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1. 发明授权

US09738751B2 Method for preparing a polymer from at least one cyclic monomer 有权
公开(公告)号：US09738751B2
公开(公告)日：2017-08-22
申请号：US14421069
申请日：2010-12-07
申请人： Christophe Navarro , Damien Delcroix , Blanca Martin-Vaca , Didier Bourissou
发明人： Christophe Navarro , Damien Delcroix , Blanca Martin-Vaca , Didier Bourissou
IPC分类号： C08G63/02 , C08G63/08 , C08G63/82 , C08G63/91 , C08G64/38 , C08G65/10 , C08G69/20
CPC分类号： C08G63/08 , C08G63/823 , C08G63/912 , C08G63/916 , C08G64/38 , C08G65/10 , C08G69/20
摘要： The present invention relates to a method for preparing a copolymer from at least one cyclic monomer selected from: a lactone, a lactam, a carbonate, a lactide and a glycolide, an oxazoline, an epoxide, a cyclosiloxane, comprising the step consisting of reacting said cyclic monomer in the presence of a substituted phosphorus-containing compound.It also relates to the polymer composition obtained according to this method, as well as the uses thereof, notably as antistatic additives, biocompatible materials, as membranes for treatment of effluents or in electrochemical systems for energy storage.

2. 发明申请

US20120108786A1 ORGANIC SYSTEM FOR THE RING-OPENING POLYMERIZATION OF CYCLIC CARBONATES IN ORDER TO OBTAIN (BIO)-POLYCARBONATES 审中-公开
标题翻译：循环碳酸酯环化聚合的有机体系（BIO） - 聚碳酸酯
公开(公告)号：US20120108786A1
公开(公告)日：2012-05-03
申请号：US13260998
申请日：2010-03-31
申请人： Christophe Navarro , Didier Bourissou , Blanca Martin-Vaca , Damien Delcroix
发明人： Christophe Navarro , Didier Bourissou , Blanca Martin-Vaca , Damien Delcroix
IPC分类号： C08G64/02 , C08G64/30 , B01J31/02
CPC分类号： C08G64/30 , C08G64/0208
摘要： An organocatalytic system, having a sulfonic acid as catalyst, for the polymerization of carbonates, and a polymerization process employing said system to obtain bio-polycarbonates devoid of ether units inserted by decarboxylation. The catalyst system for the ring-opening polymerization reaction of cyclic carbonates is formed of an initiator and, as catalyst, of a sulfonic acid of formula R′—SO3H, where R′ denotes either: a linear alkyl group including from 1 to 20 carbon atoms or a branched or cyclic alkyl group including from 3 to 20 carbon atoms, or a an aryl group.
摘要翻译：具有磺酸作为催化剂的有机催化体系用于碳酸酯的聚合，以及使用所述体系获得没有通过脱羧插入的醚单元的生物聚碳酸酯的聚合方法。环状碳酸酯的开环聚合反应的催化剂体系由引发剂和作为催化剂的式R'-SO3H的磺酸形成，其中R'表示：包括1至20个碳的直链烷基原子或包含3至20个碳原子的支链或环状烷基或芳基。

3. 发明申请

US20150218306A1 METHOD FOR PREPARING A POLYMER FROM AT LEAST ONE CYCLIC MONOMER 有权
标题翻译：从一个循环单体制备聚合物的方法
公开(公告)号：US20150218306A1
公开(公告)日：2015-08-06
申请号：US14421069
申请日：2010-12-07
申请人： Christophe Navarro , Damien Delcroix , Blanca Martin-Vaca , Didier Bourissou
发明人： Christophe Navarro , Damien Delcroix , Blanca Martin-Vaca , Didier Bourissou
IPC分类号： C08G63/08
CPC分类号： C08G63/08 , C08G63/823 , C08G63/912 , C08G63/916 , C08G64/38 , C08G65/10 , C08G69/20
摘要： The present invention relates to a method for preparing a copolymer from at least one cyclic monomer selected from: a lactone, a lactam, a carbonate, a lactide and a glycolide, an oxazoline, an epoxide, a cyclosiloxane, comprising the step consisting of reacting said cyclic monomer in the presence of a substituted phosphorus-containing compound.It also relates to the polymer composition obtained according to this method, as well as the uses thereof, notably as antistatic additives, biocompatible materials, as membranes for treatment of effluents or in electrochemical systems for energy storage.
摘要翻译：本发明涉及从至少一种选自以下的环状单体制备共聚物的方法：内酯，内酰胺，碳酸酯，丙交酯和乙交酯，恶唑啉，环氧化物，环硅氧烷，其包含以下步骤：所述环状单体在取代的含磷化合物存在下进行。它还涉及根据该方法获得的聚合物组合物，以及其用途，特别是抗静电添加剂，生物相容性材料，作为用于处理流出物的膜或用于储能的电化学体系中的用途。

4. 发明申请

US20100121021A1 PROCESS FOR THE PREPARATION OF POLYLACTONES AND POLYLACTAMS 有权
标题翻译：制备聚合物和聚合物的方法
公开(公告)号：US20100121021A1
公开(公告)日：2010-05-13
申请号：US12527113
申请日：2008-02-15
申请人： Stéphanie Magnet , Christophe Navarro , Stéphanie Gazeau-Bureau , Blanca Martin-Vaca , Didier Bourissou
发明人： Stéphanie Magnet , Christophe Navarro , Stéphanie Gazeau-Bureau , Blanca Martin-Vaca , Didier Bourissou
IPC分类号： C08G73/06 , C08G63/78
CPC分类号： C08G63/823 , C08G63/08 , C08G63/81 , C08G69/14 , C08G69/16 , C08G69/24 , C08J5/2256 , C08J2367/04 , C08L67/04 , C08L77/02 , C08L101/00 , C08L2201/04 , D01F6/60 , D01F6/625 , C08L2666/14
摘要： The present invention relates to a process for the preparation of a lactone or lactam homopolymer, comprising the stage consisting in reacting a lactone or lactam with a nonpolymeric initiator comprising at least one hydroxyl or thiol functional group in a nonchlorinated solvent in the presence of a sulfonic acid of formula R—SO3H.It also relates to the polymer composition thus obtained and to its uses, in particular as antistatic additive.
摘要翻译：本发明涉及一种制备内酯或内酰胺均聚物的方法，该方法包括在内酯或内酰胺与非氯化溶剂中在磺酸存在下使含有至少一个羟基或硫醇官能团的非聚合引发剂反应的步骤式R-SO 3 H的酸。它还涉及由此获得的聚合物组合物及其用途，特别是抗静电添加剂。

5. 发明申请

US20100121024A1 METHOD FOR PRODUCING A COPOLYMER OF AT LEAST ONE CYCLIC MONOMER 审中-公开
标题翻译：用于生产至少一个循环单体的共聚物的方法
公开(公告)号：US20100121024A1
公开(公告)日：2010-05-13
申请号：US12527105
申请日：2008-02-15
申请人： Stèphanie Magnet , Christophe Navarro , Stèphanie Gazeau-Bureau , Blanca Martin-Vaca , Didier Bourissou
发明人： Stèphanie Magnet , Christophe Navarro , Stèphanie Gazeau-Bureau , Blanca Martin-Vaca , Didier Bourissou
IPC分类号： C08G63/08
CPC分类号： C08G63/823 , C08G63/08 , C08G63/664 , C08G69/04 , C08G69/16 , C08G2261/126 , C09K3/16 , D01F6/78
摘要： The present invention relates to a process for the preparation of a copolymer of at least one cyclic monomer chosen from a lactone, a lactam, a lactide and a glycolide, comprising the stage consisting in reacting said cyclic monomer with a polymeric initiator in the presence of a compound carrying a sulfonic acid functional group.It also relates to the polymer composition obtained according to this process and to its uses, in particular as antistatic additive.
摘要翻译：本发明涉及一种制备至少一种选自内酯，内酰胺，丙交酯和乙交酯的环状单体的共聚物的方法，该方法包括使所述环状单体与聚合物引发剂在存在下反应的阶段携带磺酸官能团的化合物。它还涉及根据该方法获得的聚合物组合物及其用途，特别是作为抗静电添加剂。

6. 发明授权

US08883957B2 Process for the preparation of polylactones and polylactams 有权
标题翻译：制备聚内酯和聚内酰胺的方法
公开(公告)号：US08883957B2
公开(公告)日：2014-11-11
申请号：US12527113
申请日：2008-02-15
申请人： Stéphanie Magnet , Christophe Navarro , Stéphanie Gazeau-Bureau , Bianca Martin-Vaca , Didier Bourissou
发明人： Stéphanie Magnet , Christophe Navarro , Stéphanie Gazeau-Bureau , Bianca Martin-Vaca , Didier Bourissou
IPC分类号： C08G63/08 , D01F6/62 , C08G63/82 , C08L101/00 , C08G69/24 , D01F6/60 , C08J5/22 , C08G69/14 , C08G69/16 , C08G63/81 , C08L67/04 , C08L77/02
CPC分类号： C08G63/823 , C08G63/08 , C08G63/81 , C08G69/14 , C08G69/16 , C08G69/24 , C08J5/2256 , C08J2367/04 , C08L67/04 , C08L77/02 , C08L101/00 , C08L2201/04 , D01F6/60 , D01F6/625 , C08L2666/14
摘要： The present invention relates to a process for the preparation of a lactone or lactam homopolymer, comprising the stage consisting in reacting a lactone or lactam with a nonpolymeric initiator comprising at least one hydroxyl or thiol functional group in a nonchlorinated solvent in the presence of a sulfonic acid of formula R—SO3H.It also relates to the polymer composition thus obtained and to its uses, in particular as antistatic additive.
摘要翻译：本发明涉及一种制备内酯或内酰胺均聚物的方法，该方法包括在内酯或内酰胺与非氯化溶剂中在磺酸存在下使含有至少一个羟基或硫醇官能团的非聚合引发剂反应的步骤式R-SO 3 H的酸。它还涉及由此获得的聚合物组合物及其用途，特别是抗静电添加剂。

7. 发明申请

US20120157601A1 PROCESS FOR CORE-SHELL IMPACT MODIFIERS AND IMPACT MODIFIED THERMOPLASTIC COMPOSITION WITH ENHANCED HYDROLYTIC RESISTANCE 有权
标题翻译：核壳体冲击改性剂的改性和改性的热塑性组合物具有增强的耐水解性
公开(公告)号：US20120157601A1
公开(公告)日：2012-06-21
申请号：US13325762
申请日：2011-12-14
申请人： Christophe Navarro , Stephane Girois , Elisabeth Bay , Jean-Claude Saint-Martin
发明人： Christophe Navarro , Stephane Girois , Elisabeth Bay , Jean-Claude Saint-Martin
IPC分类号： C08F2/22 , C08L9/00 , C08L33/12
CPC分类号： C08F285/00 , C08F2/22 , C08F6/006 , C08F6/22 , C08F279/06 , C08L51/003 , C08L67/02 , C08L69/00 , C08F212/36 , C08F212/08 , C08F220/12
摘要： The present invention relates to a process for producing impact modifiers, impact modified thermoplastic molding compositions and in particular impact modified polycarbonate or polycarbonate/polyester blends having improved resistance to degradation. More particularly the present invention relates to a process for producing polymeric impact modifiers with a core-shell structure made by a multistage process comprising a control and adjustment if necessary of the pH value before and during the recovery step.
摘要翻译：本发明涉及一种生产抗冲改性剂，抗冲改性热塑性成型组合物的方法，特别涉及具有改进的降解抗性的抗冲改性聚碳酸酯或聚碳酸酯/聚酯共混物。更具体地说，本发明涉及一种制备具有由多级方法制成的核 - 壳结构的聚合物抗冲改性剂的方法，包括在恢复步骤之前和期间必要时控制和调节pH值。

8. 发明授权

US08183322B2 Composition containing a lactic acid homopolymer and a block copolymer 有权
标题翻译：含有乳酸均聚物和嵌段共聚物的组合物
公开(公告)号：US08183322B2
公开(公告)日：2012-05-22
申请号：US12678799
申请日：2008-08-26
申请人： Pierre Gerard , Christophe Navarro
发明人： Pierre Gerard , Christophe Navarro
IPC分类号： C08L53/00 , C08L67/00 , C08L69/00
CPC分类号： C08F293/005 , C08L53/00 , C08L2666/04 , C08L2666/14 , C08L2666/02
摘要： The present invention relates to a composition containing at least one lactic acid homopolymer and at least one block copolymer with a polydispersity index ranging from 1.5 to 5 and comprising: at least one block A that is miscible with the homopolymer and formed from monomers containing at least one methacrylate of formula CH2═C(CH3)—COOR1, and at least one block B that is immiscible with the homopolymer and formed from monomers containing at least one alkyl acrylate of formula CH2═CH—COOR2 and/or at least one methacrylate of formula CH2═C(CH3)—COOR3. The invention also relates to the use of this composition for the manufacture of medical articles, textile fibers, thermoformed plates or packaging, in particular films or bottles.
摘要翻译：本发明涉及含有至少一种乳酸均聚物和至少一种多分散指数为1.5至5的嵌段共聚物的组合物，其包含：至少一种与均聚物可混溶并由至少含有至少一种式CH 2 = C（CH 3）-COOR 1的甲基丙烯酸酯和至少一种与均聚物不混溶并由含有至少一种式CH 2 = CH-COOR 2的丙烯酸烷基酯和/或至少一种甲基丙烯酸甲酯的单体形成的嵌段B 式CH 2 = C（CH 3）-COOR 3。本发明还涉及该组合物用于制造医疗制品，纺织纤维，热成型板或包装，特别是薄膜或瓶子的用途。

9. 发明申请

US20090306246A1 CROSSLINKED COMPOSITION COMPRISING A CORE/SHELL COPOLYMER, METHOD OF OBTAINING SAME AND USES THEREOF 审中-公开
标题翻译：包含核心/壳共聚物的交联组合物，其获得方法及其用途
公开(公告)号：US20090306246A1
公开(公告)日：2009-12-10
申请号：US12096237
申请日：2006-12-01
申请人： Laurent Gervat , Gilles Meunier , Christophe Navarro , Elisabeth Bay , Laure Mauboules
发明人： Laurent Gervat , Gilles Meunier , Christophe Navarro , Elisabeth Bay , Laure Mauboules
IPC分类号： C08L33/12
CPC分类号： C08L23/16 , A43B13/04 , B60C1/00 , B60C1/0008 , B60C1/0016 , B60C1/0025 , B60C2009/0021 , C08F255/02 , C08F265/04 , C08F279/02 , C08K3/06 , C08K3/22 , C08K3/36 , C08K5/0025 , C08K5/09 , C08K5/54 , C08L21/00 , C08L23/02 , C08L23/0815 , C08L23/22 , C08L51/00 , C08L51/04 , C08L51/06 , C08L61/06 , C08L2314/06 , C08L2666/24 , C08L2666/04 , C08L2666/02 , C08L2666/06
摘要： The invention relates to is a crosslinked composition containing in parts by weight: 20 to 100 parts of at least one elastomer (I), 2 to 50 parts of at least one core/shell copolymer (II), and 0 to 100 parts of at least one thermoplastic polymer (III). The invention also relates to a method of producing one such crosslinked composition, which is characterized in that it consists in: mixing an elastomer and a core/shell copolymer optionally in the presence of: a grafted polyolefin, a plasticizer, fillers and/or additives, and a suitably-selected crosslinking system, and subsequently crosslinking said mixture at a suitable temperature. In a preferred embodiment of the invention, the mixture is crosslinked at a temperature of between 150 and 320° C. The invention method be carried out in an internal mixer, or, alternately, in a twin-screw extruder or a Buss®-type co-kneader. Depending on the case, the resulting mass is calendared or extruded, cooled and subsequently granulated. The granules thus obtained are then ready to be transformed, by means of heating, into sheets, plates, extrusions, tubes or other desired products. The invention further relates to the use of one such composition in the production of ducts, pipes, tubing, couplers or similar for conveying fluids, such as the fluid transfer conduits, pipes and other elements which are used in the automobile industry in braking, cooling, steering and air-conditioning systems. The inventive crosslinked composition can also be used in the production of belts, tires, electrical cable sheaths, and shoe soles.”
摘要翻译：本发明涉及一种交联组合物，其含有重量份：20-100份至少一种弹性体（I），2-50份至少一种核/壳共聚物（II）和0-100份至少一种热塑性聚合物（III）。本发明还涉及生产一种这样的交联组合物的方法，其特征在于它包括：将弹性体和核/壳共聚物任选地在以下存在下混合：接枝聚烯烃，增塑剂，填料和/或添加剂和适当选择的交联体系，随后在合适的温度下交联所述混合物。在本发明的一个优选实施方案中，该混合物在150-320℃的温度下交联。本发明方法在内部混合器中进行，或者在双螺杆挤出机或Buss（R）型共捏合机。根据情况，将所得物料压延或挤出，冷却并随后造粒。然后将如此获得的颗粒通过加热转化成片，板，挤出物，管或其它所需产物。本发明还涉及一种这样的组合物在制造用于输送流体的管道，管道，管道，耦合器或类似物中的用途，例如用于汽车工业中的流体输送导管，管道和其它元件，用于制动，冷却，转向和空调系统。本发明的交联组合物也可用于生产带，轮胎，电缆护套和鞋底。“

10. 发明申请

US20050237854A1 Method for continuously and dynamically mixing at least two fluids, and micromixer 失效
标题翻译：用于连续和动态地混合至少两种流体的方法和微混合器
公开(公告)号：US20050237854A1
公开(公告)日：2005-10-27
申请号：US10517190
申请日：2003-05-23
申请人： Christophe Navarro , Peter Walzel
发明人： Christophe Navarro , Peter Walzel
IPC分类号： B01F3/10 , B01F7/00 , B01F7/16 , B01F7/18 , B01F13/00 , B01J14/00 , C08F2/01 , C08F20/00 , C08F120/06 , B01F7/12
CPC分类号： B01F7/008 , B01F3/10 , B01F7/00808 , B01F7/00816 , B01F7/183 , B01F13/0059 , B01F2215/045 , B01F2215/0468 , B01F2215/0472 , B01F2215/0481 , B01F2215/0495 , Y10S366/01 , Y10S366/02 , Y10S366/03 , Y10S366/04
摘要： The invention relates to a method for continuously and dynamically mixing at least two fluids. Said method comprises the following steps: a) the rotor (1) of a micromixer is rotatably driven, said micromixer comprising a rotor (1) which is provided with a shaft (2) encompassing blades (3) that are arranged in groups (3a-3g), a stator (4) which is provided with at least one inlet (5) for a first fluid, at least one inlet (6) for a second fluid, and an outlet (7); b) the fluids are fed into the micromixer; and c) a micromixture of the fluids is collected at the outlet (7) of the micromixer. The inventive method is particularly suitable for rapid and/or complex kinetic chemical reactions such as anionic polymerization. The invention also relates to a micromixer for carrying out said method.
摘要翻译：本发明涉及一种用于连续和动态地混合至少两种流体的方法。所述方法包括以下步骤：a）微型混合器的转子（1）被可旋转地驱动，所述微型混合器包括转子（1），转子（1）设置有围绕叶片（3）的轴（2）设有至少一个用于第一流体的入口（5）的定子（4），用于第二流体的至少一个入口（6）和出口（7）; b）将流体进料到微混合器中; 和c）在微混合器的出口（7）收集流体的微混合物。本发明的方法特别适用于快速和/或复杂的动力学化学反应，如阴离子聚合。本发明还涉及一种用于执行所述方法的微混合器。

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