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1. 发明授权

US08889890B2 Ketal esters of oxocarboxylic acids and process of making 有权
标题翻译：氧代羧酸的酮酯和制备方法
公开(公告)号：US08889890B2
公开(公告)日：2014-11-18
申请号：US13395317
申请日：2010-09-13
申请人： Douglas A. Wicks , Sergey Selifonov , Marc Davis Scholten
发明人： Douglas A. Wicks , Sergey Selifonov , Marc Davis Scholten
IPC分类号： C07D317/24 , C07D317/14
CPC分类号： C07D317/14
摘要： A ketal ester of an oxocarboxylic acid and a process to make the same, where the ketal ester is of Structure (I): wherein a is 0 or an integer from 1 to 12; n is 0 or 1; R1 is a linear alkyl, aryl, arylalkylene, or branched alkyl group with 1-18 carbon atoms; R2 and R5 can be hydrogen, C1-6 straight chain or branched alkyl, phenyl, substituted phenyl, C1-6 alkyl substituted with up to four OH groups, C1-6 alkyl, or acetyl optionally substituted hydrocarbon radicals, or R2 and R4 together with the α-carbon form a cycloaliphatic or heterocyclic ring with 3-6 carbon atoms and 0-3 heteroatoms, provided that only one of R2 and R5 is hydrogen; R3 is a linear alkyl or branched alkyl group with 1-18 carbon atoms; and R4 is hydrogen, or an alkyl, aryl, aralkyl or branched alkyl group with 1-10 carbon atoms.
摘要翻译：一种氧代羧酸的缩酮酯及其制备方法，其中缩酮为结构式（I）：其中a为0或1至12的整数; n为0或1; R1是具有1-18个碳原子的直链烷基，芳基，芳基亚烷基或支链烷基; R 2和R 5可以是氢，C 1-6直链或支链烷基，苯基，取代的苯基，被至多四个OH基取代的C 1-6烷基，C 1-6烷基或乙酰基任选取代的烃基，或者R 2和R 4一起与α-碳形成具有3-6个碳原子和0-3个杂原子的脂环族或杂环，条件是只有一个R2和R5是氢; R3是具有1-18个碳原子的直链烷基或支链烷基; 和R 4是氢，或具有1-10个碳原子的烷基，芳基，芳烷基或支链烷基。

2. 发明申请

US20120323024A1 KETAL ESTERS OF OXOCARBOXYLIC ACIDS AND PROCESS OF MAKING 有权
标题翻译：羟基羧酸的酯盐和制备方法
公开(公告)号：US20120323024A1
公开(公告)日：2012-12-20
申请号：US13395317
申请日：2010-09-13
申请人： Douglas A. Wicks , Sergey Selifonov , Marc Davis Scholten
发明人： Douglas A. Wicks , Sergey Selifonov , Marc Davis Scholten
IPC分类号： C07D317/24 , C07D319/06
CPC分类号： C07D317/14
摘要： A ketal ester of an oxocarboxylic acid and a process to make the same, where the ketal ester is of Structure (I): wherein a is 0 or an integer from 1 to 12; n is 0 or 1; R1 is a linear alkyl, aryl, arylalkylene, or branched alkyl group with 1-18 carbon atoms; R2 and R5 can be hydrogen, C1-6 straight chain or branched alkyl, phenyl, substituted phenyl, C1-6 alkyl substituted with up to four OH groups, C1-6 alkyl, or acetyl optionally substituted hydrocarbon radicals, or R2 and R4 together with the α-carbon form a cycloaliphatic or heterocyclic ring with 3-6 carbon atoms and 0-3 heteroatoms, provided that only one of R2 and R5 is hydrogen; R3 is a linear alkyl or branched alkyl group with 1-18 carbon atoms; and R4 is hydrogen, or an alkyl, aryl, aralkyl or branched alkyl group with 1-10 carbon atoms.
摘要翻译：一种氧代羧酸的缩酮酯及其制备方法，其中缩酮为结构式（I）：其中a为0或1至12的整数; n为0或1; R1是具有1-18个碳原子的直链烷基，芳基，芳基亚烷基或支链烷基; R 2和R 5可以是氢，C 1-6直链或支链烷基，苯基，取代的苯基，被至多四个OH基取代的C 1-6烷基，C 1-6烷基或乙酰基任选取代的烃基，或者R 2和R 4一起与α-碳形成具有3-6个碳原子和0-3个杂原子的脂环族或杂环，条件是只有一个R2和R5是氢; R3是具有1-18个碳原子的直链烷基或支链烷基; 和R 4是氢，或具有1-10个碳原子的烷基，芳基，芳烷基或支链烷基。

3. 发明授权

US08546519B2 Polyketal compounds, synthesis, and applications 有权
标题翻译：聚缩酮化合物，合成和应用
公开(公告)号：US08546519B2
公开(公告)日：2013-10-01
申请号：US12682267
申请日：2008-10-09
申请人： Sergey Selifonov , Scott D. Rothstein , Douglas A. Wicks , Brian D. Mullen , Tara J. Mullen , Jason D. Pratt , Charles T. Williams , Chunyong Wu , Ning Zhou
发明人： Sergey Selifonov , Scott D. Rothstein , Douglas A. Wicks , Brian D. Mullen , Tara J. Mullen , Jason D. Pratt , Charles T. Williams , Chunyong Wu , Ning Zhou
IPC分类号： C08G4/00 , C08G63/00 , C08G65/34
CPC分类号： C08G63/672 , C07D493/04 , C07D493/06 , C07D493/10 , C07D493/12 , C08L25/06 , C08L27/06 , C08L59/00 , C08L67/04 , C08L2666/14 , C08L2666/04
摘要： The invention relates to polyketal compounds. The compounds are synthesized by the selective ketalization of oxocarboxylic acids, e.g. keto acids and semialdehydes, and esters thereof with tetrols and higher polyols that products two or more cyclic ketal ester moieties per molecule, wherein the cyclic ketal moieties are situated in a bis-, tris-, or polyketal conformation. The invention further relates to applications of these compounds and subsequent reactions thereof.
摘要翻译：本发明涉及聚缩酮化合物。这些化合物是通过氧化羧酸的选择性缩酮化合成的。酮酸和半醛，以及其与四元醇和高级多元醇的酯，其每分子产生两个或多个环状缩酮酯部分，其中环状缩酮部分位于双 - ，三 - 或多缩醛构象。本发明还涉及这些化合物的应用及其后续反应。

4. 发明授权

US08604223B2 Method of making ketals and acetals 有权
标题翻译：缩酮和缩醛的制备方法
公开(公告)号：US08604223B2
公开(公告)日：2013-12-10
申请号：US12757065
申请日：2010-04-09
申请人： Sergey Selifonov , Scott D. Rothstein , Brian D. Mullen
发明人： Sergey Selifonov , Scott D. Rothstein , Brian D. Mullen
IPC分类号： C07D317/20
CPC分类号： C07D407/12 , C07D317/14
摘要： The reaction of alcohols with oxocarboxylates to form acetals or ketals is catalyzed by unexpectedly low levels of protic acids. By employing low acid catalyst levels compared to amounts conventionally used, rapid formation of acetal or ketal is facilitated while the formation of oxocarboxylate esters is minimized. Further employing a significant molar excess of oxocarboxylate in conjunction with low acid catalyst level gives rise to the rapid and clean formation of acetals and ketals from oxocarboxylates and alcohols.
摘要翻译：醇与氧代羧酸酯反应形成缩醛或缩酮反应由意想不到的低水平的质子酸催化。通过使用与常规使用的量相比低的酸催化剂水平，促进缩醛或缩酮的快速形成，同时氧化羧酸酯的形成最小化。进一步使用显着摩尔过量的氧代羧酸酯与低酸催化剂水平相结合，导致来自氧代羧酸酯和醇的缩醛和缩酮的快速和清洁的形成。

5. 发明申请

US20080050782A1 Methods for making character strings, polynucleotides and polypeptides having desired characteristics 有权
公开(公告)号：US20080050782A1
公开(公告)日：2008-02-28
申请号：US11975638
申请日：2007-10-18
申请人： Sergey Selifonov , Willem Stemmer , Claes Gustafsson , Matthew Tobin , Stephen Cardayre , Phillip Patten , Jeremy Minshull , Lorraine Giver
发明人： Sergey Selifonov , Willem Stemmer , Claes Gustafsson , Matthew Tobin , Stephen Cardayre , Phillip Patten , Jeremy Minshull , Lorraine Giver
IPC分类号： C12P19/34 , C40B30/02 , C40B60/04
CPC分类号： G06F19/16 , B01J2219/007 , C40B50/02 , G06F19/14 , G06F19/18 , G06F19/22 , G06F19/24
摘要： In silico nucleic acid recombination methods, related integrated systems utilizing genetic operators and libraries made by in silico shuffling methods are provided.

6. 发明申请

US20060155153A1 Methods for making(-)-menthol and oxygenated menthane compounds 审中-公开
标题翻译：（ - ） - 薄荷醇和含氧薄荷烷化合物的制备方法
公开(公告)号：US20060155153A1
公开(公告)日：2006-07-13
申请号：US10523050
申请日：2003-07-24
申请人： Sergey Selifonov
发明人： Sergey Selifonov
IPC分类号： C12P7/12 , C12P7/02
CPC分类号： C12P41/002 , C07B2200/07 , C07C29/172 , C07C2601/16 , C12P7/02 , C07C35/12
摘要： Processes are described for the preparation of (−) menthol from 4R-(+)-menthene or from (+)-limonene, wherein the starting material is hydroxylated using a catalyst comprising at least on polypeptide to form trans-piperitol or trans-isopiperitenol, respectively, followed by hydrogenation to from (−)-menthol.
摘要翻译：描述了用于从4R - （+） - 薄荷烯或（+） - 柠檬烯制备（ - ）薄荷醇的方法，其中使用至少包含多肽的催化剂将起始物质羟基化以形成反式胡椒醇或反式异戊二醇，然后氢化成（ - ） - 薄荷醇。

7. 发明申请

US20130085201A1 KETAL LACTONES AND STEREOSPECIFIC ADDUCTS OF OXOCARBOXYLIC KETALS WITH TRIMETHYLOL COMPOUNDS, POLYMERS CONTAINING THE SAME, METHODS OF MANUFACTURE, AND USES THEREOF 审中-公开
标题翻译：含三羧甲基化合物的聚氧乙烯酮的硬脂酸酯和立体化学添加剂，含有它们的聚合物，制造方法及其用途
公开(公告)号：US20130085201A1
公开(公告)日：2013-04-04
申请号：US13497345
申请日：2010-09-27
申请人： Sergey Selifonov , Ning Zhou , Brian D. Mullen
发明人： Sergey Selifonov , Ning Zhou , Brian D. Mullen
IPC分类号： C07D493/08 , C08G63/06 , C08L67/04 , C07D319/06 , C07D493/18
CPC分类号： C07D493/08 , C07D319/06 , C07D493/18 , C08G18/4269 , C08G63/06 , C08G63/664 , C08L67/04
摘要： Ketal lactones of and methods for making such ketal lactones are disclosed. Also described are methods for making isolated cis- and trans-stereoisomers of hydroxyester ketals of oxocarboxylic acids and polymers having ketal units of such stereoisomers within the polymer backbone.
摘要翻译：公开了酮缩酮内酯和制备此类缩酮内酯的方法。还描述了在聚合物主链中制备具有氧代羧酸的羟酯缩酮的分离的顺式和反式立体异构体和具有这种立体异构体的缩酮单元的聚合物的方法。

8. 发明授权

US08084635B2 Glyceryl ether compounds and their use 有权
标题翻译：甘油醚化合物及其用途
公开(公告)号：US08084635B2
公开(公告)日：2011-12-27
申请号：US13112070
申请日：2011-05-20
申请人： Sergey Selifonov
发明人： Sergey Selifonov
IPC分类号： C07C69/003
CPC分类号： C07D317/22 , A01N25/30 , C07C43/132 , C07C59/305 , C07C69/708 , C07D307/20 , C07D407/12
摘要： Glyceryl ether compounds prepared by the reaction of glycerol and olefin epoxides are disclosed. The compounds are renewable biomass-based surfactants useful as detergents and emulsifiers in formulations for cleaning, laundry, personal care, cosmetics, and industrial uses.
摘要翻译：公开了通过甘油和烯烃环氧化物的反应制备的甘油醚化合物。这些化合物是可用作清洁剂，洗衣，个人护理，化妆品和工业用途的制剂中的洗涤剂和乳化剂的可再生生物质基表面活性剂。

9. 发明授权

US08053468B2 Glycerol levulinate ketals and their use 有权
标题翻译：甘油乙酰丙酮缩酮及其用途
公开(公告)号：US08053468B2
公开(公告)日：2011-11-08
申请号：US11915549
申请日：2006-11-22
申请人： Sergey Selifonov
发明人： Sergey Selifonov
IPC分类号： A61K31/34 , C07D317/22
CPC分类号： C08G18/4283 , C07D317/30 , C07D493/08 , C07D493/18 , Y10T428/139
摘要： The present disclosure relates to the preparation of ketal compounds from glycerol and levulinic acid and esters, and uses thereof.
摘要翻译：本公开涉及由甘油和乙酰丙酸和酯制备缩酮化合物及其用途。

10. 发明申请

US20110082264A1 TRANSKETALIZED COMPOSITIONS, SYNTHESIS, AND APPLICATIONS 有权
标题翻译：复合组合物，合成和应用
公开(公告)号：US20110082264A1
公开(公告)日：2011-04-07
申请号：US12988034
申请日：2009-04-16
申请人： Sergey Selifonov , Adam Edward Goetz , Feng Jing
发明人： Sergey Selifonov , Adam Edward Goetz , Feng Jing
IPC分类号： C08G69/48 , C08G69/26 , C07D407/14 , C07D407/04 , C07D407/12 , C07D493/10 , C07D493/04 , C07D493/14 , C07D493/22 , C07D493/16
CPC分类号： C07D407/14 , C07D317/12 , C07D317/22 , C07D317/30 , C07D407/04 , C07D407/12 , C07D493/04 , C07D493/10 , C07D493/14 , C07D493/16 , C07D493/18 , C07D493/22 , C08G63/668 , C08G69/26 , C08G69/28 , C08G69/44 , C08G69/48 , C08L77/06 , C08L77/12
摘要： The present disclosure relates to the preparation of ketal compounds from polyols and oxocarboxylates, and uses thereof.
摘要翻译：本公开涉及由多元醇和氧代羧酸盐制备缩酮化合物及其应用。

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