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1. 发明申请

US20120325678A1 STRUCTURES AND FABRICATION TECHNIQUES FOR SOLID STATE ELECTROCHEMICAL DEVICES 审中-公开
标题翻译：固态电化学装置的结构和制造技术
公开(公告)号：US20120325678A1
公开(公告)日：2012-12-27
申请号：US13599362
申请日：2012-08-30
申请人： Steven J. Visco , Craig P. Jacobson , Lutgard C. De Jonghe
发明人： Steven J. Visco , Craig P. Jacobson , Lutgard C. De Jonghe
IPC分类号： C25B1/02 , C25B9/16
CPC分类号： H01M4/8885 , B01D53/326 , B01D2257/108 , C25B9/00 , H01M4/9025 , H01M4/9033 , H01M4/905 , H01M4/9066 , H01M8/004 , H01M8/1213 , H01M8/1226 , H01M8/1231 , H01M8/1246 , H01M8/1253 , H01M8/126 , H01M8/1266 , H01M8/2425 , H01M8/243 , H01M8/2483 , H01M2008/1293 , H01M2300/0074 , Y02E60/525 , Y02P70/56 , Y10T29/49115
摘要： Porous substrates and associated structures for solid-state electrochemical devices, such as solid-oxide fuel cells (SOFCs), are low-cost, mechanically strong and highly electronically conductive. Some preferred structures have a thin layer of an electrocatalytically active material (e.g., Ni-YSZ) coating a porous high-strength alloy support (e.g., SS-430) to form a porous SOFC fuel electrode. Electrode/electrolyte structures can be formed by co-firing or constrained sintering processes.
摘要翻译：用于固态电化学装置（例如固体氧化物燃料电池（SOFC））的多孔基材和相关结构是低成本，机械强度和高电子导电性的。一些优选的结构具有涂覆多孔高强度合金载体（例如SS-430）的电催化活性材料（例如，Ni-YSZ）的薄层，以形成多孔SOFC燃料电极。电极/电解质结构可以通过共烧或约束烧结工艺形成。

2. 发明授权

US07901837B2 Structures for dense, crack free thin films 失效
标题翻译：密集，无裂纹薄膜的结构
公开(公告)号：US07901837B2
公开(公告)日：2011-03-08
申请号：US11567056
申请日：2006-12-05
申请人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
发明人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
IPC分类号： H01M8/10
CPC分类号： C04B38/0038 , B01D53/326 , B01D2257/108 , C04B35/016 , C04B2111/00801 , C04B2111/00853 , C25B9/00 , H01M4/9025 , H01M4/9033 , H01M4/9066 , H01M8/1213 , H01M8/1226 , H01M8/1231 , H01M8/124 , H01M8/1246 , H01M8/1253 , H01M8/126 , H01M8/1266 , H01M8/1286 , H01M8/2425 , H01M8/243 , H01M2008/1293 , H01M2300/0074 , Y02E60/525 , Y02P70/56 , C04B38/0054 , C04B38/0074
摘要： The process described herein provides a simple and cost effective method for making crack free, high density thin ceramic film. The steps involve depositing a layer of a ceramic material on a porous or dense substrate. The deposited layer is compacted and then the resultant laminate is sintered to achieve a higher density than would have been possible without the pre-firing compaction step.
摘要翻译：本文所述的方法提供了制造无裂纹的高密度薄陶瓷膜的简单且成本有效的方法。这些步骤包括在多孔或致密基底上沉积陶瓷材料层。沉积层被压实，然后将所得的层压体烧结以实现比没有预烧结压实步骤可能的密度更高的密度。

3. 发明申请

US20100038012A1 JOINED CONCENTRIC TUBES 有权
标题翻译：连接集中管
公开(公告)号：US20100038012A1
公开(公告)日：2010-02-18
申请号：US12304191
申请日：2006-07-28
申请人： Michael C. Tucker , Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
发明人： Michael C. Tucker , Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
IPC分类号： B29C65/02 , F16L9/14
CPC分类号： B22F5/106 , B22F7/004 , B22F7/062 , H01M8/004 , H01M8/0252 , H01M8/0297 , H01M8/1213 , H01M8/243 , H01M2008/1293 , Y02P70/56
摘要： Tubular objects having two or more concentric layers that have different properties are joined to one another during their manufacture primarily by compressive and friction forces generated by shrinkage during sintering and possibly mechanical interlocking. It is not necessary for the concentric tubes to display adhesive-, chemical- or sinter-bonding to each other in order to achieve a strong bond. This facilitates joining of dissimilar materials, such as ceramics and metals.
摘要翻译：具有不同性质的具有两个或更多个同心层的管状物体在其制造期间彼此接合，主要是通过在烧结期间收缩和可能的机械互锁而产生的压缩和摩擦力。同心圆管不需要彼此粘合，化学或烧结，以达到很好的粘结。这有助于不同材料如陶瓷和金属的接合。

4. 发明申请

US20080193803A1 Precursor Infiltration and Coating Method 审中-公开
标题翻译：前体渗透和涂层方法
公开(公告)号：US20080193803A1
公开(公告)日：2008-08-14
申请号：US11911959
申请日：2006-04-21
申请人： Tal Z. Sholklapper , Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
发明人： Tal Z. Sholklapper , Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
IPC分类号： H01M4/00 , B05D3/02 , B05D5/12 , C25B11/04 , B05D7/22
CPC分类号： H01M4/8621 , H01M4/8652 , H01M4/8885
摘要： A method of forming a composite (e.g., a mixed electrode) by infiltration of a porous structure (e.g., one formed from an ionically conductive material) with a solution of a precursor (e.g., for an electronically conductive material) results in a particulate layer on and within the porous structure with a single infiltration. The method involves forming a solution comprising at least one metal salt and a surfactant; heating the solution to substantially evaporate solvent and form a concentrated salt and surfactant solution; infiltrating the concentrated solution into a porous structure to create a composite; and heating the composite to substantially decompose the salt and surfactant to oxide and/or metal particles. The result is a particulate layer on the pore walls of the porous structure. In some instances the particulate layer is a continuous network. Corresponding devices have improved properties and performance.
摘要翻译：通过用前体（例如，用于电子导电材料）的溶液渗透多孔结构（例如由离子导电材料形成的多孔结构）形成复合材料（例如，混合电极）的方法导致颗粒层在多孔结构内部和内部具有单次渗透。该方法包括形成包含至少一种金属盐和表面活性剂的溶液; 加热溶液以使溶剂基本蒸发并形成浓盐和表面活性剂溶液; 将浓缩溶液渗透到多孔结构中以产生复合材料; 并加热复合物以将盐和表面活性剂基本上分解成氧化物和/或金属颗粒。结果是多孔结构的孔壁上的颗粒层。在某些情况下，颗粒层是连续的网络。对应的设备具有改进的性能和性能。

5. 发明授权

US07468120B2 Fluorine separation and generation device 有权
标题翻译：氟分离和生成装置
公开(公告)号：US07468120B2
公开(公告)日：2008-12-23
申请号：US11121272
申请日：2005-05-02
申请人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe , Constantin I. Stefan
发明人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe , Constantin I. Stefan
IPC分类号： C25B13/04 , C25B9/00 , C25B1/24
CPC分类号： H01M8/124 , B01D53/326 , B01D2257/2027 , Y02P70/56
摘要： A process and apparatus for the electrolytic separation of fluorine from a mixture of gases is disclosed. Also described is the process and apparatus for the generation of fluorine from fluorine/fluoride containing solids, liquids or gases.
摘要翻译：公开了一种从气体混合物中电解氟分离氟的方法和装置。还描述了用于从含氟/氟化物的固体，液体或气体产生氟的方法和装置。

6. 发明申请

US20080268323A1 Sealed Joint Structure for Electrochemical Device 有权
标题翻译：电化学装置密封接头结构
公开(公告)号：US20080268323A1
公开(公告)日：2008-10-30
申请号：US11791270
申请日：2005-11-28
申请人： Michael C. Tucker , Craig P. Jacobson , Lutgard C. De Jonghe , Steven J. Visco
发明人： Michael C. Tucker , Craig P. Jacobson , Lutgard C. De Jonghe , Steven J. Visco
IPC分类号： H01M2/08
CPC分类号： H01M2/08 , B32B2315/02 , C04B35/016 , C04B37/006 , C04B37/026 , C04B2235/3213 , C04B2235/3227 , C04B2237/125 , C04B2237/348 , H01M8/0271 , H01M8/2404 , H01M8/243 , Y02P70/56 , Y10T29/4911
摘要： Several members make up a joint in a high-temperature electrochemical device, wherein the various members perform different functions. The joint is useful for joining multiple cells (generally tubular modules) of an electrochemical device to produce a multi-cell segment-in-series stack for a solid oxide fuel cell, for instance. The joint includes sections that bond the joining members to each other; one or more seal sections that provide gas-tightness, and sections providing electrical connection and/or electrical insulation between the various joining members. A suitable joint configuration for an electrochemical device has a metal joint housing, a first porous electrode, a second porous electrode, separated from the first porous electrode by a solid electrolyte, and an insulating member disposed between the metal joint housing and the electrolyte and second electrode. One or more brazes structurally and electrically connects the first electrode to the metal joint housing and forms a gas tight seal between the first electrode and the second electrode.
摘要翻译：几个构件在高温电化学装置中构成接头，其中各种构件执行不同的功能。该接头可用于连接电化学装置的多个电池（通常为管状模块），以产生例如用于固体氧化物燃料电池的多电池段串联堆叠。接头包括将接合构件彼此接合的部分; 提供气密性的一个或多个密封部分，以及在各种连接部件之间提供电连接和/或电绝缘的部分。用于电化学装置的合适的接头构造具有金属接头壳体，第一多孔电极，第二多孔电极，通过固体电解质与第一多孔电极分离，以及设置在金属接头壳体和电解质之间的绝缘构件，第二多孔电极电极。一个或多个钎焊结构地和电连接第一电极和金属接头壳体，并在第一电极和第二电极之间形成气密密封。

7. 发明授权

US07829213B2 Planar electrochemical device assembly 失效
标题翻译：平面电化学装置组装
公开(公告)号：US07829213B2
公开(公告)日：2010-11-09
申请号：US11796659
申请日：2007-04-27
申请人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
发明人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
IPC分类号： H01M4/00 , H01M8/00 , H01M8/10 , H01M2/02
CPC分类号： H01M8/2425 , H01M8/0202 , H01M8/0297 , H01M8/1226 , H01M8/2483 , Y02P70/56 , Y10T29/4911 , Y10T29/49114
摘要： A pre-fabricated electrochemical device having a dense electrolyte disposed between an anode and a cathode preferably deposited as thin films is bonded to a porous electrically conductive support. A second porous electrically conductive support may be bonded to a counter electrode of the electrochemical device. Multiple electrochemical devices may be bonded in parallel to a single porous support, such as a perforated sheet to provide a planar array. Planar arrays may be arranged in a stacked interconnected array. A method of making a supported electrochemical device is disclosed wherein the method includes a step of bonding a pre-fabricated electrochemical device layer to an existing porous metal or porous metal alloy layer.
摘要翻译：设置在优选沉积为薄膜的阳极和阴极之间的具有致密电解质的预制电化学装置被接合到多孔导电支撑体上。第二多孔导电支撑件可以结合到电化学装置的对电极。多个电化学装置可以与单个多孔载体（例如穿孔板）平行地结合以提供平面阵列。平面阵列可以布置在堆叠的互连阵列中。公开了一种制造负载电化学装置的方法，其中该方法包括将预制的电化学装置层接合到现有的多孔金属或多孔金属合金层的步骤。

8. 发明授权

US07740966B2 Electrochemical cell stack assembly 有权
标题翻译：电化学电池堆组件
公开(公告)号：US07740966B2
公开(公告)日：2010-06-22
申请号：US11512521
申请日：2006-08-30
申请人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
发明人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
IPC分类号： H01M8/10
CPC分类号： H01M8/0232 , H01M4/8621 , H01M4/8885 , H01M8/0206 , H01M8/0247 , H01M8/025 , H01M8/0271 , H01M8/0273 , H01M8/04097 , H01M8/1007 , H01M8/2415 , H01M8/243 , H01M8/2484 , H01M2008/1293 , Y02P70/56
摘要： Multiple stacks of tubular electrochemical cells having a dense electrolyte disposed between an anode and a cathode preferably deposited as thin films arranged in parallel on stamped conductive interconnect sheets or ferrules. The stack allows one or more electrochemical cell to malfunction without disabling the entire stack. Stack efficiency is enhanced through simplified gas manifolding, gas recycling, reduced operating temperature and improved heat distribution.
摘要翻译：多层堆叠的管状电化学电池具有设置在阳极和阴极之间的致密电解质，优选沉积为平行布置在冲压的导电互连片或套圈上的薄膜。该堆叠允许一个或多个电化学电池故障而不使整个堆叠失效。通过简化的气体歧管，气体回收，降低的操作温度和改善的热分布来提高堆积效率。

9. 发明授权

US07232626B2 Planar electrochemical device assembly 有权
标题翻译：平面电化学装置组装
公开(公告)号：US07232626B2
公开(公告)日：2007-06-19
申请号：US10423472
申请日：2003-04-24
申请人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
发明人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
IPC分类号： H01M4/00 , H01M8/00 , H01M8/10 , H01M2/02
CPC分类号： H01M8/2425 , H01M8/0202 , H01M8/0297 , H01M8/1226 , H01M8/2483 , Y02P70/56 , Y10T29/4911 , Y10T29/49114
摘要： A pre-fabricated electrochemical device having a dense electrolyte disposed between an anode and a cathode preferably deposited as thin films is bonded to a porous electrically conductive support. A second porous electrically conductive support may be bonded to a counter electrode of the electrochemical device. Multiple electrochemical devices may be bonded in parallel to a single porous support, such as a perforated sheet to provide a planar array. Planar arrays may be arranged in a stacked interconnected array. A method of making a supported electrochemical device is disclosed wherein the method includes a step of bonding a pre-fabricated electrochemical device layer to an existing porous metal or porous metal alloy layer.
摘要翻译：设置在优选沉积为薄膜的阳极和阴极之间的具有致密电解质的预制电化学装置被接合到多孔导电支撑体上。第二多孔导电支撑件可以结合到电化学装置的对电极。多个电化学装置可以与单个多孔载体（例如穿孔板）平行地结合以提供平面阵列。平面阵列可以布置在堆叠的互连阵列中。公开了一种制造负载电化学装置的方法，其中该方法包括将预制的电化学装置层接合到现有的多孔金属或多孔金属合金层的步骤。

10. 发明授权

US07163713B2 Method for making dense crack free thin films 失效
标题翻译：制造密集无裂纹薄膜的方法
公开(公告)号：US07163713B2
公开(公告)日：2007-01-16
申请号：US10162511
申请日：2002-06-03
申请人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
发明人： Craig P. Jacobson , Steven J. Visco , Lutgard C. De Jonghe
IPC分类号： B05D5/12
CPC分类号： C04B38/0038 , B01D53/326 , B01D2257/108 , C04B35/016 , C04B2111/00801 , C04B2111/00853 , C25B9/00 , H01M4/9025 , H01M4/9033 , H01M4/9066 , H01M8/1213 , H01M8/1226 , H01M8/1231 , H01M8/124 , H01M8/1246 , H01M8/1253 , H01M8/126 , H01M8/1266 , H01M8/1286 , H01M8/2425 , H01M8/243 , H01M2008/1293 , H01M2300/0074 , Y02E60/525 , Y02P70/56 , C04B38/0054 , C04B38/0074
摘要： The process described herein provides a simple and cost effective method for making crack free, high density thin ceramic film. The steps involve depositing a layer of a ceramic material on a porous or dense substrate. The deposited layer is compacted and then the resultant laminate is sintered to achieve a higher density than would have been possible without the pre-firing compaction step.
摘要翻译：本文所述的方法提供了制造无裂纹的高密度薄陶瓷膜的简单且成本有效的方法。这些步骤包括在多孔或致密基底上沉积陶瓷材料层。沉积层被压实，然后将所得的层压体烧结以实现比没有预烧结压实步骤可能的密度更高的密度。

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