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1. 发明授权

US4179450A Process for the preparation of 1-acylamino-5(8)-chloroanthraquinones 失效
标题翻译：制备1-酰基氨基-5（8） - 氯蒽醌的方法
公开(公告)号：US4179450A
公开(公告)日：1979-12-18
申请号：US794143
申请日：1977-05-05
申请人： Detlef-Ingo Schutze , Hans-Samuel Bien, deceased , Petra Bien, heir , Daniel Bien, heir
发明人： Detlef-Ingo Schutze , Hans-Samuel Bien, deceased , Petra Bien, heir , Daniel Bien, heir
IPC分类号： C07C225/34 , C07C233/07 , C07C233/33 , C07C233/43 , C09B1/22 , C09B1/36 , C07C97/24 , C07C103/75
CPC分类号： C09B1/22 , C09B1/36
摘要： The invention relates to a novel process for the preparation of 1-acylamino-5(8)-chloroanthraquinones, which are starting materials for the preparation of vat dyes. It is characterized in that 1,5(8)-dichloroanthraquinones is reacted with ammonia at temperatures of 190.degree. to 240.degree. C., the amino groups in the reaction mixture are completely acylated and the more sparingly soluble diacylaminoanthraquinone is separated off from the more readily soluble monoacylaminochloroanthraquinone.The new process yields reaction products which are purer and cheaper than those which are obtained by conventional methods. Moreover there are smaller waste water problems.
摘要翻译：本发明涉及一种制备1-酰基氨基-5（8） - 氯蒽醌的新方法，它是制备还原染料的起始原料。其特征在于，在190〜240℃的温度下，使1,5（8） - 二氯蒽醌与氨反应，反应混合物中的氨基被完全酰化，并且更多的微溶于二酰基氨基蒽醌与更多的易溶单酰基氨基氯蒽醌。新方法产生的反应产物比通过常规方法获得的产物更纯净和便宜。此外还有较小的废水问题。

2. 发明授权

US4220779A Process for the preparation of quinoline derivatives 失效
标题翻译：喹啉衍生物的制备方法
公开(公告)号：US4220779A
公开(公告)日：1980-09-02
申请号：US920778
申请日：1978-06-30
申请人： Volker Ehrig , Hans-Samuel Bien, deceased , Erich Klauke , Detlef-Ingo Schutze
发明人： Volker Ehrig , Hans-Samuel Bien, deceased , Erich Klauke , Detlef-Ingo Schutze
IPC分类号： C07D215/48 , C07D215/04 , C07D215/20 , C07D215/36 , C07D215/54 , C07D219/02 , C07D215/12 , C07D215/14 , C07D215/18
CPC分类号： C07D215/04 , C07D215/20 , C07D215/36 , C07D215/54 , C07D219/02
摘要： Quinoline derivatives, especially those of the formula ##STR1## wherein X represents halogen, nitro or CF.sub.3,Z represents hydrogen, alkyl or aryl,Y represents hydrogen, OH, CN, COR or SO.sub.3 H,R represents alkyl, alkoxy or aryl andn represents an integer from 0 to 4,are obtained in high yields when corresponding aromatic orthodichloromethyl isocyanates are converted by hydrolysis and decarboxylation into the corresponding ortho-aminoaldehydes and these are subjected to a condensation reaction with carbonyl compounds containing an active .alpha.-methylene group.The process products are starting materials for dyestuffs, insecticides and others.
摘要翻译：喹啉衍生物，特别是式的那些，其中X表示卤素，硝基或CF 3，Z表示氢，烷基或芳基，Y表示氢，OH，CN，COR或SO 3 H，R表示烷基，烷氧基或芳基，n表示当相应的芳族二氯甲基异氰酸酯通过水解和脱羧转化成相应的邻氨基醛时，以高产率获得0-4的整数，并且它们与含有活性α-亚甲基的羰基化合物进行缩合反应。工艺产品为染料，杀虫剂等原料。

3. 发明授权

US4812568A Process for the preparation of 6,13-dihydroquinacridones and quinacridones 失效
标题翻译：制备6,13-二氢喹吖啶酮和喹吖啶酮的方法
公开(公告)号：US4812568A
公开(公告)日：1989-03-14
申请号：US12921
申请日：1987-02-10
申请人： Helmut Herzog , Detlef-Ingo Schutze , Jurgen Schneider , Reinold Schmitz
发明人： Helmut Herzog , Detlef-Ingo Schutze , Jurgen Schneider , Reinold Schmitz
IPC分类号： C07D471/04 , C09B48/00
CPC分类号： C07D471/04 , C09B48/00
摘要： Process for the preparation of a 6,13-dihydroquinacridone of the general formula (I) ##STR1## in which R.sup.1, R.sup.2, R.sup.3 and R.sup.4 designate hydrogen or substituents customary for quinacridone, characterized in that an optionally substituted dialkyl 2,5-di-(phenylamino)-3,6-dihydroterephthalate is heated to temperatures of 240.degree.-320.degree. C. in an essentially oxygen-free atmosphere in the presence of a dimethyl-diphenyl ether isomer mixture of the formula ##STR2## as the solvent and/or diluent, and a process for the preparation of optionally substituted quinacridone, characterized in that the resulting 6,13-dihydroquinacridone is oxidized in the customary manner.
摘要翻译：用于制备通式（I）的化合物（I）的6,13-二氢喹吖啶酮的方法其中R 1，R 2，R 3和R 4表示氢或通常用于喹吖啶酮的取代基，其特征在于任选取代的二烷基2，将5-二 - （苯基氨基）-3,6-二氢对苯二甲酸酯在基本上不含氧的气氛中在二甲基 - 二苯基醚异构体混合物存在下加热到240-320℃的温度，式 II）和/或作为溶剂和/或稀释剂的（IIa）和/或制备任选取代的喹吖啶酮的方法，其特征在于所得的6,13-二氢喹吖啶酮以常规方式被氧化。

4. 发明授权

US4435589A Process for the preparation of dimethyl succinylosuccinate, the disodium salt thereof, dianilinodihydroterephthalic acids, the dimethyl esters and salts thereof, and dianilinoterephthalic acids, and the dimethyl esters and salts thereof 失效
标题翻译：制备二琥珀酸琥珀酸二甲酯，其二钠盐，二苯胺二氢对苯二甲酸，其二甲酯和盐，以及二苯胺基对苯二甲酸的方法及其二甲酯及其盐
公开(公告)号：US4435589A
公开(公告)日：1984-03-06
申请号：US341047
申请日：1982-01-21
申请人： Meinhard Rolf , Detlef-Ingo Schutze , Rutger Neeff , Hans-Volker Runzheimer
发明人： Meinhard Rolf , Detlef-Ingo Schutze , Rutger Neeff , Hans-Volker Runzheimer
IPC分类号： C07C69/90 , C07C67/00 , C07C69/757 , C07C69/95 , C07C227/00 , C07C227/08 , C07C227/16 , C07C227/18 , C07C229/62 , C07C231/00 , C07C231/12 , C07C237/30 , C07C101/38 , C07C101/68 , C07C103/76
CPC分类号： C07C69/95
摘要： Process for the preparation of dimethyl succinylosuccinate, or the disodium salt thereof, by condensation of dimethyl succinate in a 35-45 percent by weight solution of sodium methylate in methanol, and a process for the preparation of dianilinodihydroterephthalic acids, the dimethyl esters and salts thereof, and of dianilinoterephthalic acids, and the dimethyl esters and salts thereof, starting from the disodium salt of dimethyl succinylosuccinate prepared according to the new process, without intermediate isolation.
摘要翻译：通过琥珀酸二甲酯在35-45重量％甲醇钠的甲醇溶液中缩合制备二甲基琥珀酸琥珀酸酯或其二钠盐的方法，以及制备二苯胺二氢对苯二甲酸的方法，其二甲酯和其盐，以及二苯胺基对苯二甲酸及其二甲酯及其盐，其由根据新方法制备的二甲基琥珀酸二琥珀酸二钠盐开始，无需中间分离。

5. 发明授权

US5738912A Dispersion of post-curable coating compounds 失效
标题翻译：后固化涂料化合物的分散
公开(公告)号：US5738912A
公开(公告)日：1998-04-14
申请号：US760093
申请日：1996-12-11
申请人： Eberhard Konig , Detlef-Ingo Schutze , Josef Pedain
发明人： Eberhard Konig , Detlef-Ingo Schutze , Josef Pedain
IPC分类号： C08G18/08 , C08G18/12 , C08G18/28 , C08G18/44 , C14C11/00 , D06N3/14 , B05D7/12
CPC分类号： D06N3/14 , C08G18/0804 , C08G18/12 , C08G18/283 , C08G18/44 , C14C11/006
摘要： The invention relates to a method for coating textiles and/or leather with an aqueous dispersion comprising (A) a mixture of (i) a urethane-containing blocked NCO prepolymer having a number average molecular weight of 2000 to 10,000, a content of blocked isocyanate groups (calculated as NCO) of 0.5 to 5 wt. %, an ethoxy group content of 2 to 50 wt. %, an ionic group content of 5 to 30 meq per 100 g of the prepolymer, and (ii) a polyamine having (cyclo)aliphatically bonded primary and/or secondary amino groups, wherein the equivalent ratio of blocked NCO groups of component (i) to amino groups of component (ii) is 1:0.9 to 1:1.2, and (B) an aqueous phase.
摘要翻译：本发明涉及一种用水分散体涂布纺织品和/或皮革的方法，其包含（A）（i）数均分子量为2000至10,000的含氨基甲酸酯的封闭NCO预聚物，封端异氰酸酯的含量基团（以NCO计算）为0.5〜5wt。％，乙氧基含量为2〜50wt。％，每100g预聚物的离子基团含量为5至30meq，和（ii）具有（环）脂族键合的伯和/或仲氨基的多胺，其中组分（i）的封闭NCO基团的当量比）至组分（ⅱ）的氨基为1：0.9至1：1.2，和（B）水相。

6. 发明授权

US5252671A Coating compositions for coatings that are permeable to water vapor and a process for their preparation 失效
标题翻译：可渗透水蒸气的涂料涂料组合物及其制备方法
公开(公告)号：US5252671A
公开(公告)日：1993-10-12
申请号：US887213
申请日：1992-05-21
申请人： Josef Pedain , Klaus Noll , Wilhelm Thoma , Detlef-Ingo Schutze
发明人： Josef Pedain , Klaus Noll , Wilhelm Thoma , Detlef-Ingo Schutze
IPC分类号： C14C11/00 , C08L75/00 , C09D133/04 , C09D175/00 , C09D175/04 , D06M15/564 , D06N3/04 , D06N3/14 , C08F8/30
CPC分类号： D06N3/14 , C09D133/04 , C09D175/04 , C08L75/00 , Y10S528/904
摘要： The present invention relates to coating compositions containing(A) 70 to 98% by weight, based on the sum of components (A) and (B), of(a) isocyanate-free polymers of ethylenically unsaturated monomers and/or polyurethanes or blocked isocyanate prepolymers, and(b) optional organic solvents, wherein component (A) contains no significant quantities of groups capable of reacting with component (B) or starting materials thereof and has a viscosity (at 23.degree. C.) of 2000 to 100,000 mPa.s;(B) 2 to 30% by weight, based on the sum of components (A) and (B), of a polyaddition product prepared in and dispersed in component (A), wherein the polyaddition product is a polyurethane, polyurethane urea, polyurea, or mixture thereof, containing ionic groups and/or potentially ionic groups in a quantity corresponding to from 0.5 to 20 milliequivalents per 100 g of component (B) but containing substantially no free isocyanate, hydroxyl, or amino groups: and(C) optional cross-linking agents;in which component (B) is formed in situ in component (A).
摘要翻译：本发明涉及涂料组合物，其包含（A）70至98重量％，基于组分（A）和（B）的总和，（a）烯属不饱和单体和/或聚氨酯或封闭的无异氰酸酯的聚合物异氰酸酯预聚物和（b）任选的有机溶剂，其中组分（A）不含有显着量的能够与组分（B）或其原料反应的基团，并且具有2000至100,000mPa的粘度（在23℃） .s; （B）基于组分（A）和（B）的总和，制备和分散在组分（A）中的加聚产物的2-30重量％，其中所述加聚产物是聚氨酯，聚氨酯脲，聚脲或其混合物，其含有相对于每100g组分（B）0.5至20毫当量但基本上不含游离异氰酸酯，羟基或氨基的量的离子基团和/或潜在的离子基团：和（C）任选的交联剂; 其中组分（B）在组分（A）中原位形成。

7. 发明授权

US4652660A Process for preparing a thioindigo derivatives comprising cyclizing in a liquid mixture of an aluminium halide an alkali metal halide, and a carboxamide or sulfonamide 失效
标题翻译：制备硫靛衍生物的方法，其包括在卤化铝和碱金属卤化物的液体混合物中环化，以及羧酰胺或磺酰胺
公开(公告)号：US4652660A
公开(公告)日：1987-03-24
申请号：US755048
申请日：1985-07-15
申请人： Detlef-Ingo Schutze , Klaus Wunderlich
发明人： Detlef-Ingo Schutze , Klaus Wunderlich
IPC分类号： C09B7/10 , C07D333/64 , C07D409/04
CPC分类号： C09B7/10
摘要： Process for preparing thioindigo compounds of the formula ##STR1## in which A and B denote identical or different, optionally substituted benzene rings or benzene rings to which may be joined further carbocyclic and heterocyclic rings,characterized in that compounds of the formulae ##STR2## in which A and B have the abovementioned meaning andX denotes halogen, such as bromine and preferably chlorine,are reacted in a liquid mixture of an aluminium halide, an alkali metal halide and a carboxamide or sulphonamide, and the resulting intermediate product is subsequently, if desired after prior isolation, oxidized in a manner known per se, and the batch is worked up for the compounds of the formula (I).
摘要翻译：制备式（I）的硫靛化合物的方法，其中A和B表示相同或不同的任选取代的苯环或苯环，其中可以连接有碳环和杂环，其特征在于式其中A和B具有上述含义并且X表示卤素如溴，优选氯，在卤化铝，碱金属卤化物的液体混合物中反应的图像（IIa）和/或

8. 发明申请

US20060128885A1 High-solids polyurethane-polyurea dispersions 审中-公开
标题翻译：高固体聚氨酯 - 聚脲分散体
公开(公告)号：US20060128885A1
公开(公告)日：2006-06-15
申请号：US11298345
申请日：2005-12-08
申请人： Thorsten Rische , Gerald Kurek , Holger Casselmann , Thomas Feller , Thomas Munzmay , Detlef-Ingo Schutze , Harald Blum , Hans-Georg Muller
发明人： Thorsten Rische , Gerald Kurek , Holger Casselmann , Thomas Feller , Thomas Munzmay , Detlef-Ingo Schutze , Harald Blum , Hans-Georg Muller
IPC分类号： C08G18/08
CPC分类号： C08G18/6659 , C08G18/0823 , C08G18/0828 , C08G18/10 , C08G18/12 , C08G18/283 , C08G18/4238 , C08G18/44 , C08G18/755 , C09D175/04 , C08G18/3228 , C08G18/3857 , C08G18/3855 , C08G18/3231 , C08G18/305 , C08G18/3225
摘要： The present invention relates to aqueous polyurethane-polyurea dispersions having two discrete maxima in the particle size distribution, wherein the maximum of the fine fraction is between 51 and 150 nm and the maximum of the coarse fraction is between 160 and 700 nm. The present invention also relates to a process for preparing the polyurethane-polyurea dispersions, to coating compositions containing these polyurethane-polyurea dispersions, and to coated substrates prepared from these coating compositions.
摘要翻译：本发明涉及在粒度分布中具有两个离散最大值的水性聚氨酯 - 聚脲分散体，其中细小部分的最大值为51-150nm，粗分数的最大值为160-700nm。本发明还涉及制备聚氨酯 - 聚脲分散体的方法，包含这些聚氨酯 - 聚脲分散体的涂料组合物以及由这些涂料组合物制备的涂布基材。

9. 发明授权

US5747582A Aqueous coating compositions and their use for the preparation of coatings that are permeable to water vapor 失效
标题翻译：水性涂料组合物及其用于制备可渗透水蒸气的涂料的用途
公开(公告)号：US5747582A
公开(公告)日：1998-05-05
申请号：US460178
申请日：1995-06-02
申请人： Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp , Josef Pedain , Reinold Schmitz
发明人： Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp , Josef Pedain , Reinold Schmitz
IPC分类号： C08G18/08 , C08G18/28 , C08G18/44 , C08G18/50 , C14C11/00 , D06N3/14 , D21H19/62 , C08J3/00 , C08K3/20 , C08L75/00
CPC分类号： C08G18/0823 , C08G18/0804 , C08G18/0828 , C08G18/283 , C08G18/3228 , C08G18/3231 , C08G18/3855 , C08G18/44 , C08G18/5072 , C08G18/73 , C14C11/006 , D06N3/14 , D21H19/62 , Y10T428/31551 , Y10T428/31558 , Y10T428/31591
摘要： The invention relates to coating compositions used to prepare coatings having water vapor permeabilities of at least 2500 g/m.sup.2 per day (DS 2109 TM1 method) containing (A) a polyurethane containing (1) 0.1 to 75 meq/100 g of ionic groups and (2) 11 to 50% by weight of --(CH.sub.2 CH.sub.2 O).sub.n -- units (wherein n is 2 to 25) incorporated into the main chain prepared from reactive components comprising (I) one or more polyisocyanates, (II) one or more polyols having a number average molecular weight of 350 to 5000, with the proviso that if any such polyol is a sulfonated polyether diol having the formula ##STR1## in which R is hydrogen or an organic group having 1 to 8 carbon atoms, m and n are 1 to 10, p is 0, 1, or 2, and M is ammonium or alkali metal cation, then an additional ethoxy-containing polyether polyol must also be present, and (III) one or more chain lengthening agents having a molecular weight of 32 to 349; and (B) 30 to 80% by weight, based on the sum of components (A) and (B), of an aqueous phase.
摘要翻译：本发明涉及用于制备具有每天至少2500g / m 2的水蒸汽渗透性（DS 2109 TM1方法）的涂层的涂料组合物，其包含（A）含有（1）0.1至75meq / 100g离子基团的聚氨酯和（2）由反应性组分制备的包含（I）一种或多种多异氰酸酯的主链中的 - （CH 2 CH 2 O）n-单元（其中n为2至25）的11至50重量％，（II）一种或多种多元醇数均分子量为350至5000，条件是如果任何这样的多元醇是具有式“IMAGE”的磺化聚醚二醇，其中R是氢或具有1至8个碳原子的有机基团，m和n分别为 1至10，p为0,1或2，M为铵或碱金属阳离子，则还必须含有另外的含乙氧基的聚醚多元醇，和（III）一种或多种链增长剂，其分子量为 32至349; 和（B）基于水相的组分（A）和（B）的总和为30至80重量％。

10. 发明授权

US5078794A Process for preparing 4,4'-diamino-1,1'-dianthraquinonyl pigments 失效
标题翻译：制备4,4'-二氨基-1,1'-二氨基乙酸染料的方法
公开(公告)号：US5078794A
公开(公告)日：1992-01-07
申请号：US573522
申请日：1990-08-27
申请人： Detlef-Ingo Schutze , Werner Steinbeck , Anton Adams
发明人： Detlef-Ingo Schutze , Werner Steinbeck , Anton Adams
IPC分类号： C09B1/16 , B01F17/08 , C09B1/00 , C09B67/14
CPC分类号： C09B1/005
摘要： Process for preparing 4,4'-diamino-1,1'-dianthraquinonyl pigments by desulphonation of 4,4'-diamino-1,1'-dianthraquinonyl-3,3'-disulphonic acid in sulphuric acid, characterized in that after the desulphonation water is added to the sulphuric acid solution, 4,4'-diamino 1,1'-dianthraquinonyl is isolated as sulphate, the sulphate is hydrolysed, if necessary by redissolving it in sulphuric acid and adding the solution to water, and the pigment is isolated, if necessary, after treatment with an organic solvent.

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