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1. 发明授权

US6136894A Aqueous epoxy resin system with curing agent from reacting acid-terminated polyalkylene glycol with epoxy-amine adduct 有权
标题翻译：具有固化剂的水性环氧树脂体系，由酸封端的聚亚烷基二醇与环氧胺加合物反应
公开(公告)号：US6136894A
公开(公告)日：2000-10-24
申请号：US443871
申请日：1999-11-19
申请人： Charles J. Stark, deceased , Gayle Edward Back , Jimmy D. Elmore , Kalyan Ghosh , Pen-Chung Wang , Kailash Dangayach
发明人： Charles J. Stark, deceased , Gayle Edward Back , Jimmy D. Elmore , Kalyan Ghosh , Pen-Chung Wang , Kailash Dangayach
IPC分类号： C08G59/44 , C08G59/18 , C08G59/50 , C08G59/62 , C08L63/00 , C09D163/00 , C08G59/14 , C08K3/20 , C08L63/02
CPC分类号： C08L63/00 , C08G59/184 , C09D163/00
摘要： An aqueous epoxy resin system suitable for coatings comprises (a) water, (b) at least one epoxy resin and (c) a curing agent prepared by (i) reacting at least one polyamine having at least 3 active amine hydrogen atoms per molecule and at least one epoxy resin in an epoxy equivalent to to polyamine mole ratio of from 0.9:1 to 1:10 to obtain an amine-terminated intermediate; (ii) reacting the amine-terminated intermediate with from 0.5 to 25 weight percent, based on the amine-terminated intermediate, of an acid-terminated polyalkylene glycol to yield an amine-terminated curing agent. The amine-terminated intermediate can be capped with a monoepoxide in an amine hydrogen to epoxy groups ratio of from about 1.5:1 to 30:1 prior to reaction with the acid-terminated polyalkylene glycol, or the amine-terminated curing agent following step (ii) can be capped with a monoepoxide in an amine hydrogen atoms to epoxy groups ratio of from about 2:1 to 30:1.
摘要翻译：适用于涂料的水性环氧树脂体系包括（a）水，（b）至少一种环氧树脂和（c）通过以下步骤制备的固化剂：（i）使至少一种每分子具有至少3个活性胺氢原子的多胺和至少一种环氧树脂的环氧当量相对于多胺摩尔比为0.9:1至1:10，以获得胺封端的中间体; （ii）使胺封端的中间体与基于胺封端的中间体0.5至25重量％的酸封端的聚亚烷基二醇反应，得到胺封端的固化剂。在与氢封端的聚亚烷基二醇反应之前，胺封端的中间体可以用胺氢气中的单环氧化物封端至约1.5:1至30:1的环氧基团比例，或者在步骤后的胺封端的固化剂（ ii）可以用胺氢原子中的单环氧化物封端至约2:1至30:1的环氧基团比例。

2. 发明授权

US6127459A Epoxy resin curing agent-reacting acid-terminated polyalkylene glycol with excess amine-terminated polyamine-epoxy resin adduct 失效
标题翻译：环氧树脂固化剂 - 使酸封端的聚亚烷基二醇与过量的胺封端的聚胺 - 环氧树脂加合物反应
公开(公告)号：US6127459A
公开(公告)日：2000-10-03
申请号：US95090
申请日：1998-06-10
申请人： Charles J. Stark, deceased , Gayle Edward Back , Jimmy D. Elmore , Kalyan Ghosh , Pen-Chung Wang , Kailash Dangayach
发明人： Charles J. Stark, deceased , Gayle Edward Back , Jimmy D. Elmore , Kalyan Ghosh , Pen-Chung Wang , Kailash Dangayach
IPC分类号： C08G59/44 , C08G59/18 , C08G59/50 , C08G59/62 , C08L63/00 , C09D163/00 , C08G59/14 , C08K3/20 , C08L63/02
CPC分类号： C08L63/00 , C08G59/184 , C09D163/00
摘要： A water-compatible curing agent for epoxy resins is prepared by (a) reacting at least one polyamine having at least 3 active amine hydrogen atoms per molecule and at least one epoxy resin in an epoxy equivalent to polyamine mole ratio of from 0.9:1 to 1:10 to obtain an amine-terminated intermediate; (b) reacting the amine-terminated intermediate with from 0.5 to 25 weight percent, based on the amine-terminated intermediate, of an acid-terminated polyalkylene glycol to yield an amine-terminated curing agent. The amine-terminated intermediate can be capped with a monoepoxide in an amine hydrogen atoms to epoxy groups ratio of from about 1.5:1 to 30:1 prior to reaction with the acid-terminated polyalkylene glycol, or the amine-terminated curing agent produced following step (b) can be capped with a monoepoxide.
摘要翻译：环氧树脂的水溶性固化剂通过以下方法制备：（a）使每分子具有至少3个活性胺氢原子的至少一种多胺与至少一种环氧树脂相当于聚胺摩尔比为0.9:1至相当于 1:10得到胺封端的中间体; （b）使胺封端的中间体与基于胺封端的中间体0.5至25重量％的酸封端的聚亚烷基二醇反应，得到胺封端的固化剂。在与酸封端的聚亚烷基二醇反应之前，胺封端的中间体可以用胺氢原子中的单环氧化物封端至约1.5:1至30:1的环氧基团比例，或者以下制备的胺封端的固化剂步骤（b）可以用单环氧化物封端。

3. 发明授权

US06359037B1 Polyamine/epoxy-functional amidoamine product with epoxy resin 有权
标题翻译：聚胺/环氧官能的酰胺胺产品与环氧树脂
公开(公告)号：US06359037B1
公开(公告)日：2002-03-19
申请号：US09635909
申请日：2000-08-10
申请人： Charles J. Stark , Gayle Edward Back , Jimmy D. Elmore , Kalyan Ghosh , Pen-Chung Wang , Kailash Dangayach
发明人： Charles J. Stark , Gayle Edward Back , Jimmy D. Elmore , Kalyan Ghosh , Pen-Chung Wang , Kailash Dangayach
IPC分类号： C08G5914
CPC分类号： C08G59/184
摘要： An aqueous system comprises at least one epoxy resin and a reaction product with an amine equivalent weight of at least 50 prepared by the reaction of an (A) epoxy-functional amidoamine derived from at least one epoxy resin and an amidoamine obtained via the reaction of an acid-terminated polyalkylene glycol and a diamine in an active hydrogen:epoxy groups ratio of from 1:15 to 1:350, with (B) at least one polyamine in an active amine hydrogen:epoxy groups equivalent ratio of from 2:1 to 30:1, and, optionally (C) a monoepoxide in a remaining active amine hydrogen:epoxy groups equivalent ratio of from 5:1 to 20:1.
摘要翻译：水性体系包含至少一种环氧树脂和胺当量重量至少为50的反应产物，该反应产物是由衍生自至少一种环氧树脂的（A）环氧官能酰胺基胺和通过活性氢：环氧基团比例为1:15至1:350的酸封端的聚亚烷基二醇和二胺，（B）活性胺氢中的至少一种多胺：环氧基当量比为2：1 至30：1，和任选地（C）单环氧化物中剩余的活性胺氢：环氧基当量比为5：1至20：1。

4. 发明授权

US06277928B1 Epoxy-functional amidoamine reacted with excess polyamine and monoepoxy as epoxy curative 失效
标题翻译：环氧官能的酰氨基胺与过量的多胺和单环氧基作为环氧固化剂反应
公开(公告)号：US06277928B1
公开(公告)日：2001-08-21
申请号：US09095079
申请日：1998-06-10
申请人： Charles J. Stark , by Ann E. Stark, adminstrator , Gayle Edward Back , Jimmy D. Elmore , Kalyan Ghosh , Pen-Chung Wang , Kailash Dangayach
发明人： Charles J. Stark , by Ann E. Stark, adminstrator , Gayle Edward Back , Jimmy D. Elmore , Kalyan Ghosh , Pen-Chung Wang , Kailash Dangayach
IPC分类号： C08G5914
CPC分类号： C08G59/184
摘要： A water-dispersible curing agent for epoxy resins is prepared by the reaction of (a) an epoxy-functional compound obtained from the reaction of at least one epoxy resin and an amidoamine derived from the reaction of an acid-terminated polyalkylene glycol and a diamine in an active amine hydrogen:epoxy groups ratio of from 1:15 to 1:350, (b) at least one polyamine in an active amine hydrogen:epoxy groups ratio of from 2:1 to 30:1 which yields an amine-terminated product having an amine equivalent weight of at least 50, and, optionally, (c) a monoepoxy in a remaining active amine hydrogen:epoxy groups ratio of from 5:1 to 20:1.
摘要翻译：用于环氧树脂的水分散性固化剂通过（a）由至少一种环氧树脂的反应获得的环氧官能化合物和源自酸封端的聚亚烷基二醇与二胺的反应的酰氨基胺的反应来制备活性胺氢：环氧基团比例为1:15至1:350，（b）活性胺氢中至少一种多胺：环氧基团比例为2：1至30：1，其产生胺封端具有至少50的胺当量的产物，和任选地（c）剩余活性胺氢环氧基团比例为5:1至20:1的单环氧基。

5. 发明授权

US06221934B1 Aqueous dispersions of epoxy resins 失效
标题翻译：环氧树脂的水性分散体
公开(公告)号：US06221934B1
公开(公告)日：2001-04-24
申请号：US09116923
申请日：1998-07-17
申请人： Charles J. Stark , Jimmy D. Elmore , Gayle Edward Back , Pen-Chung Wang , Ernest Charles Galgoci, Jr.
发明人： Charles J. Stark , Jimmy D. Elmore , Gayle Edward Back , Pen-Chung Wang , Ernest Charles Galgoci, Jr.
IPC分类号： C08K320
CPC分类号： C08J3/03 , C08J2363/00 , C08L63/00 , C08L2666/22
摘要： Stable aqueous emulsions of epoxy resins are provided using an epoxy-functional surfactant prepared by reacting an amidoamine having the formula: wherein R1 is an alkyl, aryl, or arylalkyl group or mixtures thereof having 1 to 15 carbon atoms, R2 is aliphatic, cycloaliphatic, or aromatic group having 2 to 18 carbon atoms optionally containing non-reactive oxygen or at most all average of 4 secondary and/or tertiary nitrogen atoms per structure in the backbone, X and Y are independently a hydrogen, methyl or ethyl group with the provision that if X is methyl or ethyl, Y is hydrogen or if Y is methyl or ethyl, X is hydrogen, and n+m+o is a real number from 40 to 400, and n+o is a real number in an amount effective to provide resin emulsification, and the ratio of (I) to (II) by weight. is in the range of 100:0 to 0:100, the ratio of (I) to (III) by weight in the range of 100:0 to 0:100, and the ratio of (II) to (III) by weight in the range of 100:0 to 0:100, and at least one epoxy resin having a functionality of from greater than 0.8 epoxide group per molecule in an amine to epoxy equivalent ratio of at least 1:2.
摘要翻译：使用环氧官能表面活性剂提供稳定的环氧树脂水性乳液，该表面活性剂通过使具有下式的酰氨基胺反应制备：其中R1是烷基，芳基或芳烷基或其具有1至15个碳原子的混合物，R2是脂族，脂环族，或任选地含有非活性氧的碳原子数为2〜18的芳族基团，或者骨架中每个结构最多具有4个仲和/或叔氮原子的平均值，X和Y独立地为氢，甲基或乙基，如果X是甲基或乙基，Y是氢或Y是甲基或乙基，X是氢，n + m + o是从40到400的实数，n + o是有效量的实数提供树脂乳化，以及（I）与（II）的重量比。在100:0至0:100的范围内，（I）至（III）的重量比在100:0至0:100的范围内，（II）与（III）的重量比在100:0至0:100的范围内，以及至少一种具有至少1：2的胺/环氧当量比的每分子具有大于0.8个环氧基的官能度的环氧树脂。

6. 发明授权

US06956086B2 Water dispersible epoxy resins 有权
标题翻译：水分散环氧树脂
公开(公告)号：US06956086B2
公开(公告)日：2005-10-18
申请号：US10671224
申请日：2003-09-24
申请人： Gayle Edward Back , Pen-Chung Wang , Larry Steven Corley , Jimmy D. Elmore
发明人： Gayle Edward Back , Pen-Chung Wang , Larry Steven Corley , Jimmy D. Elmore
IPC分类号： C08G73/02 , C08J3/03 , C08L63/00 , C08L79/02 , C08F283/00 , C08L77/06
CPC分类号： C08J3/03 , C08G73/028 , C08J2363/00 , C08L63/00 , C08L79/02 , C08L77/00
摘要： A amidoamine composition containing oligomeric amidoamine compounds having the structure: the average of x based on the amidoamine composition is at least 0.2, and Z is the residue of a polyoxyalkylene polyether polycarboxylic acid compound, and the amidoamine composition is the reaction product of primary polyamine compounds with polyoxyalkylene polyether polycarboxylic acid compounds at a corresponding equivalent weight ratio of at least 4.0:1 under oligomeric reaction conditions effective to increase the amine nitrogen equivalent weight of the amidoamine composition by at least 10% over the average acid equivalent weight of said polyoxyalkylene polyether polyacid composition. There is also provided glycidated amidoamine compositions used as epoxy functional surfactants, and the aqueous epoxy resin dispersions thereof, and the curable epoxy resin compositions thereof.
摘要翻译：含有具有以下结构的低聚酰氨基胺化合物的酰氨基胺组合物：基于酰氨基胺组成的x的平均值为至少0.2，Z为聚氧化烯聚醚多元羧酸化合物的残基，酰胺基胺组合物为初级多胺化合物其中聚氧亚烷基聚醚多元羧酸化合物在低聚反应条件下的相应当量重量比至少为4.0:1，有效地将酰氨基胺组合物的胺氮当量重量比所述聚氧化烯聚醚多元酸的平均酸当量重量提高至少10％组成。还提供用作环氧官能表面活性剂的缩水甘油酰氨基胺组合物及其环氧树脂水分散体及其可固化环氧树脂组合物。

7. 发明授权

US06653436B2 Water dispersible epoxy resins 有权
标题翻译：水分散环氧树脂
公开(公告)号：US06653436B2
公开(公告)日：2003-11-25
申请号：US09733290
申请日：2000-12-08
申请人： Gayle Edward Back , Pen-Chung Wang , Larry Steven Corley , Jimmy D. Elmore
发明人： Gayle Edward Back , Pen-Chung Wang , Larry Steven Corley , Jimmy D. Elmore
IPC分类号： C08G6926
CPC分类号： C08J3/03 , C08G73/028 , C08J2363/00 , C08L63/00 , C08L79/02 , C08L77/00
摘要： A amidoamine composition containing oligomeric amidoamine compounds having the structure: the average of x based on the amidoamine composition is at least 0.2, and Z is the residue of a polyoxyalkylene polyether polycarboxylic acid compound, and the amidoamine composition is the reaction product of primary polyamine compounds with polyoxyalkylene polyether polycarboxylic acid compounds at a corresponding equivalent weight ratio of at least 4.0:1 under oligomeric reaction conditions effective to increase the amine nitrogen equivalent weight of the amidoamine composition by at least 10% over the average acid equivalent weight of said polyoxyalkylene polyether polyacid composition. There is also provided glycidated amidoamine compositions used as epoxy functional surfactants, and the aqueous epoxy resin dispersions thereof, and the curable epoxy resin compositions thereof.
摘要翻译：含有具有以下结构的低聚酰氨基胺化合物的酰氨基胺组合物：基于酰氨基胺组成的x的平均值为至少0.2，Z为聚氧化烯聚醚多元羧酸化合物的残基，酰胺基胺组合物为初级多胺化合物其中聚氧亚烷基聚醚多元羧酸化合物在低聚反应条件下的相应当量重量比至少为4.0:1，有效地将酰氨基胺组合物的胺氮当量重量比所述聚氧化烯聚醚多元酸的平均酸当量重量提高至少10％组成。还提供了用作环氧官能表面活性剂的缩水甘油酰氨基胺组合物及其环氧树脂水分散体及其可固化环氧树脂组合物。

8. 发明授权

US06235931B1 Partial oxidation of polyoxyalkylene polyol compositions to polycarboxylic acid compositions 有权
标题翻译：聚氧化烯多元醇组合物对多元羧酸组合物的部分氧化
公开(公告)号：US06235931B1
公开(公告)日：2001-05-22
申请号：US09223549
申请日：1998-12-30
申请人： Pen-Chung Wang , Gayle Edward Back , Glynnda Addicks , Jimmie Dale Elmore , Herbert Elliott Fried
发明人： Pen-Chung Wang , Gayle Edward Back , Glynnda Addicks , Jimmie Dale Elmore , Herbert Elliott Fried
IPC分类号： C07C5127
CPC分类号： C08G65/325 , C08G65/324 , C08L71/02 , C08L63/00
摘要： A process for partially oxidizing and converting a polyoxyalkylene polyol composition to a polycarboxylic acid composition comprising reacting a polyoxyalkylene polyol composition with a stable free radical nitroxide in the presence of an NOx generating compound, a flow of air or oxygen, and optionally water, at elevated temperatures. The oxidation reaction is discontinued by deactivating the catalyst and removing the source of air or oxygen, the NOx generating source, and the optional water. From 60% to no more than 95% of the polyoxyalkylene polyol composition is converted.
摘要翻译：一种将聚氧化烯多元醇组合物部分氧化并转化为多元羧酸组合物的方法，包括在产生NO x的化合物，空气或氧气以及任选的水的存在下，将聚氧化烯多元醇组合物与稳定的自由基氮氧化物反应，温度。通过使催化剂失活并除去空气或氧气源，NOx产生源和任选的水来停止氧化反应。转化聚氧化烯多元醇组合物的60％至不超过95％。

9. 发明授权

US5684080A Aqueous polymer emulsion 失效
标题翻译：水性聚合物乳液
公开(公告)号：US5684080A
公开(公告)日：1997-11-04
申请号：US559523
申请日：1995-11-15
申请人： Evert van der Heide , Gerrit Vietje , Pen-Chung Wang
发明人： Evert van der Heide , Gerrit Vietje , Pen-Chung Wang
IPC分类号： C08G81/00 , B32B21/08 , C08G67/02 , C08K5/17 , C08L73/00 , C08L97/02 , C09J173/00 , C08K5/06
CPC分类号： C09J173/00 , B32B21/08 , C08G67/02 , C08K5/17 , C08L73/00 , C08L97/02 , Y10S524/906 , Y10S525/939 , Y10T428/24066 , Y10T428/31895 , Y10T428/31989
摘要： An emulsion of a copolymer of carbon monoxide with an olefinically unsaturated compound dispersed in an aqueous diluent; a curable resin composition in the form of an oil-in-water emulsion comprising a copolymer of carbon monoxide with an olefinically unsaturated compound and a curing agent; and a process for producing a laminated wood composite comprising applying said curable resin composition onto wood parts of the composite, bringing the wood parts of the composite together such that curable resin composition is positioned between adjacent wood parts, and curing the curable resin such that after curing cured resin adheres adjacent wood parts to one another.
摘要翻译：一氧化碳与分散在水性稀释剂中的烯属不饱和化合物的共聚物的乳液; 包含一氧化碳与烯属不饱和化合物的共聚物和固化剂的水包油乳液形式的可固化树脂组合物; 以及一种生产层压木材复合材料的方法，包括将所述可固化树脂组合物施加到复合材料的木材部分上，使复合材料的木材部分在一起，使得可固化树脂组合物位于相邻的木材部件之间，并固化可固化树脂，固化的固化树脂将相邻的木质部分粘附在一起。

10. 发明授权

US5606006A Trisepoxy resin compositions 失效
标题翻译：三环氧树脂组合物
公开(公告)号：US5606006A
公开(公告)日：1997-02-25
申请号：US629310
申请日：1996-04-08
申请人： Pen-Chung Wang
发明人： Pen-Chung Wang
IPC分类号： C07D407/12 , C07D407/14 , C08G59/20 , C08G59/32 , C08G59/50 , C08G59/62 , C08G59/00
CPC分类号： C07D407/14 , C08G59/3236
摘要： Cure of a novel trisepoxy resin-based composition provides a thermoset having high Tg, low dielectric constant, low water absorption and good flexural strength.
摘要翻译：一种新型三环氧树脂基组合物的固化提供了具有高Tg，低介电常数，低吸水性和良好弯曲强度的热固性材料。

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