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    • 5. 发明申请
    • Precursor Infiltration and Coating Method
    • 前体渗透和涂层方法
    • US20080193803A1
    • 2008-08-14
    • US11911959
    • 2006-04-21
    • Tal Z. SholklapperCraig P. JacobsonSteven J. ViscoLutgard C. De Jonghe
    • Tal Z. SholklapperCraig P. JacobsonSteven J. ViscoLutgard C. De Jonghe
    • H01M4/00B05D3/02B05D5/12C25B11/04B05D7/22
    • H01M4/8621H01M4/8652H01M4/8885
    • A method of forming a composite (e.g., a mixed electrode) by infiltration of a porous structure (e.g., one formed from an ionically conductive material) with a solution of a precursor (e.g., for an electronically conductive material) results in a particulate layer on and within the porous structure with a single infiltration. The method involves forming a solution comprising at least one metal salt and a surfactant; heating the solution to substantially evaporate solvent and form a concentrated salt and surfactant solution; infiltrating the concentrated solution into a porous structure to create a composite; and heating the composite to substantially decompose the salt and surfactant to oxide and/or metal particles. The result is a particulate layer on the pore walls of the porous structure. In some instances the particulate layer is a continuous network. Corresponding devices have improved properties and performance.
    • 通过用前体(例如,用于电子导电材料)的溶液渗透多孔结构(例如由离子导电材料形成的多孔结构)形成复合材料(例如,混合电极)的方法导致颗粒层 在多孔结构内部和内部具有单次渗透。 该方法包括形成包含至少一种金属盐和表面活性剂的溶液; 加热溶液以使溶剂基本蒸发并形成浓盐和表面活性剂溶液; 将浓缩溶液渗透到多孔结构中以产生复合材料; 并加热复合物以将盐和表面活性剂基本上分解成氧化物和/或金属颗粒。 结果是多孔结构的孔壁上的颗粒层。 在某些情况下,颗粒层是连续的网络。 对应的设备具有改进的性能和性能。