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1. 发明申请

WO2006020375A3 A SYNTHESIS GAS PROCESS COMPRISING PARTIAL OXIDATION USING CONTROLLED AND OPTIMIZED TEMPERATURE PROFILE 审中-公开
标题翻译：使用控制和优化温度曲线包含部分氧化的合成气体过程
公开(公告)号：WO2006020375A3
公开(公告)日：2007-05-31
申请号：PCT/US2005026396
申请日：2005-07-26
申请人： CONOCOPHILLIPS CO , DUTTA SUBHASH , WRIGHT HAROLD A
发明人： DUTTA SUBHASH , WRIGHT HAROLD A
IPC分类号： C10J3/00 , C01B3/32
CPC分类号： B01J23/63 , B01J8/009 , B01J8/0411 , B01J8/0438 , B01J8/0453 , B01J8/048 , B01J8/0492 , B01J8/0496 , B01J2208/0015 , B01J2208/00203 , B01J2208/00309 , B01J2208/00548 , B01J2208/00628 , C01B3/386 , C01B2203/0244 , C01B2203/0261 , C01B2203/0283 , C01B2203/1047 , C01B2203/1241 , C01B2203/141 , C01B2203/143 , C01B2203/1614 , Y02P20/52
摘要： This invention relates to methods for reacting a hydrocarbon, molecular oxygen, and optionally water and/or carbon dioxide, to form synthesis gas. The preferred embodiments are characterized by delivering a substochiometric amount of oxygen to each of a multitude of reaction zones, which allows for optimum design of the catalytic packed bed and the gas distribution system, and for the optimization and control of the temperature profile of the reaction zones. The multitude of reaction zones may include a series of successive fixed beds, or a continuous zone housed within an internal structure having porous, or perforated, walls, through which an oxygen-containing stream can permeate. By controlling the oxygen supply, the temperatures, conversion, and product selectivity of the reaction can be in turn controlled and optimized. Furthermore the potential risks of explosion associated with mixing hydrocarbon and molecular oxygen is minimized with increased feed carbon-to-oxygen molar ratios.
摘要翻译：本发明涉及使烃，分子氧和任选的水和/或二氧化碳反应以形成合成气的方法。优选的实施方案的特征在于将几何量的氧气输送到多个反应区域中的每一个，这允许催化填充床和气体分配系统的最佳设计，以及优化和控制反应的温度曲线区域。多个反应区可以包括一系列连续的固定床，或者容纳在具有多孔或穿孔壁的内部结构内的连续区域，含氧流可以通过这些壁渗透。通过控制供氧，可以控制和优化反应的温度，转化率和产物选择性。此外，与碳氢化合物和分子氧混合相关的爆炸的潜在风险可以通过增加进料碳 - 氧摩尔比来最小化。

2. 发明申请

WO2004082819A2 PARTIAL OXIDATION REACTORS AND SYNGAS COOLERS USING NICKEL-CONTAINING COMPONENTS 审中-公开
标题翻译：部分氧化反应器和使用含镍组分的合成冷却剂
公开(公告)号：WO2004082819A2
公开(公告)日：2004-09-30
申请号：PCT/US2004007788
申请日：2004-03-12
申请人： CONOCOPHILLIPS CO , PAN CHIEN-PING , WRIGHT HAROLD A
发明人： PAN CHIEN-PING , WRIGHT HAROLD A
IPC分类号： B01J8/02 , B01J8/18 , B01J19/00 , B01J19/02 , C01B3/38 , C22C19/05 , B01J
CPC分类号： C01B3/386 , B01J8/025 , B01J8/1836 , B01J19/0026 , B01J19/02 , B01J2208/00132 , B01J2219/00247 , B01J2219/0277 , C01B2203/00 , C01B2203/0261 , C01B2203/062 , C01B2203/0883 , C01B2203/1241 , C01B2203/1276 , C22C19/058
摘要： Disclosed are methods and apparatus for producing synthesis gas and higher hydrocarbons from light hydrocarbons and molecular oxygen as well as the higher hydrocarbons produced by the disclosed methods and apparatus. The methods and apparatus disclosed utilize components comprising nickel and nickel alloys.
摘要翻译：公开了由轻烃和分子氧生产合成气和高级烃的方法和装置以及通过所公开的方法和装置生产的高级烃。所公开的方法和装置使用包括镍和镍合金的组件。

3. 发明申请

WO2004092056A3 COGENERATION OF ORGANIC COMPOUNDS WITH SYNTHESIS GAS BY CATALYTIC PARTIAL OXIDATION 审中-公开
标题翻译：有机化合物与合成气体的催化部分氧化
公开(公告)号：WO2004092056A3
公开(公告)日：2005-05-12
申请号：PCT/US2004009665
申请日：2004-03-30
申请人： CONOCOPHILLIPS CO , STRAGUZZI GLORIA I , WOLF MARY E , WRIGHT HAROLD A
发明人： STRAGUZZI GLORIA I , WOLF MARY E , WRIGHT HAROLD A
IPC分类号： C07C2/84 , C07C29/151 , C07C51/215 , C07C67/39 , C07C27/00 , B01J35/02 , C01B3/26 , C07C1/02
CPC分类号： C07C51/215 , C07C2/84 , C07C29/1518 , C07C67/39 , C07C2523/46 , Y02P20/52 , C07C15/02 , C07C53/00 , C07C31/04
摘要： Disclosed herein are methods and apparatuses for cogenerating organic compounds (e.g., benzene, toluene, xylene, formate, acetate, propionate, butyrate, C1-C4 acids, C1-C4 alcohols, methanol, naphthalene, acenaphthylene, fluorene, phenanthrene, anthracene, fluoranthene, and pyrene) along with synthesis gas in a synthesis gas reactor, preferably a catalytic partial oxidation reactor.
摘要翻译：本文公开了有机化合物（例如苯，甲苯，二甲苯，甲酸酯，乙酸酯，丙酸酯，丁酸酯，C 1 -C 4酸，C 1 -C 4醇，甲醇，萘，苊，芴，菲，蒽，荧蒽和芘）以及合成气在合成气反应器中，优选催化部分氧化反应器。

4. 发明申请

WO2004106461A2 RECYCLE OF LOW BOILING POINT PRODUCTS TO A FISCHER-TROPSCH REACTOR 审中-公开
标题翻译：低沸点产品回收到FISCHER-TROPSCH反应器
公开(公告)号：WO2004106461A2
公开(公告)日：2004-12-09
申请号：PCT/US2004016133
申请日：2004-05-20
申请人： CONOCOPHILLIPS CO , ESPINOZA RAFAEL L , WRIGHT HAROLD A , ZHANG JIANPING
发明人： ESPINOZA RAFAEL L , WRIGHT HAROLD A , ZHANG JIANPING
IPC分类号： C07C27/00 , C07C27/06 , C10G20060101 , C10G2/00 , C10G
CPC分类号： C10G2/32
摘要： Methods for reducing the average molecular weight of liquid hydrocarbons in a Fischer-Tropsch reactor are disclosed. The preferred embodiments of the present invention are characterized by feeding a hydrocarbon stream, which lowers the average molecular weight of the hydrocarbon liquids inside the reactor, and more preferably by recycling a portion of low-molecular weight hydrocarbon products back into the reactor. Lowering the molecular weight of the hydrocarbon liquids inside the reactor increases the mass transfer and solubility, and diffusivity of the reactants in the hydrocarbons present in the slurry.
摘要翻译：公开了降低费 - 托反应器中液体烃的平均分子量的方法。本发明的优选实施方案的特征在于进料烃流，其降低反应器内的烃液体的平均分子量，更优选通过将一部分低分子量烃产物再循环回反应器。降低反应器内的烃液体的分子量增加了浆料中存在的烃中的反应物的传质和溶解度以及扩散性。

5. 发明申请

WO2006130280A3 SUPPORTS AND CATALYSTS COMPRISING RARE EARTH ALUMINATES, AND THEIR USE IN PARTIAL OXIDATION 审中-公开
标题翻译：包含稀土铝的支持和催化剂及其在部分氧化中的应用
公开(公告)号：WO2006130280A3
公开(公告)日：2007-11-15
申请号：PCT/US2006015952
申请日：2006-04-26
申请人： CONOCOPHILLIPS CO , ERCAN CEMAL , XIE SHUIBO , WRIGHT HAROLD A , JIN YAMING , WANG DAXIANG , FJARE KRISTI A , MINAHAN DAVID M , ORTEGO BEATRICE C , SIMON DAVID E
发明人： ERCAN CEMAL , XIE SHUIBO , WRIGHT HAROLD A , JIN YAMING , WANG DAXIANG , FJARE KRISTI A , MINAHAN DAVID M , ORTEGO BEATRICE C , SIMON DAVID E
IPC分类号： C01B3/26 , B01J21/04 , B01J21/10 , B01J21/12 , B01J23/00 , B01J23/63 , B01J23/75 , B01J23/89 , B01J37/06 , B01J37/08 , C01B3/38 , C01B3/40
CPC分类号： C01B3/386 , B01J21/04 , B01J21/10 , B01J21/12 , B01J23/002 , B01J23/10 , B01J23/40 , B01J23/464 , B01J23/63 , B01J23/75 , B01J23/8913 , B01J35/002 , B01J35/0053 , B01J35/0066 , B01J35/08 , B01J35/1009 , B01J35/1038 , B01J35/1061 , B01J37/0207 , B01J37/0244 , B01J37/06 , B01J37/08 , B01J37/18 , B01J2523/00 , C01B3/40 , C01B2203/0261 , C01B2203/062 , C01B2203/1011 , C01B2203/1041 , C01B2203/1047 , C01B2203/1064 , C01B2203/1082 , C01B2203/1094 , C01B2203/1241 , C01B2203/1247 , Y02P20/52 , B01J2523/31 , B01J2523/3706 , B01J2523/3737 , B01J2523/822
摘要： The present invention relates to thermally stable supports and catalysts for use in high temperature operation, and methods of preparing such supports and catalysts, which includes adding a rare earth metal to an aluminum-containing precursor prior to calcining. The present invention can be more specifically seen as a support, process and catalyst wherein the thermally stable support comprises two rare earth aluminates of different molar ratios of aluminum to rare earth metal, and optionally, alumina and/or a rare earth oxide. More particularly, the invention relates to the use of noble metal catalysts comprising the thermally stable support for synthesis gas production via partial oxidation of light hydrocarbon (e.g., methane) with minimal deactivation over long-term operations and further relates to gas-to-liquids conversion processes.
摘要翻译：本发明涉及用于高温操作的热稳定性载体和催化剂，以及制备这种载体和催化剂的方法，其包括在煅烧之前向含铝前体中加入稀土金属。本发明可以更具体地看作是一种载体，方法和催化剂，其中热稳定载体包括两种不同摩尔比的铝与稀土金属的稀土铝酸盐，以及任选的氧化铝和/或稀土氧化物。更具体地说，本发明涉及贵金属催化剂的用途，所述催化剂包括热稳定性载体，用于通过在长期操作下具有最小失活的轻质烃（例如甲烷）的部分氧化产生合成气，并且还涉及气体 - 液体转换过程。

6. 发明申请

WO2004060549A8 GASEOUS HYDROCARBON-OXYGEN BUBBLE TANK MIXER 审中-公开
标题翻译：气体碳氢氧化物泡沫搅拌机
公开(公告)号：WO2004060549A8
公开(公告)日：2005-12-08
申请号：PCT/US0339249
申请日：2003-12-11
申请人： CONOCOPHILLIPS CO
发明人： JIANG YI , WRIGHT HAROLD A , JACK DOUG S
IPC分类号： B01F3/02 , B01F13/02 , C01B3/38 , B01J10/00 , B01F3/04 , C01B3/24
CPC分类号： B01F3/02 , B01F13/02 , C01B3/386 , C01B2203/0261 , C01B2203/1276 , Y02P20/582
摘要： The invention relates to methods and apparatus for mixing a plurality of gases. The preferred embodiments of the invention comprise forming bubbles (280) of at least two gases(250), (240) injected separately into a liquid, and passing said bubbles through a gas-induced turbulent liquid region to enhance gas transfer between bubbles and to thereby mix the at least two gases. Creating the gas-induced turbulent liquid region preferably includes using a high gas superficial velocity, and may further include using powered mechanical devices, static internal structures, fluid recirculation (235), or combinations thereof. The gas mixture is preferably supplied to a reaction zone (210). In one embodiment a bubble tank mixer (220) supplies a gas mixture comprising oxygen (250) and a hydrocarbon gas (240) to an oxidation reaction zone (210) disposed above said mixer. In alternative embodiments the reaction zone (210) and mixer (220) may be integrated into the same vessel.
摘要翻译：本发明涉及用于混合多种气体的方法和装置。本发明的优选实施例包括形成分别注入液体中的至少两种气体（250），（240）的气泡（280），并使气泡通过气体引起的湍流液体区域，以增强气泡之间的气体传递和从而混合至少两种气体。产生气体诱导的湍流液体区域优选地包括使用高气体表观速度，并且还可以包括使用动力机械装置，静态内部结构，流体再循环（235）或其组合。气体混合物优选供应到反应区（210）。在一个实施例中，气泡箱混合器（220）将包含氧气（250）和烃气体（240）的气体混合物供应到设置在所述混合器上方的氧化反应区域（210）。在替代实施例中，反应区（210）和混合器（220）可以整合到相同的容器中。

7. 发明申请

WO2004085575A3 COMMERCIAL FISCHER-TROPSCH REACTOR 审中-公开
标题翻译：商业FISCHER-TROPSCH反应堆
公开(公告)号：WO2004085575A3
公开(公告)日：2005-03-31
申请号：PCT/US2004008936
申请日：2004-03-24
申请人： CONOCOPHILLIPS CO , ESPINOZA RAFAEL L , ZHANG JIANPING , WRIGHT HAROLD A , HARKINS TODD H
发明人： ESPINOZA RAFAEL L , ZHANG JIANPING , WRIGHT HAROLD A , HARKINS TODD H
IPC分类号： B01J8/06 , B01J12/00 , B01J23/745 , B01J23/75 , C10G2/00 , C07C27/00 , B01J10/00 , B01J19/32 , B01J35/02
CPC分类号： C10G2/341 , B01J8/06 , B01J8/067 , B01J12/00 , B01J23/745 , B01J23/75 , B01J2208/00053 , B01J2208/00061 , B01J2208/00097 , B01J2208/00212
摘要： A process for producing hydrocarbons comprises providing a multi-tubular reactor having at least 100 tubes units containing a catalyst, each tube being between 2 and 5 meters tall and in thermal contact with a cooling fluid; feeding hydrogen and carbon monoxide to each tube at a linear gas superficial velocity less than about 60 cm/s; and converting the gas feedstream to hydrocarbons on the catalyst, wherein the yield of hydrocarbons in each tube is greater than 100 (kg hydrocarbons)/hr/(m reaction zone). Each tube may have an internal diameter greater than 2 centimeters. The catalyst may be active for Fischer Tropsch synthesis and may comprise cobalt or iron. The maximum difference in the radially-averaged temperature between two points that are axially spaced along the reactor is less than 15°C, preferably less than 10°C. The catalyst loading or intrinsic activity may vary along the length of the reactor.
摘要翻译：制备烃的方法包括提供具有至少100个含有催化剂的管单元的多管式反应器，每个管的高度在2和5米之间并与冷却流体热接触; 以低于约60cm / s的线性气体表观速度向每个管供给氢气和一氧化碳; 并将气体进料流转化为催化剂上的烃，其中每个管中烃的产率大于100（kg烃）/ hr /（m 3反应区）。每根管子的内径可以大于2厘米。该催化剂可用于费 - 托合成，并且可以包含钴或铁。沿着反应器轴向间隔的两个点之间的径向平均温度的最大差值小于15℃，优选小于10℃。催化剂负载或固有活性可以沿反应器的长度变化。

8. 发明申请

WO2004043584A3 NOVEL SYNGAS CATALYSTS AND THEIR METHOD OF USE 审中-公开
标题翻译：新型SYNGAS催化剂及其使用方法
公开(公告)号：WO2004043584A3
公开(公告)日：2004-07-15
申请号：PCT/US0336008
申请日：2003-11-12
申请人： CONOCOPHILLIPS CO
发明人： XIE SHUIBO , RICKETSON CHAD M , MINAHAN DAVID M , JIN YAMING , WRIGHT HAROLD A , WOLF MARY E , ERCAN CEMAL , DUTTA SUBHASH
IPC分类号： B01J21/04 , B01J21/10 , B01J21/12 , B01J23/00 , B01J23/10 , B01J23/40 , B01J23/63 , B01J23/75 , B01J23/89 , B01J35/00 , B01J37/02 , B01J37/06 , B01J37/08 , C01B3/38 , C01B3/40 , B01J23/46 , C01B3/26
CPC分类号： C01B3/40 , B01J21/04 , B01J21/10 , B01J21/12 , B01J23/002 , B01J23/10 , B01J23/40 , B01J23/63 , B01J23/75 , B01J23/8913 , B01J35/002 , B01J37/0201 , B01J37/06 , B01J37/08 , C01B3/386 , C01B2203/0261 , C01B2203/062 , C01B2203/1011 , C01B2203/1017 , C01B2203/1041 , C01B2203/1052 , C01B2203/1064 , C01B2203/1082 , C01B2203/1094 , C01B2203/1241 , C01B2203/1633 , Y02P20/52
摘要： The present invention relates to improved catalyst compositions, as well as methods of making and using such compositions. Preferred embodiments of the present invention comprise catalyst compositions having high melting point metallic alloys, and methods of preparing and using the catalysts. In particular, the metallic alloys are preferably rhodium alloys. Accordingly, the present invention also encompasses an improved method for converting a hydrocarbon containing gas and an atomic oxygen-containing gas to a gas mixture comprising hydrogen and carbon monoxide, i.e., syngas, using the catalyst compositions in accordance with the present invention. In addition, the present invention contemplates an improved method for converting hydrocarbon gas to liquid hydrocarbons using the novel syngas catalyst compositions described herein.
摘要翻译：本发明涉及改进的催化剂组合物，以及制备和使用这些组合物的方法。本发明的优选实施方案包括具有高熔点金属合金的催化剂组合物，以及制备和使用催化剂的方法。特别地，金属合金优选为铑合金。因此，本发明还包括使用本发明的催化剂组合物将含烃气体和原子含氧气体转化为包含氢气和一氧化碳即合成气的气体混合物的改进方法。此外，本发明考虑了使用本文所述的新型合成气催化剂组合物将烃气体转化为液体烃的改进方法。

9. 发明申请

WO2006020375A9 A SYNTHESIS GAS PROCESS COMPRISING PARTIAL OXIDATION USING CONTROLLED AND OPTIMIZED TEMPERATURE PROFILE 审中-公开
标题翻译：采用控制和优化温度曲线合成含部分氧化反应的合成气工艺
公开(公告)号：WO2006020375A9
公开(公告)日：2006-04-06
申请号：PCT/US2005026396
申请日：2005-07-26
申请人： CONOCOPHILLIPS CO , DUTTA SUBHASH , WRIGHT HAROLD A
发明人： DUTTA SUBHASH , WRIGHT HAROLD A
IPC分类号： C01B3/26 , B01J8/00
CPC分类号： B01J23/63 , B01J8/009 , B01J8/0411 , B01J8/0438 , B01J8/0453 , B01J8/048 , B01J8/0492 , B01J8/0496 , B01J2208/0015 , B01J2208/00203 , B01J2208/00309 , B01J2208/00548 , B01J2208/00628 , C01B3/386 , C01B2203/0244 , C01B2203/0261 , C01B2203/0283 , C01B2203/1047 , C01B2203/1241 , C01B2203/141 , C01B2203/143 , C01B2203/1614 , Y02P20/52
摘要： This invention relates to methods for reacting a hydrocarbon, molecular oxygen, and optionally water and/or carbon dioxide, to form synthesis gas. The preferred embodiments are characterized by delivering a substochiometric amount of oxygen to each of a multitude of reaction zones, which allows for optimum design of the catalytic packed bed and the gas distribution system, and for the optimization and control of the temperature profile of the reaction zones. The multitude of reaction zones may include a series of successive fixed beds, or a continuous zone housed within an internal structure having porous, or perforated, walls, through which an oxygen-containing stream can permeate. By controlling the oxygen supply, the temperatures, conversion, and product selectivity of the reaction can be in turn controlled and optimized. Furthermore the potential risks of explosion associated with mixing hydrocarbon and molecular oxygen is minimized with increased feed carbon-to-oxygen molar ratios.
摘要翻译：本发明涉及使烃，分子氧和任选的水和/或二氧化碳反应以形成合成气的方法。优选的实施方案的特征在于向多个反应区中的每一个递送低浓度的氧气，这允许催化填充床和气体分配系统的最佳设计，并且用于优化和控制反应的温度曲线区域。多个反应区可以包括一系列连续的固定床，或者容纳在内部结构内的连续区，该内部结构具有多孔或穿孔壁，含氧流可穿过该壁。通过控制氧气供应，反应的温度，转化率和产物选择性可以被控制和优化。此外，随着进料碳 - 氧摩尔比的增加，与混合烃和分子氧相关的爆炸的潜在风险被最小化。

10. 发明申请

WO2004088226A3 GAS AGITATED MULTIPHASE CATALYTIC REACTOR WITH REDUCED BACKMIXING 审中-公开
标题翻译：具有降低回弹性能的气体催化多相催化反应器
公开(公告)号：WO2004088226A3
公开(公告)日：2005-04-28
申请号：PCT/US2004008937
申请日：2004-03-24
申请人： CONOCOPHILLIPS CO , JIANG YI , ZHANG JIANPING , ESPINOZA RAFAEL L , WRIGHT HAROLD A
发明人： JIANG YI , ZHANG JIANPING , ESPINOZA RAFAEL L , WRIGHT HAROLD A
IPC分类号： B01F13/02 , B01F15/00 , B01J8/22 , B01J19/00 , B01J19/24 , C10G2/00 , C07C27/00 , B01J35/02
CPC分类号： C10G2/34 , B01F13/0255 , B01F15/00915 , B01F2215/0422 , B01F2215/0427 , B01F2215/0431 , B01J8/22 , B01J19/006 , B01J19/24 , B01J2208/00132 , B01J2208/00141 , B01J2208/0084 , B01J2219/00081 , B01J2219/00083 , B01J2219/00777
摘要： The present invention provides an apparatus and method for optimizing the degree of backmixing within a gas agitated multiphase reactor at a given gas linear velocity. The embodiments of the present invention involve novel configurations of the multiphase reactor internal structures. In general, the configurations comprise creating a dense area of internal structures in the central region and/or wall regions of the multiphase reactor.
摘要翻译：本发明提供一种用于在给定气体线速度下优化气体搅拌多相反应器内的回混程度的装置和方法。本发明的实施例涉及多相反应器内部结构的新颖结构。通常，构造包括在多相反应器的中心区域和/或壁区域中产生密集的内部结构区域。

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