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1. 发明申请

WO2002064102A1 PROCESS FOR THE PREPARATION OF A POLYMERISABLE DENTAL COMPOSITION 审中-公开
标题翻译：制备聚合物牙科组合物的方法
公开(公告)号：WO2002064102A1
公开(公告)日：2002-08-22
申请号：PCT/EP2002/000338
申请日：2002-01-15
申请人： DENTSPLY DETREY GMBH , KLEE, Joachim, E. , WALZ, Uwe , FACHER, Andreas , WEBER, Christoph , MÜLHAUPT, Rolf , FREY, Holger , MÜH, Ekkehard
发明人： KLEE, Joachim, E. , WALZ, Uwe , FACHER, Andreas , WEBER, Christoph , MÜLHAUPT, Rolf , FREY, Holger , MÜH, Ekkehard
IPC分类号： A61K6/093
CPC分类号： A61K6/0008 , A61K6/083 , C08L51/085
摘要： A process for the preparation of a polymerisable dental composition comprising the steps of (a) preparing a liquid mixture comprising (i) 1 to 99% w/w of a hybrid monomer component containing at least one hybrid monomer compound having one hydrolysable siloxane group and at least one polymerisable organic moiety, and (ii) 99 to 1% w/w of a monomer component polymerisable with the polymerisable organic moiety of the hybrid monomer compounds; and (b) adding at least a stoichiometrically sufficient amount of water to the mixture to hydrolyse the hydrolysable siloxane group of the hybrid monomer compound and to form spherical polymerisable nanoparticles having an average particle size of from 1 to 100 nm dispersed in the monomer component, whereby the nanoparticles have a structure with Si-O-Si bonds and peripherally exposed polymerisable organic moieties.
摘要翻译：一种用于制备可聚合牙科用组合物的方法，包括以下步骤：（a）制备液体混合物，其包含（i）1至99％w / w的含有至少一种具有一个可水解硅氧烷基团的杂化单体化合物的杂化单体组分和至少一个可聚合有机部分，和（ii）99-1％w / w的可与所述杂化单体化合物的可聚合有机部分聚合的单体组分; 和（b）向所述混合物中加入至少一种化学计量的足够量的水以水解所述杂化单体化合物的可水解硅氧烷基团并形成分散在单体组分中的平均粒度为1至100nm的球形可聚合纳米颗粒，由此纳米颗粒具有具有Si-O-Si键和周边暴露的可聚合有机部分的结构。

2. 发明申请

WO2005063778A1 ONE-PART SELF-ETCHING, SELF-PRIMING DENTAL ADHESIVE COMPOSITION 审中-公开
标题翻译：一部分自我蚀刻，自制牙膏粘合剂组合物
公开(公告)号：WO2005063778A1
公开(公告)日：2005-07-14
申请号：PCT/EP2004/014307
申请日：2004-12-15
申请人： DENTSPLY DETREY GMBH , KLEE, Joachim, E. , LEHMANN, Uwe , WALZ, Uwe
发明人： KLEE, Joachim, E. , LEHMANN, Uwe , WALZ, Uwe
IPC分类号： C07F9/09
CPC分类号： A61K6/0023 , C07F9/091 , C08L33/00 , C08L43/02
摘要： One-part self-etching, self-priming dental adhesive composition having a pH of at most 2, which comprises (a) a polymerizable acidic phosphoric acid ester monomer (b) one or more polymerisable acidic monomers (c) a polymerizable N-substituted alkylacrylic or acrylic acid amide monomer; (d) optionally an organic and/or inorganic acid; (e) an organic water soluble solvent and/or water; and (f) polymerization initiator, inhibitor and stabilizer.
摘要翻译：一部分自蚀刻自粘牙科粘合剂组合物，其pH值至多为2，其包含（a）可聚合的酸性磷酸酯单体（b）一种或多种可聚合的酸性单体（c）可聚合的N-取代的烷基丙烯酸或丙烯酰胺单体; （d）任选的有机和/或无机酸; （e）有机水溶性溶剂和/或水; 和（f）聚合引发剂，抑制剂和稳定剂。

3. 发明申请

WO2003035013A1 HYDROLYSIS STABLE SELF-ETCHING, SELF-PRIMING ADHESIVE 审中-公开
标题翻译：水解稳定自我蚀刻，自粘胶
公开(公告)号：WO2003035013A1
公开(公告)日：2003-05-01
申请号：PCT/EP2002/011940
申请日：2002-10-25
申请人： DENTSPLY DETREY GMBH , KLEE, Joachim , WALZ, Uwe , LEHMANN, Uwe
发明人： KLEE, Joachim , WALZ, Uwe , LEHMANN, Uwe
IPC分类号： A61K6/00
CPC分类号： A61K6/0023 , C08L33/00
摘要： An aqueous one-pack self-etching and self-priming dental adhesive composition having a pH of at most 2, which comprises: (i) a polymerizable N-substituted alkylacrylic or acrylic acid amide monomer which optionally contains an inorganic acidic moiety selected from a phosphonic acid moiety or a sulfonic acid moiety, and (ii) a curing system.
摘要翻译：一种pH值至多为2的含水单组份自蚀刻和自吸牙科粘合剂组合物，其包含：（i）可聚合的N-取代烷基丙烯酸或丙烯酸酰胺单体，其任选地含有选自以下的无机酸性部分：膦酸部分或磺酸部分，和（ii）固化体系。

4. 发明申请

WO2002085974A1 LIGHT-POLYMERIZABLE DENTAL COMPOSITION CONTAINING AN INHIBITOR 审中-公开
标题翻译：含有抑制剂的光聚合牙本质组合物
公开(公告)号：WO2002085974A1
公开(公告)日：2002-10-31
申请号：PCT/US2002/011978
申请日：2002-04-16
申请人： DENTSPLY INTERNATIONAL INC. , KLEE, Joachim, E. , WALZ, Uwe
发明人： KLEE, Joachim, E. , WALZ, Uwe
IPC分类号： C08K5/01
CPC分类号： B82Y30/00 , A61K6/083 , A61K6/09 , C08L75/16 , C08L33/00
摘要： Light-polymerizable dental composition comprising (i) a polymerizable monomer component, (ii) a light-sensitive polymerization initiator, (iii) an inhibitor, (iv) optionally a filler and/or pigment, and (v) optionally a solvent, characterized in that the inhibitor is a substituted fullerene compound present in an amount suitable for improving light stability of the dental composition.
摘要翻译：光聚合性牙科用组合物，其包含（i）可聚合单体组分，（ii）光敏聚合引发剂，（iii）抑制剂，（iv）任选的填料和/或颜料，和（v）任选的溶剂，因为抑制剂是以适于改善牙齿组合物的光稳定性的量存在的取代的富勒烯化合物。

5. 发明申请

WO2005058182A1 A SINGLE-USE STORAGE AND APPLICATION DEVICE FOR A DENTAL MATERIAL HAVING FLOWABILITY 审中-公开
标题翻译：具有流动性的牙科材料的单一使用存储和应用装置
公开(公告)号：WO2005058182A1
公开(公告)日：2005-06-30
申请号：PCT/EP2004/012673
申请日：2004-11-09
申请人： DENTSPLY DE TREY GMBH , KLEE, Joachim, E. , EVERS, Markus , WALZ, Uwe , GRÜTZNER, Andreas, E.
发明人： KLEE, Joachim, E. , EVERS, Markus , WALZ, Uwe , GRÜTZNER, Andreas, E.
IPC分类号： A61C5/06
CPC分类号： A61C5/60
摘要： A single-use storage and application device for a dental material having flowability, said device comprising: (a) a reservoir container having a compressible container wall, said reservoir container being adapted for (a-1) storing said dental material and (a-2) delivering said dental material during use upon compression of said container wall; and (b) a cannula having a passage extending from the proximal end to the distal end of the cannula, said distal end comprising a bibulous material adapted for (b-1) soaking in said dental material delivered during use from said reservoir container via said passage and (b-2) releasing said dental material after being soaked in said bibulous material for applying said dental material to an application site; whereby said device is adapted for (i) preventing a flow of said dental material from said reservoir container through said passage during storage, (ii) providing a fluid-flow communication from said reservoir container through said passage I during use, and (iii) providing a flow resistance for the dental material such that said dental material is prevented from spurting out of said distal end.
摘要翻译：一种用于具有流动性的牙科材料的一次性存储和应用装置，所述装置包括：（a）具有可压缩容器壁的储存容器，所述储存容器适于（a-1）储存所述牙科材料和（a- 2）在使用时在压缩所述容器壁时递送所述牙科材料; （b）套管，其具有从套管的近端到远端延伸的通道，所述远端包括适于（b-1）浸泡在使用期间从所述储存容器输送的所述牙科材料中的所述吸入材料，通道和（b-2）在将所述牙科材料施用于所述吸水材料浸泡到施用部位之后释放所述牙科材料; 由此所述装置适于（i）在储存期间防止所述牙科材料从所述储存容器流过所述通道，（ii）在使用期间通过所述通道I从所述储存容器提供流体流动连通，以及（iii）为牙科材料提供流动阻力，使得防止所述牙科材料从所述远端喷出。

6. 发明申请

WO2008094580A8 DENTAL COMPOSITIONS COMPRISING BISACRYLAMIDES AND USE THEREOF 审中-公开
公开(公告)号：WO2008094580A8
公开(公告)日：2008-08-07
申请号：PCT/US2008/001201
申请日：2008-01-29
申请人： DENTSPLY INTERNATIONAL INC. , WALZ, Uwe , KLEE, Joachim, E.
发明人： WALZ, Uwe , KLEE, Joachim, E.
IPC分类号： A61K6/083
摘要： The invention concerns a dental composition comprising bisacrylamides that are polymerizable by free-radical polymerization and by Michael-addition polymerization with amines. The application of polymerization and addition polymerization with amines opens the possibility to completely reacted materials that have no oxygen inhibited layers. The claimed bisacrylamides have an improved hydrolytic stability.

7. 发明申请

WO2004078100A2 A POYMERIZABLE PHOSPHORIC ACID ESTER DERIVATIVE AND A DENTAL COMPOSITION EMPLOYING IT. 审中-公开
标题翻译：一种可磷化的磷酸酯衍生物和一种使用它的牙齿组合物。
公开(公告)号：WO2004078100A2
公开(公告)日：2004-09-16
申请号：PCT/EP2004/002289
申请日：2004-03-05
申请人： DENTSPLY DE TREY GMBH , KLEE, Joachim, E. , LEHMANN, Uwe , WALZ, Uwe , LIU, Huaibing
发明人： KLEE, Joachim, E. , LEHMANN, Uwe , WALZ, Uwe , LIU, Huaibing
IPC分类号： A61K
CPC分类号： A61K6/083 , A61K6/0023 , C07F9/091 , C07F9/093 , C08F30/02 , C08L43/02 , C08L33/00
摘要： The present invention provides a polymerizable phosphoric acid ester derivative having the following formula (A): wherein Z is COOR 1 , COSR 1 , CON(R 1 ) 2 , CONR 1 R 2 , or CONHR 1 , R 1 and R 2 independently are a hydrogen atom, a substituted or unsubstituted C 1 to C 18 alkyl group optionally substituted by a C 3 to C 8 cycloalkyl group, a substituted or unsubstituted C 3 to C 8 cycloalkyl group, a substituted or unsubstituted C 4 to C, 18 aryl or heteroaryl group, a substituted or unsubstituted C 5 to C 18 alkylaryl or alkylheteroaryl group, or a substituted or unsubstituted C 7 to C 30 aralkyl group, whereby two R 1 residues may form together with the N-atom to which they are bonded a 5- to 7-membered heterocyclic ring which may contain beside said N-atom a further nitrogen atom or an oxygen atom, and whereby the substituted groups may be substituted by 1 to 5 C 1 to C 5 alkyl group(s); a is an integer of from 1 to 10, preferably 1 to 5; b is an integer of from 1 to 10, preferably 1 to 5; and R represents an organic residue containing a + b carbon atoms selected from primary and secondary aliphatic carbon atoms, secondary alicyclic carbon atoms, and aromatic carbon atoms, each of said carbon atoms linking a phosphate or 2-(oxa-ethyl)acryl derivative group.
摘要翻译：本发明提供具有下式（A）的可聚合磷酸酯衍生物：其中Z为COOR1，COSR1，CON （R 1）2，CONR 1 R 2或CONHR 1，其中R 1，R 2， R 1和R 2独立地为氢原子，取代或未取代的C 1至C 18烷基任选被C 3-8 C 1-8环烷基取代，取代或未取代的C 3-8 C 1-8环烷基基团，取代或未取代的C 4至C 18芳基或杂芳基，取代或未取代的C 5至C 18 烷基芳基或烷基杂芳基，或者取代或未取代的C7-C30芳烷基，其中两个R 1残基可以形成与它们所键合的N原子一起形成5至7元杂环，其可以在所述N原子旁边含有另外的氮原子或氧原子，并且其中所述取代的基团可以被1至5个C 1至C 5的烷基取代;并且其中所述取代的基团可以被1至5个C 1至C 5的烷基取代。 a是1至10的整数，优选1至5; b是1至10的整数，优选1至5; R表示选自伯和仲脂族碳原子，仲脂环碳原子和芳族碳原子的含有α+β碳原子的有机残基，每个所述碳原子连接磷酸酯或2-（氧杂 - 乙基）丙烯酰基衍生物基团。

8. 发明申请

WO2013087223A1 COMPOSITE FILLER PARTICLES AND PROCESS FOR THE PREPARATION THEREOF 审中-公开
标题翻译：复合填料颗粒及其制备方法
公开(公告)号：WO2013087223A1
公开(公告)日：2013-06-20
申请号：PCT/EP2012/005206
申请日：2012-12-17
申请人： DENTSPLY DETREY GMBH
发明人： STELZIG, Simon , KEMPTER, Jörg , NOERPEL, Stephanie , KLEE, Joachim, E. , FACHER, Andreas , WALZ, Uwe , WEBER, Christoph
IPC分类号： A61K6/083 , A61K6/02
CPC分类号： C09D143/04 , A61K6/0008 , A61K6/0076 , A61K6/0085 , A61K6/0091 , A61K6/0215 , A61K6/024 , A61K6/025 , A61K6/083 , B01J2/16 , B05D7/24 , C01P2004/61 , C03C14/008 , C03C17/00 , C03C17/30 , C03C2214/12 , C08K3/40 , C08K5/5419 , C09C1/40 , C09C3/00 , C09C3/006 , C09C3/045 , C09C3/08 , C09C3/12 , C08L33/00
摘要： A process for the preparation of composite filler particles, comprising: (a) coating a particulate filler having a median particle size (D50) of from 1 to 1200 nm with a coating composition containing a film-forming agent forming a coating layer on the surface of the particulate filler, said coating layer displaying reactive groups on the surface of the coating layer, said reactive groups being selected from addition polymerizable groups and step-growth polymerizable groups, thereby forming a coated particulate filler; subsequently or concurrently (b) agglomerating the coated particulate filler, optionally in the presence of a further crosslinking agent and optionally in the presence of a further particulate filler not displaying reactive groups, for providing a granulation of the coated particulate filler wherein the granulation contains the coated particulate filler particles and the optional further particulate filler particles separated from and connected to each other by at least one coating layer, whereby the at least one coating layer may be crosslinked by crosslinking groups obtained by reacting the reactive groups and optionally a further crosslinking agent; (c) optionally milling, classifying and/or sieving the granulation of the coated particulate filler; and (d) optionally further crosslinking the granulation of the coated particulate filler; for providing composite filler particles having a median particle size (D50) of from 1 to 70 μιτι, wherein reactive groups are transformed into crosslinking groups obtained by reacting reactive groups and optionally a further crosslinking agent, and wherein the particulate filler is the main component by volume of the composite filler particles.
摘要翻译：一种制备复合填料颗粒的方法，包括：（a）用包含在表面上形成涂层的成膜剂的涂料组合物涂覆中等颗粒尺寸（D50）为1至1200nm的颗粒填料所述涂层在涂层的表面上显示反应性基团，所述反应性基团选自加成聚合基团和步进生长可聚合基团，从而形成涂布的颗粒填料; 随后或同时（b）任选地在另外的交联剂的存在下和任选地在不显示反应性基团的另外的颗粒填料的存在下任选地使涂覆的颗粒填料附聚，以提供涂覆的颗粒填料的造粒，其中造粒物包含涂覆的颗粒填料颗粒和任选的另外的颗粒填料颗粒通过至少一个涂层彼此分离和连接，由此至少一个涂层可以通过使反应基团和任选的另外的交联剂反应获得的交联基团交联 ; （c）任选地研磨，分级和/或筛分涂覆的颗粒填料的造粒物; 和（d）任选地进一步交联涂覆的颗粒填料的造粒物; 用于提供中值粒径（D50）为1至70μmolataotaotaota的复合填料颗粒，其中反应性基团转化为通过反应性基团和任选另外的交联剂反应获得的交联基团，并且其中颗粒填料是主要组分复合填料颗粒的体积。

9. 发明申请

WO2018002326A1 DENTAL COMPOSITION COMPRISING A DENTAL FILLER CONTAINING A STRUCTURAL FILLER AND SILANATED GLASS FLAKES 审中-公开
标题翻译：包含包含结构填充物和硅酸盐玻璃薄片的牙科填充物的牙科组合物
公开(公告)号：WO2018002326A1
公开(公告)日：2018-01-04
申请号：PCT/EP2017/066323
申请日：2017-06-30
申请人： DENTSPLY DETREY GMBH
发明人： WEBER, Christoph , WALZ, Uwe , NOERPEL, Stephanie
IPC分类号： A61K6/027 , A61K6/083 , A61K6/00 , A61K6/02
CPC分类号： A61K6/0091 , A61K6/0008 , A61K6/005 , A61K6/0052 , A61K6/0205 , A61K6/0235 , A61K6/083 , C03C3/087 , C03C3/093 , C08L33/10
摘要： The present invention relates to a dental composition comprising a dental filler containing a structural filler and silanated glass flakes. Furthermore, the present invention relates to the use of silanated glass flakes for preparing a dental composition.
摘要翻译：本发明涉及包含含有结构填料和硅烷化玻璃片的牙科填料的牙科组合物。此外，本发明涉及硅烷化玻璃片用于制备牙科组合物的用途。

10. 发明申请

WO2016202744A1 AQUEOUS DENTAL GLASS IONOMER COMPOSITION 审中-公开
标题翻译：水性透明玻璃离子组合物（AQUEOUS DENTAL GLASS IONOMER COMPOSITION）
公开(公告)号：WO2016202744A1
公开(公告)日：2016-12-22
申请号：PCT/EP2016/063515
申请日：2016-06-13
申请人： DENTSPLY DETREY GMBH
发明人： RENN, Caroline , ELSNER, Oliver , GANSEL, Julia , SCHEUFLER, Christian , WALZ, Uwe
IPC分类号： A61K6/083
CPC分类号： A61K6/0835
摘要： The present invention relates to an aqueous dental glass ionomer composition comprising (A) a reactive particulate glass, (B) a water-soluble, polymerizable polymer comprising acidic groups, which is reactive with the particulate glass in a cement reaction, whereby the polymerizable polymer has a polymer backbone and hydrolysis-stable pendant groups having one or more polymerizable carbon-carbon double bonds, wherein the polymerizable polymer is obtainable by a process comprising a) a step of copolymerizing a mixture comprising (i) a first copolymerizable monomer comprising at least one optionally protected carboxylic acid group and a first polymerizable organic moiety, and (ii) a second copolymerizable monomer comprising one or more optionally protected primary and/or secondary amino groups and a second polymerizable organic moiety, for obtaining an amino group containing copolymer; b) a step of coupling to the amino group containing copolymer a compound having a polymerizable moiety and a functional group reactive with an amino group of repeating units derived from the second copolymerizable monomer in the amino group containing copolymer obtained in the first step, wherein the optionally protected amino group is deprotected, so that polymerizable pendant groups are linked to the backbone by hydrolysis-stable linking groups, and, optionally, a step of deprotecting the protected carboxylic acid group after step a) or step b), for obtaining a polymerizable polymer; (C) a hydrolysis-stable, water-soluble monomer having one polymerizable double bond and optionally a carboxylic acid group, said monomer having a molecular weight of at most 200 Da; (D) a polymerization initiator system; and (E) a polymerizable hydrolysis-stable crosslinker having at least two polymerizable carbon-carbon double bonds.
摘要翻译：本发明涉及一种水性牙科玻璃离聚物组合物，其包含（A）反应性颗粒玻璃，（B）包含酸性基团的水溶性可聚合聚合物，其在水泥反应中与颗粒状玻璃反应，由此可聚合聚合物具有聚合物主链和具有一个或多个可聚合碳 - 碳双键的水解稳定侧基，其中可聚合聚合物可通过以下方法获得：a）使混合物共聚的步骤，该混合物包含（i）至少包含第一可共聚单体一种任选保护的羧酸基团和第一可聚合有机部分，和（ii）包含一个或多个任选保护的伯和/或仲氨基和第二可聚合有机部分的第二可共聚单体，用于获得含氨基的共聚物; b）在第一步骤中获得的含氨基共聚物中与含氨基的共聚物偶联具有可聚合部分的化合物和与源自第二可共聚单体的重复单元的氨基反应的官能团的步骤，其中，任选地保护的氨基被去保护，使得可聚合侧基通过水解稳定的连接基团连接到主链上，并且任选地在步骤a）或步骤b）之后使被保护的羧酸基脱保护的步骤，以获得可聚合的聚合物; （C）具有一个可聚合双键和任选的羧酸基团的水解稳定的水溶性单体，所述单体的分子量至多为200Da; （D）聚合引发剂体系; 和（E）具有至少两个可聚合碳 - 碳双键的可聚合水解稳定的交联剂。

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