溶剂介质中，然后加入烯属不饱和单体并将混合物倒入水性介质中。进行加成聚合以产生水性复合聚氨酯/丙烯酸聚合物分散体，并且任何残留的碳酸烷基酯都被水解。所得水性聚合物分散体是环境友好的，并且适用于常规含有在N-甲基吡咯烷酮存在下制备的相似分散体的涂料组合物。观察到相当的物理性质。

10. 发明申请

US20110245415A1 PROCESS FOR FORMING A WATERBORNE COMPOSITE POLYURETHANE/ACRYLIC POLYMER DISPERSION 有权
标题翻译：形成水性复合聚氨酯/丙烯酸聚合物分散体的方法
公开(公告)号：US20110245415A1
公开(公告)日：2011-10-06
申请号：US12752372
申请日：2010-04-01
申请人： Shanti Swarup
发明人： Shanti Swarup
IPC分类号： C08G18/08
CPC分类号： C08G18/0823 , C08G18/2825 , C08G18/4063 , C08G18/4238 , C08G18/6229
摘要： The present invention provides a process for forming a waterborne composite polyurethane/acrylic polymer dispersion without the use of N-methyl pyrrolidone. The process includes polymerizing a reaction mixture of polyisocyanate, polyol, and a hydroxyl and carboxylic acid functional reactant in an organic solvent medium of alkyl carbonate, then adding ethylenically unsaturated monomers and inverting the mixture into an aqueous medium. Addition polymerization is performed to yield a waterborne composite polyurethane/acrylic polymer dispersion, and any remaining alkyl carbonate is hydrolyzed. The resulting aqueous polymer dispersions are environmentally friendly and are suitable for use in coating compositions that conventionally contained similar dispersions prepared in the presence of N-methyl pyrrolidone. Comparable physical properties are observed.
摘要翻译：本发明提供了不使用N-甲基吡咯烷酮形成水性复合聚氨酯/丙烯酸类聚合物分散体的方法。该方法包括将多异氰酸酯，多元醇和羟基和羧酸官能反应物的反应混合物聚合在碳酸烷基酯的有机溶剂介质中，然后加入烯属不饱和单体并将混合物倒入水性介质中。进行加成聚合以产生水性复合聚氨酯/丙烯酸聚合物分散体，并且任何残留的碳酸烷基酯都被水解。所得水性聚合物分散体是环境友好的，并且适用于常规含有在N-甲基吡咯烷酮存在下制备的相似分散体的涂料组合物。观察到相当的物理性质。

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