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1. 发明申请

WO2020159792A1 MEASUREMENT OF PRESSURE DIFFERENCES WITHIN A VESSEL OF SPIRAL WOUND MEMBRANE MODULES 审中-公开
公开(公告)号：WO2020159792A1
公开(公告)日：2020-08-06
申请号：PCT/US2020/014750
申请日：2020-01-23
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： JONS, Steven D. , FRANKLIN, Luke , TOMLINSON, Ian A.
IPC分类号： B01D63/10 , B01D63/12
摘要： A spiral wound membrane module including a specialized endcap assembly including a connecting conduit defining a passageway extending radially inward from its outer periphery, and a differential pressure sensor connected to the passageway of the connecting conduit.

2. 发明申请

WO2016010755A1 METHOD FOR TREATING FOOD SURFACES WITH QUATERNARY AMMONIUM SALTS 审中-公开
标题翻译：用季铵盐处理食物表面的方法
公开(公告)号：WO2016010755A1
公开(公告)日：2016-01-21
申请号：PCT/US2015/039180
申请日：2015-07-06
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： CURTIS-FISK, Jaime L. , DEO, Puspendu , HUGHES, Stephanie L. , RAJAN, Janardhanan S. , TOMLINSON, Ian A.
IPC分类号： C07D471/04 , C07D519/00 , A23L1/314 , A23L1/315 , A23L3/3463 , A23L3/3526 , A23L1/0534 , A23L3/358
CPC分类号： A23L3/3526 , A23L13/432 , A23L29/262 , A23V2002/00
摘要： A method for reducing bacterial contamination on a food surface. The method comprises applying to the food surface a quaternary ammonium salt and a methylcellulose, The methylcellulose has anhydroglucose units joined by 1-4 linkages wherein hydroxy groups of anhydroglucose units are substituted with methyl groups such that s23/s26 is 0.36 or less, wherein s23 is the molar fraction of anhydroglucose units wherein only the two hydroxy groups in the 2- and 3 -positions of the anhydroglucose unit are substituted with methyl groups and wherein s26 is the molar fraction of anhydroglucose units wherein only the two hydroxy groups in the 2- and 6-positions of the anhydroglucose unit are substituted with methyl groups.
摘要翻译：一种减少食物表面细菌污染的方法。该方法包括向食品表面施用季铵盐和甲基纤维素。甲基纤维素具有通过1-4键连接的脱水葡萄糖单元，其中脱水葡萄糖单元的羟基被甲基取代使得s23 / s26为0.36以下，其中s23 是脱水葡萄糖单元的摩尔分数，其中只有脱水葡萄糖单元的2-和3-位中的两个羟基被甲基取代，并且其中s26是脱水葡萄糖单元的摩尔分数，其中只有2-羟基中的两个羟基在2- 脱水葡萄糖单元的6位被甲基取代。

3. 发明申请

WO2015175258A1 COMPOSITE POLYAMIDE MEMBRANE POST-TREATED WITH NITROUS ACID 审中-公开
标题翻译：复合聚酰胺膜后处理硝酸
公开(公告)号：WO2015175258A1
公开(公告)日：2015-11-19
申请号：PCT/US2015/029141
申请日：2015-05-05
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： PAUL, Mou , JANSMA, Matthew J. , ROY, Abhishek , TOMLINSON, Ian A.
IPC分类号： B01D67/00 , B01D69/12 , B01D71/56
CPC分类号： B01D69/125 , B01D67/0006 , B01D67/0093 , B01D71/56 , B01D2323/40 , B05D3/107 , B05D3/108 , C08G69/48 , C09D177/00
摘要： A method for making a composite polyamide membrane comprising a porous support and a polyamide layer, including the steps of: i) applying a polar solution comprising a polyfunctional amine monomer and a non-polar solution comprising a polyfunctional acyl halide monomer to a surface of a porous support and interfacially polymerizing the monomers to form a polyamide layer; and ii) exposing the thin film polyamide layer to nitrous acid; wherein the method is characterized by at least one of: conducting the interfacial polymerization of step i) in the presence of a subject amine compound, or applying a subject amine compound to the interfacially polymerized polyamide layer prior to step ii), wherein the subject amine compound is different from the polyfunctional acyl halide and polyfunctional amine monomers.
摘要翻译：一种制备包括多孔载体和聚酰胺层的复合聚酰胺膜的方法，包括以下步骤：i）将包含多官能胺单体的极性溶液和包含多官能酰卤单体的非极性溶液施加到多孔载体和界面聚合单体以形成聚酰胺层; 和ii）将薄膜聚酰胺层暴露于亚硝酸; 其特征在于以下至少一个：在主题胺化合物的存在下进行步骤i）的界面聚合，或在步骤ii）之前将主题胺化合物施用于界面聚合的聚酰胺层，其中主题胺化合物与多官能酰卤和多官能胺单体不同。

4. 发明申请

WO2015105631A1 DESALINATION OF AQUEOUS MIXTURE CONTAINING NANO-SIZED PARTICLES USING FOULING RESISTANT REVERSE OSMOSIS MEMBRANE 审中-公开
标题翻译：使用耐反射反渗透膜对含有纳米尺寸颗粒的水性混合物进行脱盐
公开(公告)号：WO2015105631A1
公开(公告)日：2015-07-16
申请号：PCT/US2014/070286
申请日：2014-12-15
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： PAUL, Mou , ROY, Abhishek , TOMLINSON, Ian A.
IPC分类号： B01D61/02 , B01D69/02 , B01D69/12 , B01D71/56
CPC分类号： B01D69/02 , B01D61/025 , B01D61/04 , B01D63/10 , B01D67/0006 , B01D67/0088 , B01D67/0093 , B01D69/10 , B01D69/125 , B01D71/56 , B01D2321/16 , B01D2323/00 , B01D2325/00 , C02F1/441 , C02F2101/10 , C02F2101/12 , C02F2103/04 , C02F2103/346 , Y02A20/131
摘要： A method for treating a NaCl containing aqueous mixture comprising at least 2 ppm of anionic nano particles comprising the step of passing the mixture through a spiral wound element to produce a permeate stream and concentrate stream wherein the concentrate stream has a relatively higher concentration of nano particles than the permeate stream, wherein the spiral wound element includes a composite polyamide membrane comprising a porous support and a thin film polyamide layer, and wherein the membrane is characterized by having: i) a NaCl rejection and a nano particle rejection of at least 99% when tested with an aqueous solution containing 2000 ppm NaCl and 2 ppm anionic nano particles at 25C, pH 8 and 1mPa (150 psi); and ii) a dissociated carboxylate content of at least 0.3 moles/kg of polyamide at pH 9.5 as measured by Rutherford Backscattering (RBS).
摘要翻译：一种用于处理含有至少2ppm阴离子纳米颗粒的含NaCl混合水混合物的方法，包括使混合物通过螺旋缠绕元件以产生渗透物流和浓缩物流的步骤，其中浓缩物流具有相对较高浓度的纳米颗粒其中所述螺旋缠绕元件包括包含多孔载体和薄膜聚酰胺层的复合聚酰胺膜，并且其中所述膜的特征在于具有：i）NaCl排斥和至少99％的纳米颗粒排斥，当用含有2000ppm NaCl和2ppm阴离子纳米颗粒的水溶液在25℃，pH8和1mPa（150psi）下测试时; 和ii）通过卢瑟福反向散射（RBS）测量的在pH9.5下至少0.3摩尔/ kg聚酰胺的解离羧酸盐含量。

5. 发明申请

WO2013101887A2 MICROCAPSULES 审中-公开
标题翻译：微胶囊
公开(公告)号：WO2013101887A2
公开(公告)日：2013-07-04
申请号：PCT/US2012/071738
申请日：2012-12-27
申请人： DOW GLOBAL TECHNOLOGIES LLC , ROHM AND HAAS COMPANY
发明人： TOMLINSON, Ian A. , WAGNER, Nicole L. , ZENG, Fanwen , ASHMORE, John , POLANUYER, Boris , SANDERS, Thomas , LAGANELLA, David
IPC分类号： A01N25/28 , B01J13/14 , B01J13/20 , B01J13/18 , A61K9/50
CPC分类号： A01N43/80 , A01N25/10 , A01N25/28 , A01N25/34 , B01J13/14 , B01J13/206
摘要： A composition is provided, comprising microcapsules, wherein said microcapsules comprise a core and an outer shell, wherein said core comprises one or more water-insoluble compound having melting point above 15°C, wherein said outer shell comprises one or more amino resin that is a reaction product of reactants comprising one or more polyamine and formaldehyde, and wherein said composition further comprises one or more formaldehyde scavenger, one or more reaction product of said amino resin with a formaldehyde scavenger, or a mixture thereof. Also provided is a method of making such a composition.
摘要翻译：提供了包含微胶囊的组合物，其中所述微胶囊包含芯和外壳，其中所述芯包含一种或多种熔点高于15℃的水不溶性化合物，其中所述外壳包含一个或多个氨基树脂，包含一种或多种聚胺和甲醛的反应物的反应产物，其中所述组合物还包含一种或多种甲醛清除剂，所述氨基树脂与甲醛清除剂的一种或多种反应产物或其混合物。还提供了制备这种组合物的方法。

6. 发明申请

WO2015167759A1 COMPOSITE POLYAMIDE MEMBRANE POST-TREATED WITH NITROUS ACID 审中-公开
标题翻译：复合聚酰胺膜后处理硝酸
公开(公告)号：WO2015167759A1
公开(公告)日：2015-11-05
申请号：PCT/US2015/024617
申请日：2015-04-07
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： PAUL, Mou , ROY, Abhishek , TOMLINSON, Ian A. , JANSMA, Matthew J.
IPC分类号： B01D67/00 , B01D69/12 , B01D71/56
CPC分类号： B01D67/0093 , B01D69/125 , B01D71/56
摘要： A method for making a composite polyamide membrane comprising a porous support and a polyamide layer, including the steps of: i) applying a polar solution comprising a polyiunctional amine monomer and a non-polar solution comprising a polyiunctional acyl halide monomer to a surface of a porous support and interfacially polymerizing the monomers to form a polyamide layer; and ii) exposing the thin film polyamide layer to nitrous acid; wherein the method is characterized by at least one of: conducting the interfacial polymerization of step i) in the presence of a subject amine- reactive compound, or applying a subject amine-reactive compound to the interfacially polymerized polyamide layer prior to step ii), wherein the subject amine-reactive compound is different from the polyiunctional acyl halide and polyiunctional amine monomers and is represented by the following formula:
摘要翻译：一种制备包括多孔载体和聚酰胺层的复合聚酰胺膜的方法，包括以下步骤：i）将包含多官能胺单体的极性溶液和包含多官能酰卤单体的非极性溶液施加到多孔载体和界面聚合单体以形成聚酰胺层; 和ii）将薄膜聚酰胺层暴露于亚硝酸; 其特征在于以下至少一个：在主题胺反应性化合物的存在下进行步骤i）的界面聚合，或在步骤ii）之前将主题胺反应性化合物施加到界面聚合的聚酰胺层上，其中主题胺反应性化合物不同于多官能酰基卤和多官能胺单体，并由下式表示：

7. 发明申请

WO2015105636A1 COMPOSITE POLYAMIDE MEMBRANE HAVING AZO CONTENT AND HIGH ACID CONTENT 审中-公开
标题翻译：具有AZO含量和高酸含量的复合聚酰胺薄膜
公开(公告)号：WO2015105636A1
公开(公告)日：2015-07-16
申请号：PCT/US2014/070305
申请日：2014-12-15
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： PAUL, Mou , CIESLINSKI, Robert C. , GERHART, Bruce B. , HAWN, David D. , QIU, XiaoHua , RICKARD, Mark A. , ROSENBERG, Steven , ROY, Abhishek , TOMLINSON, Ian A. , ZU, Chengli
IPC分类号： B01D67/00 , B01D69/12 , B01D71/56
CPC分类号： B01D71/56 , B01D67/0006 , B01D67/0093 , B01D67/0095 , B01D67/0097 , B01D69/02 , B01D69/125 , B01D2323/36 , B01D2323/40
摘要： A thin film composite polyamide membrane comprising a porous support and a thin film polyamide layer characterized by possessing: i) an azo (-N=N-) content of from 0.40% to 1.00%, as measured by pyrolysis gas chromatography; and ii) a dissociated carboxylate content of at least 0.40 mol/kg as measured by RBS at pH 9.5.
摘要翻译：一种薄膜复合聚酰胺薄膜，包括多孔载体和薄膜聚酰胺层，其特征在于具有：i）通过热解气相色谱测定的偶氮（-N = N-）含量为0.40％至1.00％和ii）通过RBS在pH 9.5测量的解离的羧酸盐含量为至少0.40mol / kg。

8. 发明申请

WO2014014666A1 MEMBRANE DERIVED FROM POLYFUNCTIONAL AMINE AND COMBINATION OF DIFFERENT POLYFUNCTIONAL AMINE-REACTIVE MONOMERS 审中-公开
标题翻译：多功能胺衍生的膜和不同多功能胺反应单体的组合
公开(公告)号：WO2014014666A1
公开(公告)日：2014-01-23
申请号：PCT/US2013/049180
申请日：2013-07-03
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： PAUL, Mou , ARROWOOD, Tina L. , CIESLINSKI, Robert C. , JONS, Steven D. , ROSENBERG, Steven , ROY, Abhishek , TOMLINSON, Ian A.
IPC分类号： B01D71/56 , B01D69/12
CPC分类号： B01D67/0006 , B01D61/025 , B01D67/0002 , B01D69/10 , B01D69/12 , B01D69/125 , B01D71/56 , B01D2323/00 , B01D2323/38 , B01D2323/40 , B01D2325/20
摘要： A method for making a composite polyamide membrane including a porous support and a thin film polyamide layer including the steps of applying a polyfunctional amine monomer and a combination amine-reactive compounds to a surface of the porous support and reacting the constituents to form a thin film polyamide layer, wherein the amine-reactive compounds include: i) a polyfunctional amine-reactive monomer including two to three amine-reactive moieties selected from acyl halide, sulfonyl halide and anhydride, ii) a polyfunctional amine-reactive monomer including at least four amine-reactive moieties selected from acyl halide, sulfonyl halide and anhydride, and iii) an acid compound including at least on carboxylic acid moiety or salt thereof and at least one amine-reactive moiety selected from acyl halide and sulfonyl halide.
摘要翻译：一种制造包括多孔载体和薄膜聚酰胺层的复合聚酰胺膜的方法，包括以下步骤：将多官能胺单体和组合胺反应性化合物施加到多孔载体的表面，并使组分反应形成薄膜聚酰胺层，其中胺反应性化合物包括：i）包含选自酰基卤，磺酰卤和酸酐的两个至三个胺反应性部分的多官能胺反应性单体，ii）包含至少四个胺的多官能胺反应性单体 - 选自酰基卤，磺酰卤和酸酐的反应性部分，和iii）至少包含羧酸部分或其盐和至少一种选自酰卤和磺酰卤的胺反应性部分的酸化合物。

9. 发明申请

WO2014014663A1 COMPOSITE POLYAMIDE MEMBRANE 审中-公开
标题翻译：复合聚酰胺膜
公开(公告)号：WO2014014663A1
公开(公告)日：2014-01-23
申请号：PCT/US2013/049177
申请日：2013-07-03
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： ROY, Abhishek , ARROWOOD, Tina L. , CIESLINSKI, Robert C. , STEVENS, Derek M. , HAWN, David D. , JONS, Steven D. , PAUL, Mou , PEERY, Martin H. , ROSENBERG, Steven , TOMLINSON, Ian A.
IPC分类号： B01D69/12 , B01D71/56
CPC分类号： B01D67/0006 , B01D61/025 , B01D67/0002 , B01D69/10 , B01D69/12 , B01D69/125 , B01D71/56 , B01D2323/00 , B01D2323/38 , B01D2323/40 , B01D2325/20
摘要： A method for making a composite polyamide membrane comprising a porous support and a thin film polyamide layer, wherein the method includes the step of applying a polyfunctional amine monomer and polyfunctional acyl halide monomer to a surface of the porous support and interfacially polymerizing the monomers to form a thin film polyamide layer, wherein the step of applying the polyfunctional acyl halide monomer to the porous support includes the step of combining the polyfunctional acyl halide monomer with a non-polar solvent at a concentration of at least 0.18 weight percent to form a coating solution which is applied to the surface of the porous support, and wherein the interfacial polymerization is conducted in the presence of a tri-hydrocarbyl phosphate compound which is provided in a molar ratio of at least 0.5:1 with the polyfunctional acyl halide monomer. Many additional embodiments are described including membranes made from the subject method and applications for such membranes.
摘要翻译：一种制备包含多孔载体和薄膜聚酰胺层的复合聚酰胺膜的方法，其中所述方法包括将多官能胺单体和多官能酰卤单体施用于多孔载体的表面并使单体界面聚合形成的步骤薄膜聚酰胺层，其中将多官能酰基卤单体施加到多孔载体上的步骤包括将多官能酰卤单体与至少0.18重量％浓度的非极性溶剂组合以形成涂布溶液的步骤其施加到多孔载体的表面上，并且其中界面聚合在三官能酰基卤单体的至少0.5:1摩尔比的三烃基磷酸酯化合物的存在下进行。描述了许多另外的实施方案，包括由本方法制备的膜和用于这种膜的膜。

10. 发明申请

WO2013048765A1 COMPOSITE POLYAMIDE MEMBRANE DERIVED FROM CARBOXYLIC ACID CONTAINING ACYL HALIDE MONOMER 审中-公开
标题翻译：由含有ACYL HALIDE MONOMER的羧酸衍生的复合聚酰胺膜
公开(公告)号：WO2013048765A1
公开(公告)日：2013-04-04
申请号：PCT/US2012/055271
申请日：2012-09-14
申请人： DOW GLOBAL TECHNOLOGIES LLC , ROY, Abhishek , JONS, Steven D. , KOOB, Joseph D. , PEERY, Martin H. , QIU, XiaoHua Sam , ROSENBERG, Steven , TOMLINSON, Ian A.
发明人： ROY, Abhishek , JONS, Steven D. , KOOB, Joseph D. , PEERY, Martin H. , QIU, XiaoHua Sam , ROSENBERG, Steven , TOMLINSON, Ian A.
IPC分类号： B01D69/12 , B01D71/56 , B01D67/00
CPC分类号： B01D69/125 , B01D67/0093 , B01D71/56
摘要： A method for making a composite polyamide membrane comprising the step of applying polyfunctional amine and acid halide monomers to a surface of a porous support and interfacially polymerizing the monomers to form a thin film polyamide layer. The method further includes the step of conducting the interfacial polymerization in the presence of: a carboxylic acid monomer comprising an aliphatic or aromatic moiety substituted with single carboxylic acid functional group and at least one acyl halide functional group, and a tri-hydrocarbyl compound.
摘要翻译：一种制备复合聚酰胺膜的方法，包括将多官能胺和酰卤单体施加到多孔载体的表面并使单体界面聚合以形成薄膜聚酰胺层的步骤。该方法还包括在以下存在下进行界面聚合的步骤：包含被单个羧酸官能团和至少一个酰卤官能团取代的脂族或芳族部分的羧酸单体和三烃基化合物。

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