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1. 发明申请

US20130256742A1 Siloxane-Compositions Including Metal-Oxide Nanoparticles Suitable For Forming Encapsulants 审中-公开
标题翻译：包含适合形成密封剂的金属氧化物纳米颗粒的硅氧烷组合物
公开(公告)号：US20130256742A1
公开(公告)日：2013-10-03
申请号：US13991840
申请日：2011-12-06
申请人： Brian R. Harkness , Ann W. Norris , Shellene K. Thurston , Masaaki Amako , Maki Itoh , Michitaka Suto
发明人： Brian R. Harkness , Ann W. Norris , Shellene K. Thurston , Masaaki Amako , Maki Itoh , Michitaka Suto
IPC分类号： H01L33/56
CPC分类号： H01L33/56 , C08G77/20 , C08K3/22 , C08L83/04 , C09D7/61 , C09D7/67 , H01L23/3171 , H01L2924/0002 , H01L2924/00
摘要： A composition includes an organopolysiloxane component (A) having at least one aryl group and having an average of at least two alkenyl groups per molecule. The composition further includes an organohydrogensiloxane component (B) having at least one of an alkyl group and an aryl group and an average of at least two silicon-bonded hydrogen atoms per molecule. Components (A) and (B) each independently have a number average molecular weight less than or equal to 1500 (g/mole). The composition yet further includes a catalytic amount of a hydrosilylation catalyst component (C), and metal-oxide nanoparticles (D) other than titanium dioxide (TiO2) nanoparticles. The composition has a molar ratio of alkyl groups to aryl groups ranging from 1:0.25 to 1:3.0. A product of the present invention is the reaction product of the composition, which may be used to make a light emitting diode.
摘要翻译：组合物包括每分子具有至少一个芳基并且平均具有至少两个烯基的有机聚硅氧烷组分（A）。该组合物还包括具有烷基和芳基中的至少一个并且每个分子具有至少两个与硅键合的氢原子平均的有机氢硅氧烷组分（B）。组分（A）和（B）各自独立地具有小于或等于1500（g / mol）的数均分子量。该组合物还包括催化量的氢化硅烷化催化剂组分（C）和除二氧化钛（TiO 2）纳米颗粒以外的金属氧化物纳米颗粒（D）。该组合物的烷基与芳基的摩尔比范围为1:0.25至1:3.0。本发明的产品是可用于制造发光二极管的组合物的反应产物。

2. 发明申请

US20130253161A1 Methods Of Modifying Metal-Oxide Nanoparticles 审中-公开
标题翻译：改性金属氧化物纳米颗粒的方法
公开(公告)号：US20130253161A1
公开(公告)日：2013-09-26
申请号：US13991851
申请日：2011-12-06
申请人： Masaaki Amako , Maki Itoh , Michitaka Suto
发明人： Masaaki Amako , Maki Itoh , Michitaka Suto
IPC分类号： C09C1/36 , C09C1/00
CPC分类号： C09C1/3676 , B82Y30/00 , C01P2002/82 , C01P2002/86 , C01P2004/51 , C01P2004/64 , C09C1/00 , C09C1/3684 , C09C3/12 , H01L23/296 , H01L2924/0002 , H01L2924/00
摘要： Methods employing acidic and basic catalysts are disclosed, and generally entail hydrolysis and condensation reactions of silicon based components. The methods are useful for forming siloxane-modified metal-oxide nanoparticles, such as modified ZrO2 nanoparticles. The siloxane-modified metal-oxide nanoparticles, and products including the siloxane-modified metal-oxide nanoparticles, can be used to form various products, such as lenses or encapsulants for making various devices, such as, but not limited to, light emitting diodes (LEDs).
摘要翻译：公开了使用酸性和碱性催化剂的方法，通常需要硅基组分的水解和缩合反应。该方法可用于形成硅氧烷改性的金属氧化物纳米颗粒，例如改性的ZrO 2纳米颗粒。硅氧烷改性的金属氧化物纳米颗粒和包含硅氧烷改性的金属氧化物纳米颗粒的产品可用于形成各种产品，例如用于制造各种装置的透镜或密封剂，例如但不限于发光二极管（LED）。

3. 发明授权

US5907019A Polymer-compatible polymethylsilsesquioxane 失效
标题翻译：聚合物相容的聚甲基硅倍半氧烷
公开(公告)号：US5907019A
公开(公告)日：1999-05-25
申请号：US977701
申请日：1997-11-25
申请人： Maki Itoh , Akihito Sakakibara-Saitoh , Michitaka Suto
发明人： Maki Itoh , Akihito Sakakibara-Saitoh , Michitaka Suto
IPC分类号： C08L83/06 , C08F283/12 , C08G77/04 , C08G77/06 , C08G77/16 , C08G77/38
CPC分类号： C08G77/06 , C08F283/12 , C08G77/04
摘要： A silylated polymethylsilsesquioxane, that contains no more than 0.12 residual silanol per Si atom and has a predetermined number average molecular weight from 380 to 2,000 is obtained by silylating the silanol in a starting polymethylsilsesquioxane with the formula(CH.sub.3 SiO.sub.3/2).sub.n (CH.sub.3 Si(OH)O.sub.2/2).sub.mwherein m and n are positive numbers that provide the specified molecular weight and 0.034/(M.times.10.sup.-3).ltoreq.m/(m+n).ltoreq.0.152/(M.times.10.sup.-3)+0.10. The silylated polymethylsilsequioxanes of the present invention exhibit compatibility with silicone polymers, e.g., polydimethylsiloxanes. As a consequence, the silylated polymethylsilsesquioxanes of the invention can be used in a wide range of applications as, for example, a reinforcing filler for rubbers.
摘要翻译：通过使甲硅烷基化的起始聚甲基硅倍半氧烷中的硅烷醇与式（CH3SiO3 / 2）n（CH3Si（OH））进行甲硅烷基化，得到甲硅烷基化的聚甲基倍半硅氧烷，其每Si原子含有不超过0.12的残留硅烷醇，并且具有380至2,000的预定数均分子量。）O 2/2）m，其中m和n是提供指定分子量的正数和0.034 /（M×10 -3）m /（m + n）≤0.22/（M×10 -3）+0.10的正数。本发明的甲硅烷基化聚甲基硅二恶烷表现出与硅氧烷聚合物例如聚二甲基硅氧烷的相容性。因此，本发明的甲硅烷基化聚甲基倍半硅氧烷可用于广泛的应用中，例如用于橡胶的增强填料。

4. 发明授权

US5981670A Alkenyl-functional silylated polymethysilses quioxane and method of preparing the same 失效
标题翻译：烯基官能甲硅烷基化聚甲基硅氧烷二恶烷及其制备方法
公开(公告)号：US5981670A
公开(公告)日：1999-11-09
申请号：US028257
申请日：1998-02-23
申请人： Maki Itoh , Akihito Sakakibara-Saitoh , Michitaka Suto
发明人： Maki Itoh , Akihito Sakakibara-Saitoh , Michitaka Suto
IPC分类号： C08L83/06 , C08G77/06 , C08G77/14 , C08G77/20 , C08L83/05 , C08L83/07 , C08F283/12
CPC分类号： C08G77/20
摘要： An alkenyl-functional silylated polymethylsilsesquioxane that contains no more than 0.12 residual silanol per Si atom and is obtained by silylating the silanol in starting polymethylsilsesquioxane. The starting polymethylsilsesquioxane has a predetermined number average molecular weight, Mn, from 380 to 2,000 and is represented by the general formula(CH.sub.3 SiO.sub.3/2).sub.n (CH.sub.3 Si(OH)O.sub.2/2).sub.mwherein m and n are positive numbers that provide the predetermined Mn, with the proviso that the value of m/(m+n) is less than or equal to 0.152/(Mn.times.10.sup.-3)+0.10 and greater than or equal to 0.034/(Mn.times.10.sup.-3). The alkenyl-functional silylated polymethylsilsesquioxane has the formula(CH.sub.3 SiO.sub.3/2).sub.n (CH.sub.3 Si(OH)O.sub.2/2).sub.m-k (CH.sub.3 Si(OSiR.sup.1 R.sup.2 R.sup.3)O.sub.2/2).sub.kwherein k is a positive number smaller than A, (m-k/(m+n) is less than or equal to 0.12, and R.sup.1, R.sup.2 and R.sup.3 are each selected from substituted and unsubstituted monovalent hydrocarbon groups with the proviso that at least 1 of said R.sup.1, R.sup.2, and R.sup.3 is a group that contains a crosslinkable carbon--carbon double bond.
摘要翻译：烯烃官能的甲硅烷基化聚甲基倍半硅氧烷，其每Si原子含有不超过0.12的残留硅烷醇，并且通过在起始的聚甲基倍半硅氧烷中硅烷化得到。起始的聚甲基倍半硅氧烷具有预定的数均分子量Mn，为380-2,000，并由通式（CH 3 SiO 3/2）n（CH 3 Si（OH）O 2/2）m表示，其中m和n是提供预定的Mn，条件是m /（m + n）的值小于或等于0.152 /（Mn×10 -3）+0.10且大于或等于0.034 /（Mn×10 -3）。烯基官能的甲硅烷基化聚甲基倍半硅氧烷具有式（CH 3 SiO 3/2）n（CH 3 Si（OH）O 2/2）mk（CH 3 Si（OSiR 1 R 2 R 3）O 2/2）k其中k是小于A的正数，（mk /（m + n）小于或等于0.12，并且R 1，R 2和R 3各自选自取代和未取代的一价烃基，条件是所述R 1，R 2和R 3中的至少1个是含有可交联碳碳双键。

5. 发明申请

US20110177342A1 Cured Organopolysiloxane Resin Film Having Gas Barrier Properties and Method Of Producing The Same 审中-公开
标题翻译：具有阻气性的固化有机聚硅氧烷树脂膜及其制造方法
公开(公告)号：US20110177342A1
公开(公告)日：2011-07-21
申请号：US13003316
申请日：2009-06-26
申请人： Maki Itoh , Michitaka Suto , Nobuo Kushibiki , Hidekatsu Hatanaka , Katsuya Eguchi , Dimitris Elias Katsoulis
发明人： Maki Itoh , Michitaka Suto , Nobuo Kushibiki , Hidekatsu Hatanaka , Katsuya Eguchi , Dimitris Elias Katsoulis
IPC分类号： B32B27/08 , B32B27/38 , B32B9/00 , C23C16/34 , C23C16/40 , C23C14/06 , C23C14/22 , B05D5/00 , B05D3/00
CPC分类号： C08J7/045 , C08J2383/04 , C08L83/04 , Y10T428/31515 , Y10T428/31663 , C08L83/00
摘要： A cured organopolysiloxane resin film having gas barrier properties in which a layer of cured organopolysiloxane that contains an organic functional group, an organic group produced by the polymerization of polymerizable organic functional groups, or the hydrosilyl group or silanol group, is formed on a visible region-transparent film comprising cured organopolysiloxane resin yielded by hydrosilylation reaction-mediated crosslinking, and in which a silicon oxynitride layer, silicon nitride layer, or silicon oxide layer is formed on the aforementioned layer of cured organopolysiloxane. Also, a method of producing this cured organopolysiloxane resin film having gas barrier properties.
摘要翻译：在具有气体阻隔性的固化有机聚硅氧烷树脂膜上形成含有有机官能团的固化有机聚硅氧烷，通过聚合性有机官能团聚合生成的有机基团或氢化硅烷基或硅烷醇基的可见区域 - 透明的膜包括通过氢化硅烷化反应介导的交联产生的固化的有机聚硅氧烷树脂，并且其中在上述固化的有机聚硅氧烷层上形成氧氮化硅层，氮化硅层或氧化硅层。另外，制造具有阻气性的固化的有机聚硅氧烷树脂膜的方法。

6. 发明授权

US07960030B2 Free films made of cured organopolysiloxane resins, process for production thereof, and laminated films 有权
标题翻译：由固化的有机聚硅氧烷树脂制成的游离膜，其制造方法和层压膜
公开(公告)号：US07960030B2
公开(公告)日：2011-06-14
申请号：US11569104
申请日：2005-05-13
申请人： Maki Itoh , Michitaka Suto , Nobuo Kushibiki , Katsuya Eguchi
发明人： Maki Itoh , Michitaka Suto , Nobuo Kushibiki , Katsuya Eguchi
IPC分类号： B32B15/08 , B29C71/00 , C08F283/12 , C08J5/18
CPC分类号： C08J5/18 , C08G77/12 , C08G77/20 , C08G77/70 , C08J2383/04 , C08K3/22 , C08L83/04 , Y10T156/1158 , Y10T428/31663 , C08L83/00
摘要： A free-standing film comprising a cured organopolysiloxane resin obtained by conducting a cross-linking reaction between (A) an organopolysiloxane resin represented by the following average siloxane unit formula: [R1aR23-aSiO1/2]v[R3SiO3/2]w (1) or [R1aR23-aSiO1/2]x[R3SiO3/2]y[SiO4/2]z (2) (where R1 designates univalent hydrocarbon groups of one or more than one type selected from alkyl groups having 1 to 4 carbon atoms and univalent aromatic hydrocarbon groups having 6 to 8 carbon atoms; R2 designate alkenyl groups having 2 to 6 carbon atoms; R3 designates alkyl groups with 1 to 4 carbon atoms or univalent aromatic hydrocarbon groups having 6 to 8 carbon atoms; at least 50 mole % of R3 groups being phenyl groups; “a” is 0, 1, or 2; 0.8≦w
摘要翻译：通过在（A）由以下平均硅氧烷单元式：[R a R 23-a SiO 1/2/2] v [R 3 SiO 3/2] w（1）表示的有机聚硅氧烷树脂之间进行交联反应获得的固化的有机聚硅氧烷树脂，）或[R1aR23-aSiO1 / 2] x [R3SiO3 / 2] y [SiO4 / 2] z（2）（其中R1表示一个或多于一种选自具有1至4个碳原子的烷基的一价烃基，具有6至8个碳原子的单价芳族烃基; R 2表示具有2至6个碳原子的烯基; R 3表示具有1至4个碳原子的烷基或具有6至8个碳原子的单价芳族烃基;至少50摩尔％ R3为苯基;“a”为0,1或2;0.8≤n1E; w <1.0且v + w = 1; 0

7. 发明申请

US20090084428A1 Copper Indium Diselenide-Based Photovoltaic Device And Method Of Preparing The Same 审中-公开
标题翻译：基于二硒化铜的光伏器件及其制备方法
公开(公告)号：US20090084428A1
公开(公告)日：2009-04-02
申请号：US12297358
申请日：2007-04-18
申请人： Thomas Duncan Barnard , Yukinari Harimoto , Hidekatsu Hatanaka , Maki Itoh , Dimitris Elias Katsoulis , Michitaka Suto , Bizhong Zhu , Lawrence M. Woods , Joseph H. Armstrong , Rosine M. Ribelin
发明人： Thomas Duncan Barnard , Yukinari Harimoto , Hidekatsu Hatanaka , Maki Itoh , Dimitris Elias Katsoulis , Michitaka Suto , Bizhong Zhu , Lawrence M. Woods , Joseph H. Armstrong , Rosine M. Ribelin
IPC分类号： H01L31/042
CPC分类号： H01L31/0322 , C08G77/12 , C08G77/16 , C08G77/20 , C08L83/04 , H01L31/072 , H01L31/0749 , Y02E10/541 , C08L83/00
摘要： A copper indium diselenide (CIS)-based photovoltaic device includes a CIS-based solar absorber layer including copper, indium, and selenium. The CIS-based photovoltaic device further includes a substrate including a silicone layer formed from a silicone composition and a metal foil layer. The substrate, due to the presence of the silicone layer and the metal foil layer, is both flexible and sufficiently able to withstand annealing temperatures in excess of 500° C. to obtain maximum efficiency of the device.
摘要翻译：基于铜铟锡（CIS）的光伏器件包括包含铜，铟和硒的基于CIS的太阳能吸收层。所述基于CIS的光电装置还包括由硅氧烷组合物和金属箔层形成的硅氧烷层的基板。由于存在硅树脂层和金属箔层，衬底既柔软又足以承受超过500℃的退火温度，以获得器件的最大效率。

8. 发明申请

US20080318067A1 Free Films Made Of Cured Organopolysiloxane Resins, Process For Production Thereof, And Laminated Films 有权
标题翻译：固化有机聚硅氧烷树脂，其生产工艺和层压薄膜制成的免费薄膜
公开(公告)号：US20080318067A1
公开(公告)日：2008-12-25
申请号：US11569104
申请日：2005-05-13
申请人： Maki Itoh , Michitaka Suto , Nobuo Kushibiki , Katsuya Eguchi
发明人： Maki Itoh , Michitaka Suto , Nobuo Kushibiki , Katsuya Eguchi
IPC分类号： B32B9/00 , C08G77/38 , B32B38/10
CPC分类号： C08J5/18 , C08G77/12 , C08G77/20 , C08G77/70 , C08J2383/04 , C08K3/22 , C08L83/04 , Y10T156/1158 , Y10T428/31663 , C08L83/00
摘要： A free-standing film comprising a cured organopolysiloxane resin obtained by conducting a cross-linking reaction between (A) an organopolysiloxane resin represented by the following average siloxane unit formula: [R1aR23-aSiO1/2]v[R3SiO3/2]w (1) or [R1aR23-aSiO1/2]x[R3SiO3/2]y[SiO4/2]z (2) (where R1 designates univalent hydrocarbon groups of one or more than one type selected from alkyl groups having 1 to 4 carbon atoms and univalent aromatic hydrocarbon groups having 6 to 8 carbon atoms; R2 designate alkenyl groups having 2 to 6 carbon atoms; R3 designates alkyl groups with 1 to 4 carbon atoms or univalent aromatic hydrocarbon groups having 6 to 8 carbon atoms; at least 50 mole % of R3 groups being phenyl groups; “a” is 0, 1, or 2; 0.8≦w
摘要翻译：通过在（A）由以下平均硅氧烷单元：[R1aR23-aSiO1 / 2] v [R3SiO3 / 2] w（1）表示的有机聚硅氧烷树脂之间进行交联反应获得的固化的有机聚硅氧烷树脂）或[R1aR23-aSiO1 / 2] x [R3SiO3 / 2] y [SiO4 / 2] z（2）（其中R1表示一个或多于一种选自具有1至4个碳原子的烷基的一价烃基，具有6至8个碳原子的一价芳族烃基; R 2表示具有2至6个碳原子的烯基; R 3表示具有1至4个碳原子的烷基或具有6至8个碳原子的单价芳族烃基;至少50摩尔％ R3为苯基;“a”为0,1或2; 0.8 <= w <1.0且v + w = 1; 0

9. 发明授权

US08207442B2 Reinforcing structures for thin-film photovoltaic device substrates, and associated methods 有权
标题翻译：薄膜光伏器件基板的增强结构及相关方法
公开(公告)号：US08207442B2
公开(公告)日：2012-06-26
申请号：US11737119
申请日：2007-04-18
申请人： Lawrence M. Woods , Joseph H. Armstrong , Rosine M. Ribelin , Thomas Duncan Barnard , Yukinari Harimoto , Hidekatsu Hatanaka , Maki Itoh , Dimitris Elias Katsoulis , Michitaka Suto , Bizhong Zhu , Nicole R. Anderson , Herschel Henry Reese
发明人： Lawrence M. Woods , Joseph H. Armstrong , Rosine M. Ribelin , Thomas Duncan Barnard , Yukinari Harimoto , Hidekatsu Hatanaka , Maki Itoh , Dimitris Elias Katsoulis , Michitaka Suto , Bizhong Zhu , Nicole R. Anderson , Herschel Henry Reese
IPC分类号： H01L31/00
CPC分类号： H01L31/0392 , H01L31/03921 , H01L31/03928 , H01L31/046 , H01L31/0463 , H01L31/0749 , Y02E10/541
摘要： In an embodiment, one reinforced substrate for use in a photovoltaic device includes a polymer base material and a reinforcing structure bonded with the base material. The reinforced substrate presents a surface in a condition that is made-ready for deposition of thin film layers of the photovoltaic device. A thin film photovoltaic device includes the reinforced substrate, a back contact layer formed on the surface of the reinforced substrate, and a solar absorber layer formed on the back contact layer. A plurality of thin film photovoltaic devices may be formed on a common reinforced substrate. A process of producing a reinforced substrate includes combining a fluid base material and a fiber reinforcing structure to form an impregnated fiber reinforcement. The impregnated fiber reinforcement is cured to form the reinforced substrate, and the reinforced substrate is annealed.
摘要翻译：在一个实施例中，用于光伏器件的一个增强衬底包括聚合物基材和与基材结合的增强结构。增强的基底呈现出一个表面，该表面被制备用于沉积光伏器件的薄膜层。薄膜光伏器件包括增强衬底，形成在增强衬底的表面上的背接触层和形成在后接触层上的太阳能吸收层。多个薄膜光伏器件可以形成在共同的增强衬底上。制造增强基材的方法包括组合流体基材和纤维增强结构以形成浸渍的纤维增强材料。浸渍的纤维增强材料被固化以形成增强的基底，并且加强的基底被退火。

10. 发明申请

US20130012087A1 Cured Organopolysiloxane Resin Film Having Gas Barrier Properties and Method Of Producing The Same 审中-公开
标题翻译：具有阻气性的固化有机聚硅氧烷树脂膜及其制造方法
公开(公告)号：US20130012087A1
公开(公告)日：2013-01-10
申请号：US13520359
申请日：2011-01-07
申请人： Maki Itoh , Michitaka Suto , Bizhong Zhu , Dimitris Elias Katsoulis , Ludmil Zambov
发明人： Maki Itoh , Michitaka Suto , Bizhong Zhu , Dimitris Elias Katsoulis , Ludmil Zambov
IPC分类号： B32B27/04 , C23C14/06 , C23C16/40 , B05D3/06 , C23C16/34 , C23C16/30
CPC分类号： C09D183/04 , C08J5/24 , C08J2383/04 , Y10T428/31663 , Y10T442/2098
摘要： A cured organopolysiloxane resin film having gas barrier properties comprising a fiber-reinforced film made of a hydrosilylation-cured organopolysiloxane resin and having a transparent inorganic layer selected from silicon oxynitride layer, silicon nitride layer, and silicon oxide layer formed on the fiber-reinforced film wherein a layer of cured organopolysiloxane that contains an organic functional group, silanol group, hydrosilyl group, or an organic group produced by the polymerization of polymerizable organic functional groups is interposed between said fiber-reinforced film and inorganic layer. Also, a method of producing this cured organopolysiloxane resin film having gas barrier properties.
摘要翻译：具有阻气性的固化的有机聚硅氧烷树脂膜包含由氢化硅烷化固化的有机聚硅氧烷树脂制成的纤维增强膜，并且具有选自形成在纤维增强膜上的氧氮化硅层，氮化硅层和氧化硅层的透明无机层其中含有有机官能团，硅烷醇基，氢化硅烷基或通过可聚合有机官能团的聚合制备的有机基团的固化的有机聚硅氧烷层被插入在所述纤维增强膜和无机层之间。另外，制造具有阻气性的固化有机聚硅氧烷树脂膜的方法。

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