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1. 发明专利

DE69929736T2 未知
公开(公告)号：DE69929736T2
公开(公告)日：2006-11-02
申请号：DE69929736
申请日：1999-11-05
申请人： CENTRAL GLASS CO LTD , NIPPON ZEON CO
发明人： TAKADA NAOTO , KANAI MASATOMI , IMURA HIDEAKI , KOMATA TAKEO
IPC分类号： C07C17/21 , C07C17/00 , C07C17/04 , C07C17/20 , C07C23/08
摘要： The invention relates to a method for preparing a fluorinated product that is a first perhalogenated five-membered cyclic compound (e.g., 1,2-dichlorohexafluorocyclopentene and 1,1-dichlorooctafluorocyclopentane). This method includes reacting in a gas phase a starting material that is a second perhalogenated five-membered cyclic compound having at least one unsaturated bond, at substantially the same time with chlorine and hydrogen fluoride, in the presence of a fluorination catalyst containing an activated carbon optionally carrying thereon a metal compound, thereby to decrease the number of the at least one unsaturated bond and to increase the number of fluorine atoms of the second compound. The method is appropriate for the production of the first perhalogenated five-membered cyclic compound in an industrial scale.

2. 发明专利

DE69929736D1 未知
公开(公告)号：DE69929736D1
公开(公告)日：2006-04-20
申请号：DE69929736
申请日：1999-11-05
申请人： CENTRAL GLASS CO LTD , NIPPON ZEON CO
发明人： TAKADA NAOTO , KANAI MASATOMI , IMURA HIDEAKI , KOMATA TAKEO
IPC分类号： C07C17/21 , C07C17/00 , C07C17/04 , C07C17/20 , C07C23/08
摘要： The invention relates to a method for preparing a fluorinated product that is a first perhalogenated five-membered cyclic compound (e.g., 1,2-dichlorohexafluorocyclopentene and 1,1-dichlorooctafluorocyclopentane). This method includes reacting in a gas phase a starting material that is a second perhalogenated five-membered cyclic compound having at least one unsaturated bond, at substantially the same time with chlorine and hydrogen fluoride, in the presence of a fluorination catalyst containing an activated carbon optionally carrying thereon a metal compound, thereby to decrease the number of the at least one unsaturated bond and to increase the number of fluorine atoms of the second compound. The method is appropriate for the production of the first perhalogenated five-membered cyclic compound in an industrial scale.

3. 发明专利

JP2000198752A PRODUCTION OF FLUORINATED CYCLOPENTANE 失效
公开(公告)号：JP2000198752A
公开(公告)日：2000-07-18
申请号：JP30146599
申请日：1999-10-22
申请人： NIPPON ZEON CO , CENTRAL GLASS CO LTD
发明人： TAKADA NAOKADO , KANAI MASATOMI , KOMATA TAKEO
IPC分类号： B01J21/18 , B01J23/18 , B01J23/20 , B01J23/89 , B01J35/10 , C07B61/00 , C07C17/04 , C07C17/21 , C07C23/08
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a chlorofluorocyclopentane useful as a raw material for producing a fluorinated cyclopentane in an industrial scale. SOLUTION: This method for producing a chlorofluorocyclopentane of formula III: C5ClDF10-D (D is an integer of 0-9; D

4. 发明专利

JP2006151998A Method for producing octafluorocyclopentene 有权
标题翻译：生产OCTAFLOOCOCOCOPENTENE的方法
公开(公告)号：JP2006151998A
公开(公告)日：2006-06-15
申请号：JP2006049387
申请日：2006-02-24
申请人： Central Glass Co Ltd , Nippon Zeon Co Ltd , セントラル硝子株式会社 , 日本ゼオン株式会社
发明人： KOMATA TAKEO , NISHINOMIYA TAKAYUKI , SAKU FUYUHIKO , IMURA HIDEAKI , UJIIE MIKIO , KANAI MASATOMI
IPC分类号： C07C17/20 , B01J27/08 , B01J27/122 , B01J27/125 , B01J27/128 , B01J27/132 , B01J27/138 , C07B61/00 , C07C23/08
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an octafluorocyclopentene, which is suitable for manufacture on a industrial scale. SOLUTION: The octafluorocyclopentene is manufactured by the following first process and second process. In the first process, a mixture of perhalogenated cyclopentene represented by General formula (2): C 5 Cl B F 8-B (wherein B is an integer of from 0 to 7, and A is larger than B) is obtained by fluorinating a perhalogenated cyclopentene represented by General formula (1): C 5 Cl A F 8-A (wherein A is an integer of from 1 to 8) with hydrogen fluoride, in the presence of a fluorinated catalyst selected from the group consisting of chromium, antimony, iron, zinc, cobalt, nickel, copper, manganese and aluminum, in a gas phase. In the second process, the octafluorocyclopentene is obtained by fluorinating the mixture of perhalogenated cyclopentene represented by General formula (2) obtained in the first process, with a metal fluoride. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：待解决的问题：提供适用于工业规模制造的八氟环戊烯的制造方法。解决方案：八氟环戊烯通过以下第一工艺和第二工艺制造。在第一方法中，由通式（2）表示的全卤代环戊烯的混合物：其中B（B）为0〜7的整数，A为大于B的整数）通过氟化由通式（1）表示的全卤代环戊烯获得：C 5 在选自铬，锑，铁，锌，钴，镍的氟化催化剂存在下，使用氟化氢的SBA 8-A （其中A为1至8的整数），铜，锰和铝，在气相中。在第二种方法中，通过氟化氟化第一种方法得到的由通式（2）表示的全卤代环戊烯的混合物，得到八氟环戊烯。版权所有（C）2006，JPO＆NCIPI

5. 发明专利

JPH11152237A PRODUCTION OF PERHALOGENATED CYCLOPENTENE 失效
公开(公告)号：JPH11152237A
公开(公告)日：1999-06-08
申请号：JP19414098
申请日：1998-07-09
申请人： NIPPON ZEON CO , CENTRAL GLASS CO LTD
发明人： KOMATA TAKEO , NISHINOMIYA TAKAYUKI , SAKU FUYUHIKO , IMURA HIDEAKI , UJIIE MIKIO , KANAI MASATOMI
IPC分类号： B01J27/132 , C07B61/00 , C07C17/20 , C07C17/21 , C07C23/08
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a perhalogenated fluorocyclopentene, suitable for a production on an industrial scale. SOLUTION: This method for producing a perhalogenated cyclopentene of the general formula (2) C5 ClBF8- B (B is an integer of 1-7) comprises fluorinating a perhalogenated cyclopentene of the general formula (1) C5 ClAF8- A (A is an integer of 1-8; A>=B) with hydrogen fluoride in a vapor phase in the presence of a fluorinating catalyst.

6. 发明申请

WO2004037760A2 PROCESS FOR PRODUCING OPTICALLY ACTIVE 2-ALKOXY-1-(TRIFLUOROMETHYL-SUBSTITUTED PHENYL)ETHANOL DERIVATIVES 审中-公开
标题翻译：生产光学活性2-烷氧基-1-（三氟甲基取代苯基）乙醇衍生物的方法
公开(公告)号：WO2004037760A2
公开(公告)日：2004-05-06
申请号：PCT/JP0313474
申请日：2003-10-22
申请人： CENTRAL GLASS CO LTD , ISHII AKIHIRO , KANAI MASATOMI , KURIYAMA YOKUSU , YASUMOTO MANABU , INOMIYA KENJIN , OOTSUKA TAKASHI , UEDA KOJI
发明人： ISHII AKIHIRO , KANAI MASATOMI , KURIYAMA YOKUSU , YASUMOTO MANABU , INOMIYA KENJIN , OOTSUKA TAKASHI , UEDA KOJI
IPC分类号： C07B53/00 , C07B61/00 , C07C41/26 , C07C43/178 , C07C59/56 , C07C67/08 , C07C69/732 , C07D309/12 , C07C43/00
CPC分类号： C07D309/12 , C07B2200/07 , C07C43/1786 , C07C59/56 , C07C69/732
摘要： A process for producing an optically active 2-alkoxy-1-(trifluoromethyl-substituted phenyl)ethanol derivative represented by the formula 5: where R2 represents a C1-C6 lower alkyl group, n represents 1 or 2 and * represents a chiral carbon, includes the steps of (a) reducing an optically active, hydroxyl-protective, trifluoromethyl-substituted mandelate represented by the formula 1, by a hydride reducing agent, into an optically active, hydroxyl-protective 2-hydroxy-1-(trifluoromethyl-substituted phenyl)ethanol represented by the formula 2; (b) reacting the hydroxyl-protective hydroxyethanol represented by the formula 2, with an alkylation agent represented by the formula 3, in the presence of a base, thereby producing an optically active, hydroxyl-protective 2-alkoxy-1-(trifluoromethyl-substituted phenyl)ethanol represented by the formula 4; and (c) deprotecting the hydroxyl-protective alkoxyethanol represented by the formula 4 into the alkoxyethanol derivative represented by the formula 5.
摘要翻译：制备由式5表示的光学活性2-烷氧基-1-（三氟甲基取代的苯基）乙醇衍生物的方法：其中R 2表示C 1 -C 6低级烷基，n表示1或2，*表示手性碳，包括以下步骤：（a）通过氢化物还原剂将由式1表示的光学活性的羟基保护的三氟甲基取代的扁桃酸酯还原成光学活性的羟基保护的2-羟基-1-（三氟甲基取代的苯基）乙醇; （b）使由式2表示的羟基保护性羟基乙醇与式3表示的烷基化剂在碱的存在下反应，由此制备光学活性的羟基保护性2-烷氧基-1-（三氟甲基 - 取代的苯基）乙醇; 和（c）将由式4表示的羟基保护性烷氧基乙醇脱保护成由式5表示的烷氧基乙醇衍生物。

7. 发明专利

DE69829678D1 未知
公开(公告)号：DE69829678D1
公开(公告)日：2005-05-12
申请号：DE69829678
申请日：1998-09-17
申请人： CENTRAL GLASS CO LTD , ZEON CORP
发明人： KOMATA TAKEO , NISHIMIYA TAKAYUKI , SAKYU FUYUHIKO , IMURA HIDEAKI , UJIIE MIKIO , KANAI MASATOMI
IPC分类号： C07B61/00 , C07C17/20 , C07C17/21 , B01J27/132 , C07C23/08
摘要： The invention relates to a method for producing a first perhalogenated cyclopentene represented by the general formula: C5ClBF8-B where B is an integer of from 0 to 7. The method includes a step of (a) fluorinating a second perhalogenated cyclopentene by hydrogen fluoride in a gas phase in the presence of a fluorination catalyst. The second perhalogenated cyclopentene is represented by general formula: C5ClAF8-A where A is an integer of from 1 to 8, and A is not smaller than B. With this method, the first perhalogenated cyclopentene (e.g., 1,2-dichloro-3,3,4,4,5,5-hexafluorocyclopentene, another chlorofluorinated cyclopentene, or octafluorocyclopentene) can continuously easily be produced, for example, from octachlorocyclopentene obtained by chlorination of hexachlorocyclopentadiene that is easily available. Therefore, the above method is very useful as an industrial scale production method. In case that the first perhalogenated cyclopentene is octafluorocyclopentene, the method may further include a step of (b) fluorinating a reaction product of the step (a) in a way that is different from that of the step (a), thereby to convert said reaction product of the step (a) into octafluoropentene. The step (a) may be conducted by a multistep reaction wherein there are provided "m" of reaction zones in number where m is an integer of from 2 to 10. In this case, the reaction zones are arranged in series and such that a reaction temperature of each reaction zone is independently controllable.

8. 发明专利

DE69801180D1 未知
公开(公告)号：DE69801180D1
公开(公告)日：2001-08-30
申请号：DE69801180
申请日：1998-04-15
申请人： CENTRAL GLASS CO LTD
发明人： KANAI MASATOMI , SAKAYA TAKASHI , WATANABE MINEO , GOTO YOSHIHIKO , NADANO RYO
IPC分类号： B01J27/08 , B01J27/125 , C07C45/63 , C07C45/82 , C07C45/83 , C07C49/16

9. 发明专利

GB2275266B Process of preparing 2-methyl-3-aminobenzotrifluoride 未知
公开(公告)号：GB2275266B
公开(公告)日：1996-03-20
申请号：GB9400447
申请日：1994-01-12
申请人： CENTRAL GLASS CO LTD
发明人： NISHIMIYA TAKAYUKI , KANAI MASATOMI , KAWAI TOSHIKAZU
IPC分类号： B01J23/44 , C07B61/00 , C07C17/00 , C07C17/12 , C07C17/23 , C07C25/13 , C07C205/12 , C07C209/36 , C07C211/52

10. 发明专利

DE4401124C2 未知
公开(公告)号：DE4401124C2
公开(公告)日：1995-08-24
申请号：DE4401124
申请日：1994-01-17
申请人： CENTRAL GLASS CO LTD
发明人： NISHIMIYA TAKAYUKI , KANAI MASATOMI , KAWAI TOSHIKAZU
IPC分类号： B01J23/44 , C07B61/00 , C07C17/00 , C07C17/12 , C07C17/23 , C07C25/13 , C07C205/12 , C07C209/36 , C07C211/52 , C07C201/08

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