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    • 3. 发明专利
    • Phosphor fine particle, method of manufacturing the same, phosphor thin film, and el device
    • 磷光体微粒,其制造方法,磷光薄膜和EL器件
    • JP2012251082A
    • 2012-12-20
    • JP2011125318
    • 2011-06-03
    • National Institute Of Advanced Industrial Science & Technology独立行政法人産業技術総合研究所
    • HAKUTA YUKIYATAKASHIMA HIROSHITO KIWAMUFURUYA TAKESHI
    • C09K11/67C09K11/00C09K11/08H05B33/10H05B33/14
    • PROBLEM TO BE SOLVED: To provide: a phosphor fine particle in which a primary particle size is at most 100 nm, there is no aggregation, and which is a single crystal, and has a perovskite type structure of high crystallinity; a method of manufacturing the phosphor fine particle in which the phosphor fine particle can be manufactured at a low temperature and for a short time comparatively, and in a water medium where an environmental load is extremely low; a phosphor thin film that uses the phosphor fine particle; and an EL device.SOLUTION: The phosphor fine particle is a phosphor fine particle that has a perovskite type structure shown by the following general formula (1), and is a single crystal, wherein the primary particle size is at most 100 nm, and there is not aggregation. ABO:Pr(1). In the formula (1), A denotes one of metallic elements of Ca, Ba, and Sr or a combination of metallic elements of at least two metallic elements in these metallic elements, and B denotes either Ti or a combination of Ti and Al.
    • 要解决的问题:提供:一次粒径为100nm以下,不存在凝集,单晶的具有高结晶度的钙钛矿型结构的荧光体微粒; 可以在低温和短时间内相对制造荧光体微粒的荧光体微粒的制造方法和环境负荷极低的水介质的制造方法; 使用荧光体微粒的荧光体薄膜; 和EL器件。 解决方案:所述荧光体微粒是具有以下通式(1)所示的钙钛矿型结构的荧光体微粒,其为一次粒径为100nm以下的单晶, 不聚合 ABO 3 :Pr 3 + (1)。 在式(1)中,A表示这些金属元素中的Ca,Ba和Sr的金属元素或至少两种金属元素的金属元素的组合中的一种,B表示Ti或Ti和Al的组合。 版权所有(C)2013,JPO&INPIT
    • 4. 发明专利
    • High-temperature high-pressure fluid mixing apparatus
    • 高温高压流体混合装置
    • JP2013000677A
    • 2013-01-07
    • JP2011135348
    • 2011-06-17
    • National Institute Of Advanced Industrial Science & Technology独立行政法人産業技術総合研究所
    • TO KIWAMUHAKUTA YUKIYAFURUYA TAKESHI
    • B01J19/24B01F3/08B01F5/00B01F15/02B01J3/02B01J19/00
    • PROBLEM TO BE SOLVED: To provide a high-temperature high-pressure fluid mixing apparatus which can cool a raw material solution to a point just before the mixing point of the high temperature high-pressure fluid and mix the high-temperature high pressure fluid from all the directions of a periphery to the raw material solution only by branching the high-temperature high-pressure fluid at most into two parts by making the apparatus a two-dimensional structure.SOLUTION: The apparatus includes: a first reaction solution channel which supplies a solution containing a substrate of a first reaction solution; a second reaction solution channel which supplies the high-temperature high-pressure fluid of a second reaction solution from the side direction to the first reaction solution channel; a liquid medium channel which is installed on the periphery of the first reaction solution channel, extends to the discharge end of the first reaction solution channel, and supplies a liquid medium; a mixing area which mixes the first reaction solution, the second reaction solution, and the liquid medium; and a mixed solution discharge channel for discharging the mixed solution.
    • 要解决的问题:提供一种高温高压流体混合装置,其能够将原料溶液冷却至高温高压流体的混合点前的一点,并将高温高压 通过使装置成为二维结构,仅通过将高温高压流体最多分支为两部分,从而从周边的所有方向到原料溶液的压力流体。 该装置包括:第一反应溶液通道,其提供含有第一反应溶液的底物的溶液; 第二反应溶液通道,其将第二反应溶液的高温高压流体从侧向供应到第一反应溶液通道; 安装在第一反应溶液通道的周围的液体介质通道延伸到第一反应溶液通道的排出端,并提供液体介质; 混合第一反应溶液,第二反应溶液和液体介质的混合区域; 以及用于排出混合溶液的混合溶液排出通道。 版权所有(C)2013,JPO&INPIT
    • 6. 发明专利
    • High temperature-high pressure micro mixing device
    • 高温高压微混合装置
    • JP2010075914A
    • 2010-04-08
    • JP2009186693
    • 2009-08-11
    • National Institute Of Advanced Industrial Science & TechnologyNihon Univ学校法人日本大学独立行政法人産業技術総合研究所
    • TO KIWAMUFURUYA TAKESHINICHIAKI TOSHIHIKOSATO TOSHIYUKI
    • B01J19/00B01F3/08B01F5/00B01F15/06B01J3/00B01J3/02
    • PROBLEM TO BE SOLVED: To provide a mixing device by which a room-temperature raw material solution supplied by using a circulation unit is mixed with the high temperature-high pressure fluid such as preheated water of high temperature-high pressure water supplied from another line so that the raw material solution can quickly be heated to the predetermined reaction temperature in a moment, in a continuous reaction crystallization process of a functional nanoparticle etc. by using a high temperature-high pressure fluid.
      SOLUTION: The micro mixing device is used for mixing a first reaction solution with a second reaction solution to quickly heat or cool the first or second reaction solution, form a reaction field of predetermined temperature in a moment and synthesize uniform fine particles. The micro mixing device has such a structure that the whole of a micro mixing part is arranged in a jacket in which a cooling or heating medium can be circulated and which has resistance to high pressure. The high temperature-high pressure micro mixing device is constituted so that the first reaction solution is mixed with the second reaction solution at a high speed to quickly heat or cool the first or second reaction solution, the heating of the first reaction solution in a flow passage before a mixing point is kept to a minimum and cores of crystallization of fine particles can be born homogeneously at the mixing point in the reaction field of a fine particle synthesis reaction system using the high temperature-high pressure fluid as a reacting medium.
      COPYRIGHT: (C)2010,JPO&INPIT
    • 要解决的问题:提供一种混合装置,通过使用循环装置供给的室温原料溶液与供给的高温高压水的预热水等高温高压流体混合 通过使用高温高压流体,在功能性纳米颗粒等的连续反应结晶过程中,可以将原料溶液在一段时间内快速加热至规定的反应温度。 解决方案:微混合装置用于将第一反应溶液与第二反应溶液混合以快速加热或冷却第一或第二反应溶液,在一定时间内形成预定温度的反应场并合成均匀的细颗粒。 微混合装置具有这样一种结构,即整个微混合部分布置在其中冷却或加热介质可以循环并且具有耐高压性的护套中。 构成高温高压微混合装置,使得第一反应溶液与第二反应溶液高速混合,以快速加热或冷却第一或第二反应溶液,将第一反应溶液以流动方式加热 在使用高温高压流体作为反应介质的细颗粒合成反应系统的反应场中的混合点,将混合点之前的通道保持最小并且细颗粒的结晶核心可以均匀地出现。 版权所有(C)2010,JPO&INPIT
    • 8. 发明专利
    • Heat-resistant, pressure-resistant, and corrosion-resistant temperature measurement micro device
    • 耐高温,耐压耐腐蚀温度测量微型器件
    • JP2013164377A
    • 2013-08-22
    • JP2012028276
    • 2012-02-13
    • National Institute Of Advanced Industrial & Technology独立行政法人産業技術総合研究所
    • TO KIWAMUHATADA KIYOTAKAFURUYA TAKESHI
    • G01K13/02B01J19/00
    • PROBLEM TO BE SOLVED: To provide a temperature measurement micro device to be used in a high-temperature site, a high-pressure site, and a high-temperature-pressure site.SOLUTION: A temperature measurement micro device comprises: a pipe provided at its end with a cone taper; a pipe adaptor in which the cone taper of the pipe is to be fitted, the pipe adaptor having a pressure-resistant sealing fitting face on which the cone taper of the pipe is to be fitted; a temperature sensor adaptor including a cylindrical recessed portion in which a temperature sensor is to be fitted and fixed; and a body including a recessed portion having a fitting face on which each of fitting faces provided at the back of the pipe fitting portion of the pipe adaptor and the temperature sensor insertion portion of the temperature sensor adaptor is to be fitted and a microchannel. The temperature measurement micro device is capable of accurately measuring a temperature of fluid flowing in the device at a position closer to the fluid without applying a pressure-resistant seal to the temperature sensor or an external force for fixing the temperature sensor.
    • 要解决的问题:提供一种用于高温部位,高压部位和高温部位的温度测量微型装置。解决方案:温度测量微型装置包括:管道, 其端部呈锥形锥形; 管道适配器,其中管子的锥形锥体将被装配,管道适配器具有耐压密封配合面,管子的锥形锥度将被安装在其上; 温度传感器适配器,包括:圆筒形凹部,其中安装和固定温度传感器; 以及具有凹部的主体,所述凹部具有嵌合面,所述嵌合面设置在所述管适配器的配管部的背面和所述温度传感器适配器的温度传感器插入部的后方配置有所述嵌合面和微通道。 温度测量微型装置能够在不对温度传感器施加耐压密封件或者用于固定温度传感器的外力的情况下,精确地测量在更靠近流体的位置处流过设备的流体温度。
    • 9. 发明专利
    • Heat-resistant, pressure-resistant, and corrosion-resistant electrochemical microcell
    • 耐高温,耐电压和耐腐蚀电化学微孔
    • JP2013164376A
    • 2013-08-22
    • JP2012028275
    • 2012-02-13
    • National Institute Of Advanced Industrial & Technology独立行政法人産業技術総合研究所
    • TO KIWAMUHATADA KIYOTAKAFURUYA TAKESHI
    • G01N27/28G01N27/416
    • PROBLEM TO BE SOLVED: To provide an electrochemical microcell to be used in a high-temperature site, a high-pressure site, and a high-temperature-pressure site.SOLUTION: A heat-resistant, pressure-resistant, and corrosion-resistant electrochemical microcell comprises: an electrode provided at its end with a cone taper; an electrode adaptor in which the electrode is to be fitted, the electrode adaptor having a pressure-resistant sealing fitting face on which the cone taper of the electrode is to be fitted; a first pipe provided at its end with a cone taper; a pipe adaptor in which the cone taper of the first pipe is to be fitted, the pipe adaptor having a sealing fitting face on which the cone taper of the first pipe is to be fitted; and a cell body including a recessed portion having a fitting face on which each of fitting faces provided at the back of the electrode fitting portion of the electrode adaptor and the pipe fitting portion of the pipe adaptor is to be fitted and a microchannel. The electrode includes a second pipe, an electrode fine wire provided in the second pipe, and a metal oxide insulation layer provided between the second pipe and the electrode fine wire. The microchannel has an inner diameter of 1.0 mm or less, and the electrode fine wire in the electrode has an outer diameter of 1.0 mm or less. The heat-resistant, pressure-resistant, and corrosion-resistant electrochemical microcell performs electrochemical measurement in a field of fluid that flows into the microchannel from the outside through the first pipe.
    • 要解决的问题:提供用于高温部位,高压部位和高温部位的电化学微细胞。解决方案:耐热,耐压,耐腐蚀 电化学微电池包括:在其端部设置有锥形锥形的电极; 电极适配器,其中电极将被装配,电极适配器具有耐压密封配合面,电极的锥形锥形将被安装在其上; 在其端部设置有锥形锥形的第一管; 管接头,其中第一管的锥形锥体将被装配,管接头具有密封配合面,第一管的锥形锥体将安装在其上; 以及具有凹部的电池体,所述凹部具有嵌合面,所述嵌合面设置在所述电极适配器的电极配合部的后方的配合面和所述管接头的配管部与所述微通道配合。 电极包括第二管,设置在第二管中的电极细线,以及设置在第二管和电极细线之间的金属氧化物绝缘层。 微通道的内径为1.0mm以下,电极中的电极细线的外径为1.0mm以下。 耐热,耐压和耐腐蚀的电化学微电池在从外部通过第一管流入微通道的流体领域中进行电化学测量。