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    • 2. 发明授权
    • Method of controlling the mobility of flows through fissures, slits or
pores
    • 控制流经裂缝,狭缝或孔隙的流动性的方法
    • US4584109A
    • 1986-04-22
    • US584648
    • 1984-02-29
    • Raimund HaasDieter OhlendorfWerner Interthal
    • Raimund HaasDieter OhlendorfWerner Interthal
    • B01F17/18C09K3/00C09K8/86E21B43/16
    • C09K8/86C09K3/00Y10S507/936
    • Method of controlling the mobility of aqueous flows through fissures, slits or pores, in particular of flooding waters in tertiary production of crude oil, wherein cationic surfactants which, on measurement of the electric birefringence with a pulsed rectangular electrical field in pure aqueous solutions, give a measurement signal, from the decrease of which a relaxation time of 0.01 .mu.s to 10 ms, in particular of 0.1 .mu.s to 2 ms, results, are added to the aqueous medium. Preferred suitable cationic compounds are those of the general formulaR.sub.1 --K.sup.+ A.sup.-in which R.sub.1 denotes C.sub.12 -C.sub.26 -alkyl or C.sub.12 -C.sub.26 -alkenyl, K.sup.+ denotes a group of the formula ##STR1## R.sub.2 denotes C.sub.1 -C.sub.3 -alkyl, preferably methyl, R'.sub.2 denotes C.sub.1 -C.sub.3 -alkyl, preferably methyl, R".sub.2 denotes C.sub.1 -C.sub.3 -alkyl, preferably methyl, or R".sub.2 denotes (CH.sub.2 CH.sub.2 O).sub.x H, where x denotes from 1 to 3, preferably 1 to 2, and A.sup.- denotes an anion of the following formulae: SCN.sup.31, R.sub.3 SO.sub.3.sup.-, where R.sub.3 is C.sub.6 -C.sub.9 -alkyl or -alkenyl and the sum of the carbon atoms in R.sub.1 and R.sub.3 should be at least 21; ##STR2## where Hal is chlorine or bromine, R.sub.4 is C.sub.1 -C.sub.5 -alkyl, C.sub.2 -C.sub.5 -alkenyl or C.sub.1 -C.sub.5 -alkoxy in positions 3, 4, 5 and 6 and R.sub.5 is hydrogen or hydroxyl in positions 2 and 3 relative to the carboxyl group, or ##STR3## where R.sub.6 is COO.sup.- or SO.sub.3.sup.- and R.sub.7 is hydrogen or methyl.
    • 控制流过裂缝,狭缝或孔隙,特别是原油三次生产中淹水的水流动性的方法,其中在纯水溶液中用脉冲矩形电场测量电双折射的阳离子表面活性剂给出 从水性介质中加入0.01μs至10ms的弛豫时间,特别是0.1μs至2ms的测量信号。 优选的合适的阳离子化合物是通式R 1 -K + A的那些,其中R 1表示C 12 -C 26 - 烷基或C 12 -C 26 - 烯基,K +表示下式的基团:R 2表示C 1 -C 3 - 烷基, 优选甲基,R'2表示C1-C3-烷基,优选甲基,R'2表示C1-C3-烷基,优选甲基,或R'2表示(CH2CH2O)xH,其中x表示1至3,优选 1〜2,A-表示下式的阴离子:SCN31,R3SO3-,其中R3为C6-C9 - 烷基或 - 烯基,R1和R3中的碳原子之和应至少为21; 其中Hal是氯或溴,R4是3,4,5和6位的C1-C5-烷基,C2-C5-烯基或C1-C5-烷氧基,R5是氢或羟基 位置2和3相对于羧基,或其中R6是COO-或SO3-,R7是氢或甲基。
    • 10. 发明授权
    • Process for producing ferroelectric liquid-crystal cells
    • 铁电液晶电池的制造方法
    • US5361152A
    • 1994-11-01
    • US949839
    • 1993-02-05
    • Takamasa HaradaClaus EscherGerhard IllianDieter OhlendorfHeinz RiegerNorbert Rosch
    • Takamasa HaradaClaus EscherGerhard IllianDieter OhlendorfHeinz RiegerNorbert Rosch
    • G02F1/13G02F1/1333G02F1/1339G02F1/1341
    • G02F1/1341
    • A process for producing a liquid-crystal cell which comprises the steps of:(a) providing a curable sealant portion in the periphey of the side of an electrode plate that has an electrode or electrodes;(b) (i) coating a ferroelectric liquid-crystal composition on the portion surrounded by said sealant portion, with a spacer being preliminarily provided in said portion;(ii) coating spacer-containing ferroelectric liquid-crystal composition on the portion surrounded by said sealant portion; or(iii) coating a ferroelectric liquid-crystal composition on the portion surrounded by said sealant portion and thereafter providing a spacer over said composition;(c) defoaming the coated layer of the liquid-crystal composition by heating during or after evacuation;(d) placing the other electrode plate in such a way that the side of said other electrode plate which has an electrode or electrodes faces the side of said one electrode plate containing the thermally defoamed coated layer of the liquid-crystal composition and compressing the two electrode plates together; and(e) curing said sealant.
    • PCT No.PCT / JP91 / 00805 Sec。 371日期:1993年2月5日 102(e)日期1993年2月5日PCT提交1991年6月14日PCT公布。 公开号WO91 / 20011 PCT 日本1991年12月26日。一种液晶盒的制造方法,其特征在于,包括以下步骤:(a)在具有电极或电极的电极板的侧面的外周设置可固化的密封剂部分; (b)(i)在由所述密封剂部分包围的部分上涂覆铁电液晶组合物,预先在所述部分中设置间隔物; (ii)在由所述密封剂部分包围的部分上涂布含有间隔物的铁电液晶组合物; 或(iii)在由所述密封剂部分包围的部分上涂覆铁电液晶组合物,然后在所述组合物上提供间隔物; (c)在抽空期间或之后通过加热使液晶组合物的涂层消泡; (d)将另一个电极板放置成使得具有电极或电极的所述另一个电极板的侧面面向包含液晶组合物的热消泡涂层的所述一个电极板的侧面并压缩两个 电极板在一起; 和(e)固化所述密封剂。