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1. 发明申请

WO2008128011A3 CONVERSION OF A MULTIHYDROXYLATED-ALIPHATIC HYDROCARBON OR ESTER THEREOF TO A CHLOROHYDRIN 审中-公开
公开(公告)号：WO2008128011A3
公开(公告)日：2008-10-23
申请号：PCT/US2008/059977
申请日：2008-04-11
申请人： DOW GLOBAL TECHNOLOGIES INC. , BRIGGS, John, R. , HOOK, Bruce, D. , KRUPER, William, J. , MEHTA, Anil, J. , ALVARADO, Robert, M. , NOORMANN, Sascha , BASILE, Perry, S.
发明人： BRIGGS, John, R. , HOOK, Bruce, D. , KRUPER, William, J. , MEHTA, Anil, J. , ALVARADO, Robert, M. , NOORMANN, Sascha , BASILE, Perry, S.
IPC分类号： C07C29/62
摘要： The present invention relates to a process for converting at least one multihydroxylated-aliphatic hydrocarbon and/or an ester thereof to at least one chlorohydrin and/or an ester thereof, comprising at least one reaction step in which the multihydroxylated-aliphatic hydrocarbon and/or ester thereof is contacted with hydrogen chloride under reaction conditions to produce the chlorohydrin and/or ester thereof, followed by at least one downstream processing step in which the effluents of the reaction step are processed, wherein the downstream processing step is performed in such conditions that the effluents containing the chlorohydrin and/or ester thereof are kept at a temperature of less than 12O°C. The invention allows to minimize the liberation of hydrogen chloride from the products of the hydrochlorination reaction, hence reducing the corrosion of the downstream equipment and reducing the need to use costly corrosion resistant materials.

2. 发明申请

WO2009129014A1 CONVERSION OF MULTIHYDROXYLATED-ALIPHATIC HYDROCARBON OR ESTER THEREOF TO A CHLOROHYDRIN 审中-公开
标题翻译：多羟基化二烃或其衍生物转化为氯仿
公开(公告)号：WO2009129014A1
公开(公告)日：2009-10-22
申请号：PCT/US2009/037488
申请日：2009-03-18
申请人： DOW GLOBAL TECHNOLOGIES INC. , BRIGGS, John, R. , HOOK, Bruce, D. , KRUPER, Jr. , MEHTA, Anil , ALVARADO, Robert, M. , NOORMANN, Sascha , BASILE, Perry, S.
发明人： BRIGGS, John, R. , HOOK, Bruce, D. , KRUPER, Jr. , MEHTA, Anil , ALVARADO, Robert, M. , NOORMANN, Sascha , BASILE, Perry, S.
IPC分类号： C07C29/62 , C07C31/42 , B01D3/00
CPC分类号： C07C29/62 , C07C31/42 , C07C31/36
摘要： The present invention relates to a process for converting at least one multihydroxylated-aliphatic hydrocarbon and/or an ester thereof to at least one chlorohydrin and/or an ester thereof, comprising at least one reaction step in which the multihydroxylated-aliphatic hydrocarbon and/or ester thereof is contacted with hydrogen chloride under reaction conditions to produce the chlorohydrin and/or ester thereof, followed by at least one downstream processing step in which the effluents of the reaction step are processed, wherein the downstream processing step is performed in such conditions that the effluents containing the chlorohydrin and/or ester thereof are kept at a temperature of less than 120 0 C. The invention allows to minimize the liberation of hydrogen chloride from the products of the hydrochlorination reaction, hence reducing the corrosion of the downstream equipment and reducing the need to use costly corrosion resistant materials.
摘要翻译：本发明涉及将至少一种多羟基化脂族烃和/或其酯转化成至少一种氯代醇和/或其酯的方法，该方法包括至少一个反应步骤，其中多羟基化脂族烃和/或其酯在反应条件下与氯化氢接触以产生氯醇和/或其酯，随后是至少一个下游处理步骤，其中反应步骤的流出物被处理，其中下游处理步骤在以下条件下进行：含有氯代醇和/或其酯的流出物保持在低于120℃的温度。本发明允许最小化氢氯化反应产物中氯化氢的释放，从而减少下游设备的腐蚀并减少使用昂贵的耐腐蚀材料的需要。

3. 发明申请

WO2009108419A1 PROCESS AND APPARATUS FOR PRODUCING AND PURIFYING EPICHLOROHYDRINS 审中-公开
标题翻译：生产和净化二氢氯仿的方法和装置
公开(公告)号：WO2009108419A1
公开(公告)日：2009-09-03
申请号：PCT/US2009/031630
申请日：2009-01-22
申请人： DOW GLOBAL TECHNOLOGIES INC. , KNEUPPER, Christian, D. , BASILE, Perry, S. , FAN, William, W. , NOORMANN, Sascha
发明人： KNEUPPER, Christian, D. , BASILE, Perry, S. , FAN, William, W. , NOORMANN, Sascha
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , C07D301/32
摘要： A process and apparatus are disclosed for the purification of epichlorohydrin. The process includes distilling and/or fractionating a feed stream containing epichlorohydrin, dichlorohydrin(s), and one or more other substances, subjecting at least a portion of the liquid phase effluent to a dichlorohydrin dehydrochlorination process for converting residual dichlorohydrin(s) in the liquid phase effluent to epichlorohydrin, and recovering purified epichlorohydrin from the vapor phase effluent in which the distillation/fractionation pressure and/or temperature of step (1) is adjusted to retain at least 5 weight-percent epichlorohydrin in the liquid phase effluent. The apparatus for making purified epichlorohydrin includes a dehydrochlorination apparatus, a first liquid-vapor contacting apparatus, and a second liquid-vapor contacting apparatus connected to the dehydrochlorination apparatus for recycling a distillate to the dehydrochlorination apparatus. Advantages include more efficient recovery of epichlorohydrins and reduced capital investment in recovery equipment.
摘要翻译：公开了用于纯化表氯醇的方法和装置。该方法包括蒸馏和/或分馏含有表氯醇，二氯丙醇和一种或多种其它物质的进料流，将至少一部分液相流出物进行二氯丙醇脱氯化氢处理，以将残留的二氯丙醇液相流出物至表氯醇，并从气相流出物回收纯化的表氯醇，其中调节步骤（1）的蒸馏/分馏分压和/或温度以在液相流出物中保留至少5重量％的表氯醇。用于制备纯化的表氯醇的装置包括脱氯化氢装置，第一液 - 蒸气接触装置和连接到脱氯化氢装置的第二液 - 蒸气接触装置，用于将馏出物再循环到脱氯化氢装置。优点包括更有效地回收表氯醇，减少回收设备的资金投入。

4. 发明公开

EP2137120A2 CONVERSION OF A MULTIHYDROXYLATED-ALIPHATIC HYDROCARBON OR ESTER THEREOF TO A CHLOROHYDRIN 审中-公开
标题翻译： CONVERSION IN AN氯代甲MULTI-羟基化的脂族烃或其酯
公开(公告)号：EP2137120A2
公开(公告)日：2009-12-30
申请号：EP08780514.9
申请日：2008-04-11
申请人： DOW GLOBAL TECHNOLOGIES INC.
发明人： BRIGGS, John, R. , HOOK, Bruce, D. , KRUPER, William, J. , MEHTA, Anil, J. , ALVARADO, Robert, M. , NOORMANN, Sascha , BASILE, Perry, S.
IPC分类号： C07C29/62
CPC分类号： C07C29/62 , C07C31/36 , C07C31/42
摘要： The present invention relates to a process for converting at least one multihydroxylated-aliphatic hydrocarbon and/or an ester thereof to at least one chlorohydrin and/or an ester thereof, comprising at least one reaction step in which the multihydroxylated-aliphatic hydrocarbon and/or ester thereof is contacted with hydrogen chloride under reaction conditions to produce the chlorohydrin and/or ester thereof, followed by at least one downstream processing step in which the effluents of the reaction step are processed, wherein the downstream processing step is performed in such conditions that the effluents containing the chlorohydrin and/or ester thereof are kept at a temperature of less than 12O°C. The invention allows to minimize the liberation of hydrogen chloride from the products of the hydrochlorination reaction, hence reducing the corrosion of the downstream equipment and reducing the need to use costly corrosion resistant materials.

5. 发明公开

EP2280917A1 CONVERSION OF MULTIHYDROXYLATED-ALIPHATIC HYDROCARBON OR ESTER THEREOF TO A CHLOROHYDRIN 审中-公开
标题翻译：复合性CONVERSION羟基化的脂族烃或其酯成氯代醇
公开(公告)号：EP2280917A1
公开(公告)日：2011-02-09
申请号：EP09733042.7
申请日：2009-03-18
申请人： Dow Global Technologies Inc.
发明人： BRIGGS, John, R. , HOOK, Bruce, D. , KRUPER, Jr. , MEHTA, Anil , ALVARADO, Robert, M. , NOORMANN, Sascha , BASILE, Perry, S.
IPC分类号： C07C29/62 , C07C31/42 , B01D3/00
CPC分类号： C07C29/62 , C07C31/42 , C07C31/36
摘要： The present invention relates to a process for converting at least one multihydroxylated-aliphatic hydrocarbon and/or an ester thereof to at least one chlorohydrin and/or an ester thereof, comprising at least one reaction step in which the multihydroxylated-aliphatic hydrocarbon and/or ester thereof is contacted with hydrogen chloride under reaction conditions to produce the chlorohydrin and/or ester thereof, followed by at least one downstream processing step in which the effluents of the reaction step are processed, wherein the downstream processing step is performed in such conditions that the effluents containing the chlorohydrin and/or ester thereof are kept at a temperature of less than 120
0 C. The invention allows to minimize the liberation of hydrogen chloride from the products of the hydrochlorination reaction, hence reducing the corrosion of the downstream equipment and reducing the need to use costly corrosion resistant materials.

6. 发明公开

EP2257537A1 PROCESS AND APPARATUS FOR PRODUCING AND PURIFYING EPICHLOROHYDRINS 无效
标题翻译：程序对清洁环氧氯丙烷
公开(公告)号：EP2257537A1
公开(公告)日：2010-12-08
申请号：EP09715473.6
申请日：2009-01-22
申请人： Dow Global Technologies Inc.
发明人： KNEUPPER, Christian, D. , BASILE, Perry, S. , FAN, William, W. , NOORMANN, Sascha
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , C07D301/32
摘要： A process and apparatus are disclosed for the purification of epichlorohydrin. The process includes distilling and/or fractionating a feed stream containing epichlorohydrin, dichlorohydrin(s), and one or more other substances, subjecting at least a portion of the liquid phase effluent to a dichlorohydrin dehydrochlorination process for converting residual dichlorohydrin(s) in the liquid phase effluent to epichlorohydrin, and recovering purified epichlorohydrin from the vapor phase effluent in which the distillation/fractionation pressure and/or temperature of step (1) is adjusted to retain at least 5 weight-percent epichlorohydrin in the liquid phase effluent. The apparatus for making purified epichlorohydrin includes a dehydrochlorination apparatus, a first liquid-vapor contacting apparatus, and a second liquid-vapor contacting apparatus connected to the dehydrochlorination apparatus for recycling a distillate to the dehydrochlorination apparatus. Advantages include more efficient recovery of epichlorohydrins and reduced capital investment in recovery equipment.

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