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1. 发明授权

US07001952B2 Coating compositions containing polyurethane dispersions and highly crosslinked polymer particles 有权
公开(公告)号：US07001952B2
公开(公告)日：2006-02-21
申请号：US10126903
申请日：2002-04-19
申请人： Dennis L. Faler , Karen A. Barkac , M. Frank Haley , Deena M. McHenry , Edward S. Pagac , Shanti Swarup , Cathy A. Taylor , Elizabeth A. Zezinka
发明人： Dennis L. Faler , Karen A. Barkac , M. Frank Haley , Deena M. McHenry , Edward S. Pagac , Shanti Swarup , Cathy A. Taylor , Elizabeth A. Zezinka
IPC分类号： C08F12/34
CPC分类号： C09D175/04 , C08G18/0823 , C08G18/0866 , C08G18/4288 , C08G18/4854 , C08G18/672 , C08G18/765 , Y10T428/31551 , Y10T428/31554 , Y10T428/31605 , C08G18/6692 , C08G18/6659
摘要： An aqueous polyurethane dispersion and thermosetting compositions containing them. The aqueous polyurethane dispersion includes an aqueous medium with dispersed polyurethane-acrylate particles, which include the reaction product obtained by polymerizing a pre-emulsion formed from hydrophobic polymerizable ethylenically unsaturated monomers, a crosslinking monomer, and an active hydrogen-containing polyurethane acrylate prepolymer, which is a reaction product obtained by reacting a polyol, a polymerizable, ethylenically unsaturated monomer containing at least one hydroxyl group, a compound that includes an alkyl group having at least one hydroxyl group and optionally a carboxylic acid group, and a polyisocyanate. The prepolymer includes at least 30 percent by weight of polyurethane acrylate prepolymers with at least one terminal ethylenic unsaturation at one end of the molecule, and at least one active hydrogen-containing group at the opposite end; and at least 10 percent by weight of prepolymers having at least one terminal ethylenic unsaturation at each end of the molecule.

2. 发明申请

US20100209697A1 METHODS FOR PRODUCING PHOTOSENSITIVE MICROPARTICLES, NON-AQUEOUS DISPERSIONS THEREOF AND ARTICLES PREPARED THEREWITH 有权
标题翻译：生产感光性微生物的方法及其制备的非水性分散体及其制备方法
公开(公告)号：US20100209697A1
公开(公告)日：2010-08-19
申请号：US12719293
申请日：2010-03-08
申请人： Steven E. Bowles , Anu Chopra , James P. Colton , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
发明人： Steven E. Bowles , Anu Chopra , James P. Colton , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
IPC分类号： G02B1/10 , H01F1/26 , H01B1/12 , G02B5/23 , C09K11/06 , C08K5/057 , C08K5/5419 , C08L75/00 , B32B5/16
CPC分类号： G02B1/10 , C08G18/3275 , C08G18/348 , C08G18/6659 , C08G18/672 , C08G18/755 , C08G18/758 , C09D175/16 , G02B1/11 , G03C1/733 , G03F7/002 , G03F7/038 , G03F7/105 , G11B7/242 , Y10T428/25 , C08G18/0823
摘要： Described are non-aqueous dispersions of photosensitive polymeric microparticles, comprising: a) an organic continuous phase comprising an organic solvent; and b) photosensitive polymeric microparticles dispersed in the organic continuous phase. The microparticles comprise an at least partially polymerized component having integral surface and interior domains, wherein the surface domain comprises a polymeric material that is solubilized by the organic solvent, the interior domain comprises a polymeric material that is insoluble in the organic solvent, and the surface domain and/or interior domain is photosensitive. Also described are methods of producing such non-aqueous dispersions, curable film-forming compositions containing them, and photosensitive coated substrates.
摘要翻译：描述的是光敏聚合物微粒的非水分散体，包括：a）包含有机溶剂的有机连续相; 和b）分散在有机连续相中的光敏聚合物微粒。微粒包括具有整体表面和内部结构域的至少部分聚合的组分，其中表面结构域包含由有机溶剂溶解的聚合材料，内部结构域包含不溶于有机溶剂的聚合材料，表面域和/或内部域是光敏的。还描述了制备这种非水分散体，含有它们的可固化成膜组合物和感光涂布基材的方法。

3. 发明授权

US08563213B2 Methods for producing photosensitive microparticles 有权
标题翻译：光敏微粒的制造方法
公开(公告)号：US08563213B2
公开(公告)日：2013-10-22
申请号：US12719335
申请日：2010-03-08
申请人： Steven E. Bowles , Anu Chopra , Randy E. Daughenbaugh , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
发明人： Steven E. Bowles , Anu Chopra , Randy E. Daughenbaugh , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
IPC分类号： G03C1/72 , G03F7/00
CPC分类号： G03F7/002 , C08F290/067 , C08G18/3271 , C08G18/3275 , C08G18/672 , C08G18/751 , C08G18/757 , C08G18/758 , C08G18/792 , C08G18/8116 , C08L25/06 , C09D175/04 , C09D175/16 , C09K9/02 , G03C1/733 , G03F7/038 , G03F7/105 , C08G18/0823 , C08L2666/14 , C08L2666/16
摘要： Described are various methods of producing non-aqueous dispersions of photosensitive polymeric microparticles, comprising: (a) preparing one or more aqueous dispersions of a polymerizable component, at least one of which contains a photosensitive material and, wherein the polymerizable components comprise at least one hydrophilic functional group and/or at least one hydrophobic functional group; (b) subjecting the dispersion of (a) to conditions sufficient to form microparticles; (c) at least partially polymerizing the polymerizable component; (d) combining the dispersion with an organic continuous phase comprising an organic solvent; (e) removing water from the dispersion such that the final water content of the non-aqueous dispersion is less than 30 percent by weight; wherein e) is performed before or after d); and (f) reacting any acid functional groups on the surface of the microparticles with a reactive material having at least one epoxy functional group, at least one thiocarbonylthio functional group, at least one alkoxyamine functional group, or at least one halide functional group.
摘要翻译：描述了生产光敏聚合物微粒非水分散体的各种方法，包括：（a）制备一种或多种可聚合组分的水分散体，其中至少一种含有感光材料，其中可聚合组分包括至少一种亲水官能团和/或至少一个疏水官能团; （b）使（a）的分散体经受足以形成微粒的条件; （c）至少部分聚合可聚合组分; （d）将分散体与包含有机溶剂的有机连续相组合; （e）从分散体中除去水，使得非水分散体的最终含水量小于30重量％; 其中e）在d）之前或之后进行; 和（f）使微粒表面上的任何酸官能团与具有至少一个环氧官能团，至少一个硫代羰硫基官能团，至少一个烷氧基胺官能团或至少一个卤化物官能团的反应性材料反应。

4. 发明授权

US08563212B2 Methods for producing photosensitive microparticles, non-aqueous dispersions thereof and articles prepared therewith 有权
标题翻译：用于制备感光性微粒的方法，非水性分散体及其制备的制品
公开(公告)号：US08563212B2
公开(公告)日：2013-10-22
申请号：US12719293
申请日：2010-03-08
申请人： Steven E. Bowles , Anu Chopra , James P. Colton , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
发明人： Steven E. Bowles , Anu Chopra , James P. Colton , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
IPC分类号： G03C1/72 , G03F7/00
CPC分类号： G02B1/10 , C08G18/3275 , C08G18/348 , C08G18/6659 , C08G18/672 , C08G18/755 , C08G18/758 , C09D175/16 , G02B1/11 , G03C1/733 , G03F7/002 , G03F7/038 , G03F7/105 , G11B7/242 , Y10T428/25 , C08G18/0823
摘要： Described are non-aqueous dispersions of photosensitive polymeric microparticles, comprising: a) an organic continuous phase comprising an organic solvent; and b) photosensitive polymeric microparticles dispersed in the organic continuous phase. The microparticles comprise an at least partially polymerized component having integral surface and interior domains, wherein the surface domain comprises a polymeric material that is solubilized by the organic solvent, the interior domain comprises a polymeric material that is insoluble in the organic solvent, and the surface domain and/or interior domain is photosensitive. Also described are methods of producing such non-aqueous dispersions, curable film-forming compositions containing them, and photosensitive coated substrates.
摘要翻译：描述的是光敏聚合物微粒的非水分散体，包括：a）包含有机溶剂的有机连续相; 和b）分散在有机连续相中的光敏聚合物微粒。微粒包括具有整体表面和内部结构域的至少部分聚合的组分，其中表面结构域包含由有机溶剂溶解的聚合材料，内部结构域包含不溶于有机溶剂的聚合材料，表面域和/或内部域是光敏的。还描述了制备这种非水分散体，含有它们的可固化成膜组合物和感光涂布基材的方法。

5. 发明申请

US20100221661A1 METHODS FOR PRODUCING PHOTOSENSITIVE MICROPARTICLES 有权
标题翻译：用于生产感光性微生物的方法
公开(公告)号：US20100221661A1
公开(公告)日：2010-09-02
申请号：US12719335
申请日：2010-03-08
申请人： Steven E. Bowles , Anu Chopra , Randy E. Daughenbaugh , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
发明人： Steven E. Bowles , Anu Chopra , Randy E. Daughenbaugh , Dennis L. Faler , M. Frank Haley , Paul H. Lamers , Yunyi Lu , Kevin J. Stewart , Cathy A. Taylor , Feng Wang , Elizabeth A. Zezinka
IPC分类号： G03F7/004
CPC分类号： G03F7/002 , C08F290/067 , C08G18/3271 , C08G18/3275 , C08G18/672 , C08G18/751 , C08G18/757 , C08G18/758 , C08G18/792 , C08G18/8116 , C08L25/06 , C09D175/04 , C09D175/16 , C09K9/02 , G03C1/733 , G03F7/038 , G03F7/105 , C08G18/0823 , C08L2666/14 , C08L2666/16
摘要： Described are various methods of producing non-aqueous dispersions of photosensitive polymeric microparticles, comprising: (a) preparing one or more aqueous dispersions of a polymerizable component, at least one of which contains a photosensitive material and, wherein the polymerizable components comprise at least one hydrophilic functional group and/or at least one hydrophobic functional group; (b) subjecting the dispersion of (a) to conditions sufficient to form microparticles; (c) at least partially polymerizing the polymerizable component; (d) combining the dispersion with an organic continuous phase comprising an organic solvent; (e) removing water from the dispersion such that the final water content of the non-aqueous dispersion is less than 30 percent by weight; wherein e) is performed before or after d); and (f) reacting any acid functional groups on the surface of the microparticles with a reactive material having at least one epoxy functional group, at least one thiocarbonylthio functional group, at least one alkoxyamine functional group, or at least one halide functional group.
摘要翻译：描述了生产光敏聚合物微粒非水分散体的各种方法，包括：（a）制备一种或多种可聚合组分的水分散体，其中至少一种含有感光材料，其中可聚合组分包括至少一种亲水官能团和/或至少一个疏水官能团; （b）使（a）的分散体经受足以形成微粒的条件; （c）至少部分聚合可聚合组分; （d）将分散体与包含有机溶剂的有机连续相组合; （e）从分散体中除去水，使得非水分散体的最终含水量小于30重量％; 其中e）在d）之前或之后执行; 和（f）使微粒表面上的任何酸官能团与具有至少一个环氧官能团，至少一个硫代羰硫基官能团，至少一个烷氧基胺官能团或至少一个卤化物官能团的反应性材料反应。

6. 发明授权

US06762240B2 Highly crosslinked polymer particles and coating compositions containing the same 有权
标题翻译：高度交联的聚合物颗粒和含有它的涂料组合物
公开(公告)号：US06762240B2
公开(公告)日：2004-07-13
申请号：US10126137
申请日：2002-04-19
申请人： Shanti Swarup , Brian Endlich , M. Frank Haley , Charles M. Kania , Kurt G. Olson , Edward S. Pagac , Kaliappa G. Ragunathan
发明人： Shanti Swarup , Brian Endlich , M. Frank Haley , Charles M. Kania , Kurt G. Olson , Edward S. Pagac , Kaliappa G. Ragunathan
IPC分类号： C08F21604
CPC分类号： C08F2/24 , C09D7/65
摘要： A latex emulsion that includes crosslinked polymeric microparticles dispersed in an aqueous continuous phase. The microparticles are prepared from a monomer mix of a crosslinking monomer, a monomer having hydrophilic functional groups, and one or more other monomers. Also disclosed is a thermosetting composition that includes a first reactant that has reactive functional groups; a curing agent that has at least two functional groups reactive with the functional groups of the first reactant; and the latex emulsion of crosslinked polymeric microparticles dispersed in an aqueous continuous phase. The thermosetting composition may be used to coat a substrate. The coating may be a multi-layer composite coating that includes a base coat layer deposited from a pigmented film-forming base coat composition containing the thermosetting composition; and a substantially pigment free top coat layer deposited over a portion of the base coat layer from a substantially pigment free top coat composition.
摘要翻译：包含分散在水相连续相中的交联聚合物微粒的胶乳乳液。微粒由交联单体，具有亲水性官能团的单体和一种或多种其它单体的单体混合物制备。还公开了一种热固性组合物，其包括具有反应性官能团的第一反应物; 具有至少两个与第一反应物的官能团反应的官能团的固化剂; 和分散在水性连续相中的交联聚合物微粒的胶乳乳液。热固性组合物可用于涂覆基材。涂层可以是多层复合涂层，其包括由含有热固性组合物的着色成膜底涂层组合物沉积的底涂层; 以及从基本上不含颜料的面漆组合物沉积在基底涂层的一部分上的基本上无颜料的顶涂层。

7. 发明授权

US08647538B2 Photochromic compounds having at least two photochromic moieties 有权
标题翻译：具有至少两个光致变色部分的光致变色化合物
公开(公告)号：US08647538B2
公开(公告)日：2014-02-11
申请号：US13302316
申请日：2011-11-22
申请人： Yunyi Lu , Wenjing Xiao , Robert W. Walters , Feng Wang , M. Frank Haley , Jason R. Lewis , Anu Chopra , Beon-Kyu Kim , Huayun Yu
发明人： Yunyi Lu , Wenjing Xiao , Robert W. Walters , Feng Wang , M. Frank Haley , Jason R. Lewis , Anu Chopra , Beon-Kyu Kim , Huayun Yu
IPC分类号： G02B5/23 , C07D265/30 , C07D295/00
CPC分类号： C07D311/94 , C07D405/14 , C09K9/02 , C09K2211/1007 , C09K2211/1011 , C09K2211/1022 , C09K2211/1029 , C09K2211/1033 , C09K2211/1059 , C09K2211/1088 , G02B5/23 , G03C1/685 , G03C1/73 , Y10T428/31504
摘要： The present invention relates to photochromic compounds that include at least two photochromic moieties that are linked together by a multivalent linking group. The multivalent linking group can be selected so as to be flexible and/or substantially prevent electronic interaction between any two photochromic moieties through the multivalent linking group. The present invention also relates to photochromic compositions and articles that include at least a photochromic amount of one or more photochromic compounds of the present invention.
摘要翻译：本发明涉及包含通过多价连接基团连接在一起的至少两个光致变色部分的光致变色化合物。可以选择多价连接基团以使其柔性和/或基本上防止通过多价连接基团的任何两个光致变色部分之间的电子相互作用。本发明还涉及至少包含光致变色量的一种或多种本发明的光致变色化合物的光致变色组合物和制品。

8. 发明申请

US20120136148A1 Photochromic Compounds Having At Least Two Photochromic Moieties 有权
标题翻译：具有至少两个光致变色部分的光致变色化合物
公开(公告)号：US20120136148A1
公开(公告)日：2012-05-31
申请号：US13302316
申请日：2011-11-22
申请人： Yunyi Lu , Wenjing Xiao , Robert W. Walters , Feng Wang , M. Frank Haley , Jason R. Lewis , Anu Chopra , Beon-Kyu Kim , Huayun Yu
发明人： Yunyi Lu , Wenjing Xiao , Robert W. Walters , Feng Wang , M. Frank Haley , Jason R. Lewis , Anu Chopra , Beon-Kyu Kim , Huayun Yu
IPC分类号： C07D407/12 , C07D405/14 , C07D413/14
CPC分类号： C07D311/94 , C07D405/14 , C09K9/02 , C09K2211/1007 , C09K2211/1011 , C09K2211/1022 , C09K2211/1029 , C09K2211/1033 , C09K2211/1059 , C09K2211/1088 , G02B5/23 , G03C1/685 , G03C1/73 , Y10T428/31504
摘要： The present invention relates to photochromic compounds that include at least two photochromic moieties that are linked together by a multivalent linking group. The multivalent linking group can be selected so as to be flexible and/or substantially prevent electronic interaction between any two photochromic moieties through the multivalent linking group. The present invention also relates to photochromic compositions and articles that include at least a photochromic amount of one or more photochromic compounds of the present invention.
摘要翻译：本发明涉及包含通过多价连接基团连接在一起的至少两个光致变色部分的光致变色化合物。可以选择多价连接基团以使其柔性和/或基本上防止通过多价连接基团的任何两个光致变色部分之间的电子相互作用。本发明还涉及至少包含光致变色量的一种或多种本发明的光致变色化合物的光致变色组合物和制品。

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