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1. 发明申请

WO2004080942B1 PROCESS FOR OBTAINING FATTY ACID ALKYL ESTERS, ROSIN ACIDS AND STEROLS FROM CRUDE TALL OIL 审中-公开
标题翻译：从原油高油获得脂肪酸烷基酯，松香酸和甾醇的方法
公开(公告)号：WO2004080942B1
公开(公告)日：2004-10-28
申请号：PCT/BR2004000016
申请日：2004-02-20
申请人： COGNIS BRASIL LTD , SATO SETSUO , SOUSA SALES HENRIQUE JORGE , PELOGGIA HERCULES , KEMPERS PETER , BOTH SABINE , SCHOERKEN ULRICH , WOLF THOMAS
发明人： SATO SETSUO , SOUSA SALES HENRIQUE JORGE , PELOGGIA HERCULES , KEMPERS PETER , BOTH SABINE , SCHOERKEN ULRICH , WOLF THOMAS
IPC分类号： C07C51/42 , C07C67/08 , C07J75/00 , C11B13/00 , C11C1/10 , C11C3/00 , C12P7/62 , C07C67/02 , C07J9/00
CPC分类号： C07C51/42 , C07C51/44 , C07C67/08 , C07C67/54 , C07J9/00 , C07J51/00 , C07J75/00 , C11B13/005 , C11C1/10 , C11C3/003 , C12P7/62 , C12P7/649 , Y02E50/13 , Y02W30/74 , C07C57/26 , C07C61/29 , C07C69/24 , C07C69/58 , C07C69/52 , C07C69/587
摘要： The invention refers to a process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil (CTO), which is characterised by the following steps: (a) reacting the free fatty acids present in the CTO with lower alcohols; (b) esterifying the sterols in the CTO with boric acid or transesteriying with catalyst; (c) separating the fatty acid lower alkyl esters and rosin acids from 10 the remaining sterol borate esters or sterol esters of fatty acids to produce a stream of sterol esters; (d) separating the fatty acid alkyl esters from the rosin acids to produce a first stream of fatty acid alky esters and a second stream of rosin acids; and (e) converting said sterol esters into the free sterols to produce a third stream of free sterols.
摘要翻译：本发明涉及从粗妥尔油（CTO）获得脂肪酸烷基酯，松香酸和甾醇的方法，其特征在于以下步骤：（a）使存在于CTO中的游离脂肪酸与低级醇反应; （b）用硼酸酯化CTO中的甾醇或与催化剂进行酯交换; （c）从剩余的甾醇硼酸酯或脂肪酸的甾醇酯中分离脂肪酸低级烷基酯和松香酸以产生甾醇酯的物流; （d）从松香酸中分离脂肪酸烷基酯以产生第一股脂肪酸烷基酯和第二股松香酸; 和（e）将所述甾醇酯转化成游离甾醇以产生游离甾醇的第三流。

2. 发明申请

WO2008003420A3 PROCESS FOR PRODUCTION OF FATTY ACIDS, FATTY ACID ESTERS AND STEROLESTERS FROM SOAPSTOCK 审中-公开
标题翻译：用于生产脂肪酸，脂肪酸酯和皂甙的脱水剂的方法
公开(公告)号：WO2008003420A3
公开(公告)日：2008-02-28
申请号：PCT/EP2007005663
申请日：2007-06-27
申请人： COGNIS IP MAN GMBH , KEMPERS PETER , SCHOERKEN ULRICH , WOLF THOMAS , SATO SETSUO , BUENO DE ALMEIDA WANDERSON , SILVA BIZZARRI PABLO , SHIGUERU ARAUJO ALEXSSANDER
发明人： KEMPERS PETER , SCHOERKEN ULRICH , WOLF THOMAS , SATO SETSUO , BUENO DE ALMEIDA WANDERSON , SILVA BIZZARRI PABLO , SHIGUERU ARAUJO ALEXSSANDER
IPC分类号： C11B13/02 , A23K1/16 , C11C3/10
CPC分类号： C11B13/02 , A23L33/11 , C10G2300/1011 , C11C1/045 , C11C1/10 , C11C3/003 , Y02E50/13 , Y02P30/20 , Y02W30/74
摘要： The invention relates to a first process for production of fatty acids directly from any soapstock generated in the alkali refining process comprising of a) adding a lipase directly to the alkaline soapstock to facilitate hydrolysis of mono-,di- and triglycerides without prior neutralisation b) neutralizing and splitting the soaps with strong acids until reaching pH 1-6, c) separating the fatty acid phase from the aqueous by settling and/or centrifugation. In a second embodiment a second process for production of fatty acids directly from any soapstock is subject of the invention. This process comprises i) neutralizing and splitting the soaps with strong acids until reaching pH 1-6 ii) adding a lipase to facilitate mono-/di-/triglyceride hydrolysis iii) separating the fatty acid phase from the aqueous by settling and / or centrifugation In a further subject matter the invention deals with the use of said fatty acids for enzymatic or chemical synthesis of C1 to C6 alcanol esters and / or for chemical dimerisation of the fatty acids. As a consequence the invention also refers to a process for obtaining sterolesters and/or fatty acid esters characterized in that the fatty acids obtained according to the processes for production of fatty acids directly from any soapstock as aforementioned described are a) esterified with C1 to C6 alkanol with a Lipase that is selective for fatty acids and does not transesterify the sterolesters b) the fatty acid esters are separated from the sterolesters by distillation The use of said sterolesters for animal feed, food, health foods and as pharmaceutical agent for lowering cholesterol and/or as precursor for steroid synthesis as well as the use of said fatty acid esters as solvent, for the production of fatty alcohols, as biofuel, and biodiesel, as plastisicer or for dimerization is also subject of the invention.
摘要翻译：本发明涉及直接从碱炼油工艺中产生的任何皂料生产脂肪酸的第一种方法，包括a）将脂肪酶直接加入到碱性皂脚中以促进单甘油酯，二甘油酯和甘油三酯的水解，而无需事先中和b）用强酸中和和分解肥皂直至达到pH1-6，c）通过沉降和/或离心将脂肪酸相与水分离。在第二个实施方案中，直接从任何皂脚生产脂肪酸的第二种方法是本发明的主题。该方法包括i）用强酸中和和分解肥皂直至达到pH 1-6，ii）加入脂肪酶以促进甘油一酯/甘油二酯/甘油三酯水解，iii）通过沉降和/或离心将脂肪酸相与水分离在另一主题中，本发明涉及所述脂肪酸用于酶促或化学合成C 1至C 6烷醇酯和/或用于化学二聚化脂肪酸的用途。因此，本发明还涉及用于获得胆固醇酯和/或脂肪酸酯的方法，其特征在于根据如前所述的任何皂料直接生产脂肪酸的方法获得的脂肪酸a）用C 1至C 6酯化链烷醇与对脂肪酸具有选择性且不使胆固醇酯交换酯基的脂肪酶反应b）通过蒸馏将脂肪酸酯与胆固醇酯分离所述胆固醇酯用于动物饲料，食品，保健食品和作为药物用于降低胆固醇和 /或作为类固醇合成的前体以及所述脂肪酸酯作为溶剂的用途，用于生产脂肪醇，生物燃料和生物柴油，作为增塑剂或用于二聚化也是本发明的主题。

3. 发明申请

WO2011038857A3 ALKOXYLATED GLYCEROL ACETALS AND THEIR DERIVATIVES 审中-公开
标题翻译：烷氧基化甘油乙缩醛及其衍生物
公开(公告)号：WO2011038857A3
公开(公告)日：2011-08-25
申请号：PCT/EP2010005825
申请日：2010-09-23
申请人： COGNIS IP MAN GMBH , FLEUTE-SCHLACHTER INGO , HELDT SANDRA , KEMPERS PETER , SCHOERKEN ULRICH , PAETZOLD ECKHARD , KRAGL UDO
发明人： FLEUTE-SCHLACHTER INGO , HELDT SANDRA , KEMPERS PETER , SCHOERKEN ULRICH , PAETZOLD ECKHARD , KRAGL UDO
IPC分类号： C07D317/18 , A01N35/02 , C07D319/06
CPC分类号： C07D317/18 , A01N43/28 , A01N43/32 , C07D319/06 , C08G65/2606 , C08G2650/44
摘要： Suggested are alkoxylated glycerol acetals according to formulae (Ia) and (Ib) in which R1 stands for a linear or branched, saturated or unsaturated and optionally substituted hydrocarbyl residue comprising 6 to 22 carbon atoms and O or 1 to 3 double bonds, a benzyl or furfuryl radical, R2 stands for hydrogen, an alkyl, alkenyl or hydroxyalkyl group having 6 to 22 carbon atoms or an acyl group having 6 to 22 carbon atoms and 0 or 1 to 3 double bonds, AO represents an ethylene oxide, an propylene oxide, an butylene oxide unit or their mixtures, and n stands for an integer of about 1 to about 100.
摘要翻译：建议的是根据式（Ia）和（Ib）的烷氧基化甘油缩醛，其中R 1代表包含6至22个碳原子和0或1至3个双键的直链或支链，饱和或不饱和和任选取代的烃基残基，或糠基，R2代表氢，具有6-22个碳原子的烷基，烯基或羟烷基或具有6-22个碳原子和0或1-3个双键的酰基，AO代表环氧乙烷，环氧丙烷，环氧丁烷单元或它们的混合物，并且n代表约1至约100的整数。

4. 发明申请

WO2011038857A8 ALKOXYLATED GLYCEROL ACETALS AND THEIR DERIVATIVES 审中-公开
标题翻译：烷氧基甘氨酸及其衍生物
公开(公告)号：WO2011038857A8
公开(公告)日：2012-01-05
申请号：PCT/EP2010005825
申请日：2010-09-23
申请人： COGNIS IP MAN GMBH , FLEUTE-SCHLACHTER INGO , HELDT SANDRA , KEMPERS PETER , SCHOERKEN ULRICH , PAETZOLD ECKHARD , KRAGL UDO
发明人： FLEUTE-SCHLACHTER INGO , HELDT SANDRA , KEMPERS PETER , SCHOERKEN ULRICH , PAETZOLD ECKHARD , KRAGL UDO
IPC分类号： C07D317/18 , A01N35/02 , C07D319/06
CPC分类号： C07D317/18 , A01N43/28 , A01N43/32 , C07D319/06 , C08G65/2606 , C08G2650/44
摘要： Suggested are alkoxylated glycerol acetals according to formulae (Ia) and (Ib) in which R1 stands for a linear or branched, saturated or unsaturated and optionally substituted hydrocarbyl residue comprising 6 to 22 carbon atoms and O or 1 to 3 double bonds, a benzyl or furfuryl radical, R2 stands for hydrogen, an alkyl, alkenyl or hydroxyalkyl group having 6 to 22 carbon atoms or an acyl group having 6 to 22 carbon atoms and 0 or 1 to 3 double bonds, AO represents an ethylene oxide, an propylene oxide, an butylene oxide unit or their mixtures, and n stands for an integer of about 1 to about 100.
摘要翻译：建议根据式（Ia）和（Ib）的烷氧基化甘油缩醛，其中R 1表示直链或支链，饱和或不饱和和任选取代的包含6至22个碳原子和O或1至3个双键的烃基，苄基或糠基，R 2表示氢，具有6至22个碳原子的烷基，烯基或羟烷基或具有6至22个碳原子的酰基和0或1至3个双键，AO表示环氧乙烷，环氧丙烷，环氧丁烷单元或其混合物，n表示约1至约100的整数。

5. 发明专利

CA2516598C PROCESS FOR OBTAINING FATTY ACID ALKYL ESTERS, ROSIN ACIDS AND STEROLS FROM CRUDE TALL OIL 未知
公开(公告)号：CA2516598C
公开(公告)日：2012-08-07
申请号：CA2516598
申请日：2004-02-20
申请人： COGNIS BRASIL LTD
发明人： SATO SETSUO , SOUSA SALES HENRIQUE JORGE , PELOGGIA HERCULES , KEMPERS PETER , BOTH SABINE , SCHOERKEN ULRICH , WOLF THOMAS
IPC分类号： C11C3/04 , C07C51/42 , C07C51/44 , C07C67/02 , C07C67/08 , C07C67/54 , C07J9/00 , C07J75/00 , C11B13/00 , C11C1/10 , C11C3/00 , C12P7/62
摘要： The invention refers to a process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil (CTO), which is characteri~sed by the following steps: (a) reacting the free fatty acids present in the CTO with lower alcohols; (b) esterifying the sterols in the CTO with boric acid or transesteri~ying with catalyst; (c) separating the fatty acid lower alkyl esters and rosin acids from 10 the remaining sterol borate esters or sterol esters of fatty acids to produce a stream of sterol esters; (d) separating the fatty acid alkyl esters from the rosin acids to pro~duce a first stream of fatty acid alky esters and a second stream of rosin a~cids; and (e) converting said sterol esters into the free sterols to produce a third stream of free sterols.

6. 发明专利

NO20053894A 未知
公开(公告)号：NO20053894A
公开(公告)日：2005-08-19
申请号：NO20053894
申请日：2005-08-19
申请人： COGNIS BRASIL LTD
发明人： SCHORKEN ULRICH , SATO SETSUO , SALES HENRIQUE JORGE SOUSA , PELOGGIA HERCULES , KEMPERS PETER , BOTH SABINE , WOLF THOMAS
IPC分类号： C07C51/42 , C07C67/08 , C07J75/00 , C11B13/00 , C11C1/10 , C11C3/00 , C12P7/62 , C07C67/02 , C01B13/00
CPC分类号： C07C51/42 , C07C51/44 , C07C67/08 , C07C67/54 , C07J9/00 , C07J51/00 , C07J75/00 , C11B13/005 , C11C1/10 , C11C3/003 , C12P7/62 , C12P7/649 , Y02E50/13 , Y02W30/74 , C07C57/26 , C07C61/29 , C07C69/24 , C07C69/58 , C07C69/52 , C07C69/587

7. 发明专利

CA2516598A1 PROCESS FOR OBTAINING FATTY ACID ALKYL ESTERS, ROSIN ACIDS AND STEROLS FROM CRUDE TALL OIL 未知
公开(公告)号：CA2516598A1
公开(公告)日：2004-09-23
申请号：CA2516598
申请日：2004-02-20
申请人： COGNIS BRASIL LTD
发明人： SATO SETSUO , PELOGGIA HERCULES , SOUSA SALES HENRIQUE JORGE , WOLF THOMAS , KEMPERS PETER , BOTH SABINE , SCHOERKEN ULRICH
IPC分类号： C07C51/42 , C07C67/08 , C07J75/00 , C11B13/00 , C11C1/10 , C11C3/00 , C12P7/62 , C07C67/02 , C07J9/00
摘要： The disclosed invention refers to a process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil (CTO), which is characterized by the following steps: (a) reacting the free fatty acids present in the CTO with lower alcohols; (b) esterifying the sterols in the CTO with boric acid or transesterifying the sterols with a catalyst; (c) separating the fatty acid lower alkyl esters and rosin acids from the remaining sterol borate esters or sterol esters of fatty acids to produce a stream of sterol esters; (d) separating the fatty acid alkyl esters from the rosin acids to produce a first stream of fatty acid alky esters and a second stream of rosin acids; and (e) converting the sterol esters into the free sterols to produce a third stream of free sterols.

8. 发明专利

AU2003303929A1 PROCESS FOR OBTAINING FATTY ACID ALKYL ESTERS, ROSIN ACIDS AND STEROLS FROM CRUDE TALL OIL 未知
公开(公告)号：AU2003303929A1
公开(公告)日：2004-09-09
申请号：AU2003303929
申请日：2003-02-21
申请人： COGNIS BRASIL LTD
发明人： SATO SETSUO , SALES HENRIQUE JORGE SOUSA , PELOGGIA HERCULES , KEMPERS PETER , BOTH SABINE , SCHORKEN ULRICH , WOLF THOMAS
IPC分类号： C07C51/42 , C07C67/08 , C07J75/00 , C11B13/00 , C11C1/10 , C11C3/00 , C12P7/62 , C07C67/02
摘要： The disclosed invention refers to a process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil (CTO), which is characterized by the following steps: (a) reacting the free fatty acids present in the CTO with lower alcohols; (b) esterifying the sterols in the CTO with boric acid or transesterifying the sterols with a catalyst; (c) separating the fatty acid lower alkyl esters and rosin acids from the remaining sterol borate esters or sterol esters of fatty acids to produce a stream of sterol esters; (d) separating the fatty acid alkyl esters from the rosin acids to produce a first stream of fatty acid alky esters and a second stream of rosin acids; and (e) converting the sterol esters into the free sterols to produce a third stream of free sterols.

9. 发明专利

NO20053893L 未知
公开(公告)号：NO20053893L
公开(公告)日：2005-08-19
申请号：NO20053893
申请日：2005-08-19
申请人： COGNIS BRASIL LTD
发明人： SCHORKEN ULRICH , SATO SETSUO , SALES HENRIQUE JORGE SOUSA , PELOGGIA HERCULES , KEMPERS PETER , BOTH SABINE , WOLF THOMAS
IPC分类号： C07C51/42 , C07C67/08 , C07J75/00 , C11B13/00 , C11C1/10 , C11C3/00 , C12P7/62 , C07C67/02 , C01B13/00
摘要： The disclosed invention refers to a process for obtaining fatty acid alkyl esters, rosin acids and sterols from crude tall oil (CTO), which is characterized by the following steps: (a) reacting the free fatty acids present in the CTO with lower alcohols; (b) esterifying the sterols in the CTO with boric acid or transesterifying the sterols with a catalyst; (c) separating the fatty acid lower alkyl esters and rosin acids from the remaining sterol borate esters or sterol esters of fatty acids to produce a stream of sterol esters; (d) separating the fatty acid alkyl esters from the rosin acids to produce a first stream of fatty acid alky esters and a second stream of rosin acids; and (e) converting the sterol esters into the free sterols to produce a third stream of free sterols.

10. 发明专利

NO20053893A 未知
公开(公告)号：NO20053893A
公开(公告)日：2005-08-19
申请号：NO20053893
申请日：2005-08-19
申请人： COGNIS BRASIL LTD
发明人： SCHORKEN ULRICH , SATO SETSUO , SALES HENRIQUE JORGE SOUSA , PELOGGIA HERCULES , KEMPERS PETER , BOTH SABINE , WOLF THOMAS
IPC分类号： C07C51/42 , C07C67/08 , C07J75/00 , C11B13/00 , C11C1/10 , C11C3/00 , C12P7/62 , C07C67/02 , C01B13/00
CPC分类号： C07C51/42 , C07C51/44 , C07C67/08 , C07C67/54 , C07J9/00 , C07J51/00 , C07J75/00 , C11B13/005 , C11C1/10 , C11C3/003 , C12P7/62 , C12P7/649 , Y02E50/13 , Y02W30/74 , C07C57/26 , C07C61/29 , C07C69/24 , C07C69/58 , C07C69/52 , C07C69/587

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