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    • 7. 发明专利
    • DE60200241T2
    • 2005-01-27
    • DE60200241
    • 2002-08-08
    • CENTRAL GLASS CO LTD
    • KOMATA TAKEOKAWAMURA MATSUEII NARIAKI
    • C07D311/58
    • A first process for producing a benzopyran carboxamide represented by the general formula Ä1Ü includes reacting 3-aminopropionitrile.1/2 sulfate, N IDENTICAL CCH2CH2NH2.1/2(H2SO4), with a benzopyran carboxylic halide represented by the general formula Ä2Ü, in the presence of a base. A second process for producing the benzopyran carboxamide includes the steps of (a) reacting 3-aminopropionitrile.1/2 sulfate with a base, thereby forming 3-aminopropionitrile; and (b) reacting the 3-aminopropionitrile with the benzopyran carboxylic halide Ä2Ü, thereby producing the benzopyran carboxamide. A process for stabilizing 3-aminopropionitrile includes turning the 3-aminopropionitrile into a sulfate of the 3-aminopropionitrile. where R is a straight-chain or non-straight-chain perfluoroalkyl group represented by CnF2n+1 where n is an integer of 1-10; and X is fluorine, chlorine, bromine or iodine.