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1. 发明申请

US20110124908A1 PROCESS FOR PREPARING ISOCYANATES 有权
标题翻译：制备异氰酸酯的方法
公开(公告)号：US20110124908A1
公开(公告)日：2011-05-26
申请号：US12675095
申请日：2008-08-27
申请人： Bernd Rumpf , Michael Bock , Martin Fiene , Eckhard Stroefer
发明人： Bernd Rumpf , Michael Bock , Martin Fiene , Eckhard Stroefer
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C263/20 , C07C265/14
摘要： The invention provides a process for preparing polyisocyanates, comprising the steps of a) reacting amines with phosgene, b) removing hydrogen chloride, excess phosgene and, if appropriate, the solvent from the reaction mixture, c) separating the liquid mixture from step b) into a liquid phase and a gaseous phase, d) working up the gaseous phase from step c) to give the polyisocyanate.
摘要翻译：本发明提供了一种制备多异氰酸酯的方法，包括以下步骤：a）使胺与光气反应，b）从反应混合物中除去氯化氢，过量的光气和（如果合适的话）溶剂; c）将液体混合物从步骤b）进入液相和气相，d）处理来自步骤c）的气相，得到多异氰酸酯。

2. 发明授权

US08273915B2 Process for preparing isocyanates 有权
标题翻译：异氰酸酯的制备方法
公开(公告)号：US08273915B2
公开(公告)日：2012-09-25
申请号：US12675095
申请日：2008-08-27
申请人： Bernd Rumpf , Michael Bock , Martin Fiene , Eckhard Stroefer
发明人： Bernd Rumpf , Michael Bock , Martin Fiene , Eckhard Stroefer
IPC分类号： C07C263/00
CPC分类号： C07C263/10 , C07C263/20 , C07C265/14
摘要： The invention provides a process for preparing polyisocyanates, comprising the steps of a) reacting amines with phosgene, b) removing hydrogen chloride, excess phosgene and, if appropriate, the solvent from the reaction mixture, c) separating the liquid mixture from step b) into a liquid phase and a gaseous phase, d) working up the gaseous phase from step c) to give the polyisocyanate.
摘要翻译：本发明提供了一种制备多异氰酸酯的方法，包括以下步骤：a）使胺与光气反应，b）从反应混合物中除去氯化氢，过量的光气和（如果合适的话）溶剂; c）将液体混合物从步骤b）进入液相和气相，d）处理来自步骤c）的气相，得到多异氰酸酯。

3. 发明授权

US08835673B2 Process for preparing isocyanates 有权
标题翻译：异氰酸酯的制备方法
公开(公告)号：US08835673B2
公开(公告)日：2014-09-16
申请号：US13513595
申请日：2010-12-03
申请人： Torsten Mattke , Eckhard Stroefer , Julia Leschinski , Radwan Abdallah , Axel Franzke , Michael Bock
发明人： Torsten Mattke , Eckhard Stroefer , Julia Leschinski , Radwan Abdallah , Axel Franzke , Michael Bock
IPC分类号： C07C263/04
CPC分类号： C07C263/04 , C07C265/12 , C07C265/14
摘要： Process for preparing aromatic isocyanates by reacting the corresponding formamides with an oxygen-comprising gas over noble metal catalysts at temperatures of from 300 to 600° C. and a contact time of from 1 to 1000 ms, wherein: a. the formamide is vaporized before entering the reaction zone, b. the reaction mixture obtained is quenched with an alcohol-comprising quenching liquid and c. the urethane formed is dissociated into isocyanate and alcohol.
摘要翻译：通过使贵金属催化剂上的相应的甲酰胺与含氧气体在300-600℃的温度和1至1000ms的接触时间下反应来制备芳族异氰酸酯的方法，其中：a。甲酰胺在进入反应区之前蒸发，b。得到的反应混合物用含醇的淬火液骤冷，c。所形成的聚氨酯被分解成异氰酸酯和醇。

4. 发明授权

US08759569B2 Process for the production of isocyanates, preferably diisocyanates and polyisocyanates with solvent recirculation 有权
标题翻译：制备异氰酸酯，优选二异氰酸酯和多异氰酸酯与溶剂再循环的方法
公开(公告)号：US08759569B2
公开(公告)日：2014-06-24
申请号：US13380680
申请日：2010-06-16
申请人： Heiner Schelling , Ulrich Penzel , Eckhard Stroefer , Matthias Eiermann , Jon S. Speier , Kai Thiele , Michael Bock
发明人： Heiner Schelling , Ulrich Penzel , Eckhard Stroefer , Matthias Eiermann , Jon S. Speier , Kai Thiele , Michael Bock
IPC分类号： C07C263/00
CPC分类号： C07C263/10 , C07C265/14
摘要： The present invention relates to a process for the production of isocyanates, preferably diisocyanates and polyisocyanates of the diphenylmethane series (MDI), by reacting an amine with phosgene in the liquid phase or in the gas phase to form the corresponding isocyanates, subsequent removal of the solvent in at least two steps to obtain at least two solvent streams, individual treatment of the at least two solvent streams, and recirculation of at least a portion of the solvent streams.
摘要翻译：本发明涉及通过使胺与气相或气相中的光气反应以形成相应的异氰酸酯来制备二异氰酸酯，优选二苯甲烷系列（MDI）的二异氰酸酯和多异氰酸酯的方法，随后除去溶剂至少两个步骤以获得至少两种溶剂流，对至少两种溶剂流进行单独处理，以及再循环至少一部分溶剂流。

5. 发明申请

US20120253072A1 PROCESS FOR THE PREPARATION OF AROMATIC FORMAMIDES 失效
标题翻译：制备芳香霉素的方法
公开(公告)号：US20120253072A1
公开(公告)日：2012-10-04
申请号：US13513752
申请日：2010-12-01
申请人： Axel Franzke , Torsten Mattke , Julia Leschinski , Radwan Abdallah , Michael Bock , Robert Baumann , Eckhard Stroefer
发明人： Axel Franzke , Torsten Mattke , Julia Leschinski , Radwan Abdallah , Michael Bock , Robert Baumann , Eckhard Stroefer
IPC分类号： C07C231/02
CPC分类号： C07C231/02 , C07C233/03 , C07C233/43
摘要： The invention relates to a process for the preparation of formamides by reacting aromatic amines with a formic acid ester in the presence of a catalyst, wherein the catalyst is a phosphorus-containing acid or a Lewis-acidic metal salt.
摘要翻译：本发明涉及一种在催化剂存在下使芳族胺与甲酸酯反应制备甲酰胺的方法，其中催化剂是含磷酸或路易斯酸性金属盐。

6. 发明申请

US20120245377A1 PROCESS FOR PREPARING ISOCYANATES BY THERMALLY CLEAVING CARBAMATES 有权
标题翻译：通过热清除碳酸钙制备异氰酸酯的方法
公开(公告)号：US20120245377A1
公开(公告)日：2012-09-27
申请号：US13513460
申请日：2010-11-30
申请人： Michael Bock , Eckhard Stroefer , Robert Baumann , Axel Franzke , Joachim Pfeffinger
发明人： Michael Bock , Eckhard Stroefer , Robert Baumann , Axel Franzke , Joachim Pfeffinger
IPC分类号： C07C263/04
CPC分类号： C07C263/04 , C07C265/14
摘要： A process is proposed for preparing isocyanates by thermally cleaving carbamates to obtain a carbamate cleavage gas comprising the corresponding isocyanate and the corresponding alcohol, which comprises quenching the carbamate cleavage gas in the presence of an ether which functions as an inhibitor for the reverse reaction of the isocyanate with the alcohol.
摘要翻译：提出了通过热裂解氨基甲酸酯制备异氰酸酯以获得包含相应的异氰酸酯和相应的醇的氨基甲酸酯裂解气体的方法，该方法包括在醚的存在下猝灭氨基甲酸酯裂解气体，该醚用作反应的反应的抑制剂异氰酸酯与醇。

7. 发明申请

US20120101299A1 PROCESS FOR THE PRODUCTION OF ISOCYANATES, PREFERABLY DIISOCYANATES AND POLYISOCYANATES WITH SOLVENT RECIRCULATION 有权
标题翻译：生产异氰酸酯，优选二异氰酸酯和溶剂回收的聚异氰酸酯的方法
公开(公告)号：US20120101299A1
公开(公告)日：2012-04-26
申请号：US13380680
申请日：2010-06-16
申请人： Heiner Schelling , Ulrich Penzel , Eckhard Stroefer , Matthias Eiermann , Jon S. Speier , Kai Thiele , Michael Bock
发明人： Heiner Schelling , Ulrich Penzel , Eckhard Stroefer , Matthias Eiermann , Jon S. Speier , Kai Thiele , Michael Bock
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： The present invention relates to a process for the production of isocyanates, preferably diisocyanates and polyisocyanates of the diphenylmethane series (MDI), by reacting an amine with phosgene in the liquid phase or in the gas phase to form the corresponding isocyanates, subsequent removal of the solvent in at least two steps to obtain at least two solvent streams, individual treatment of the at least two solvent streams, and re-circulation of at least a portion of the solvent streams.
摘要翻译：本发明涉及通过使胺与气相或气相中的光气反应以形成相应的异氰酸酯来制备二异氰酸酯，优选二苯甲烷系列（MDI）的二异氰酸酯和多异氰酸酯的方法，随后除去溶剂至少两个步骤以获得至少两种溶剂流，对至少两种溶剂流进行单独处理，以及再循环至少一部分溶剂流。

8. 发明授权

US08822718B2 Process for preparing isocyanates by thermally cleaving carbamates 有权
标题翻译：通过热裂解氨基甲酸酯制备异氰酸酯的方法
公开(公告)号：US08822718B2
公开(公告)日：2014-09-02
申请号：US13513460
申请日：2010-11-30
申请人： Michael Bock , Eckhard Stroefer , Robert Baumann , Axel Franzke , Joachim Pfeffinger
发明人： Michael Bock , Eckhard Stroefer , Robert Baumann , Axel Franzke , Joachim Pfeffinger
IPC分类号： C07C263/04
CPC分类号： C07C263/04 , C07C265/14
摘要： A process is proposed for preparing isocyanates by thermally cleaving carbamates to obtain a carbamate cleavage gas comprising the corresponding isocyanate and the corresponding alcohol, which comprises quenching the carbamate cleavage gas in the presence of an ether which functions as an inhibitor for the reverse reaction of the isocyanate with the alcohol.
摘要翻译：提出了通过热裂解氨基甲酸酯制备异氰酸酯以获得包含相应的异氰酸酯和相应的醇的氨基甲酸酯裂解气体的方法，该方法包括在醚的存在下猝灭氨基甲酸酯裂解气体，该醚用作反应的反应的抑制剂异氰酸酯与醇。

9. 发明授权

US08440856B2 Method for treating residues from the production of isocyanates 失效
标题翻译：处理异氰酸酯生产残留物的方法
公开(公告)号：US08440856B2
公开(公告)日：2013-05-14
申请号：US12936080
申请日：2009-04-09
申请人： Michael Bock , Martin Sesing , Eckhard Stroefer
发明人： Michael Bock , Martin Sesing , Eckhard Stroefer
IPC分类号： C07C293/10 , C07C209/84 , C07C209/86 , C07C265/14 , C07C211/50
CPC分类号： C07C263/10 , C07C209/62 , C07C209/86 , C07C265/14 , C07C211/51
摘要： This invention relates to a process for working up residues from production of isocyanates. This process involves hydrolyzing residues from production of at least one isocyanate with water to form a hydrolysis product, and processing the hydrolysis product within an extruder or a kneader having a heat transfer surface, to form a mixed product containing at least one amine and water. The amine and the water are separated from the mixed product to form an amine/water mixture, which is then separated to obtain the water and the amine. The process may also involve separating all or part of the water from the hydrolysis, or separating part of the amine from the hydrolysis, prior to the processing of the hydrolysis product.
摘要翻译：本发明涉及一种处理异氰酸酯生产残留物的方法。该方法包括用水生产至少一种异氰酸酯的残余物水解以形成水解产物，并在挤出机或具有传热表面的捏合机中加工水解产物，以形成含有至少一种胺和水的混合产物。将胺和水从混合产物中分离以形成胺/水混合物，然后将其分离，得到水和胺。该方法还可以包括在加工水解产物之前将全部或部分水从水解中分离出来，或者将胺的一部分与水解分离。

10. 发明授权

US09000213B2 Process for coproducing di- and/or polyisocyanates and glycols 有权
标题翻译：共聚产生二 - 和/或多异氰酸酯和二醇的方法
公开(公告)号：US09000213B2
公开(公告)日：2015-04-07
申请号：US13502763
申请日：2010-10-27
申请人： Michael Bock , Robert Baumann , Axel Franzke , Eckhard Stroefer , Gerhard Theis
发明人： Michael Bock , Robert Baumann , Axel Franzke , Eckhard Stroefer , Gerhard Theis
IPC分类号： C07C263/04 , C07C29/12 , C07C29/128 , C07C68/06
CPC分类号： C07C263/04 , C07C29/12 , C07C29/128 , C07C68/065 , C07C2601/14 , C07C69/96 , C07C265/12 , C07C265/14 , C07C31/202
摘要： A process for coproducing di- and/or polyisocyanates and glycols, comprising process stages A, B, C and E for preparing glycols and process stages A, C, D, E, F and G for preparing di- and/or polyisocyanates,which comprises accomplishing the material coupling via the separation of the reaction mixture obtained in process stage A into process stages B and C, by in process stage A, reacting an aqueous alkylene oxide with carbon dioxide to give a reaction mixture comprising alkylene carbonate, hydrolyzing a portion of the alkylene carbonate-comprising reaction mixture obtained in process stage A to glycol in process stage B, dewatering the remaining alkylene carbonate-comprising stream of the reaction mixture from process stage A in process stage C, in process stage D, synthesizing amine by hydrogenating an aromatic nitro compound or a nitrile, in process stage E, transesterifying the dewatered alkylene carbonate-comprising mixture from process stage C with a monohydroxy alcohol to give the corresponding dialkyl carbonate, obtaining glycol as a coproduct, in process stage F, reacting the dialkyl carbonate-comprising reaction mixture obtained in process stage E with the amine obtained in process stage D to a mixture comprising the corresponding mono-, di- and/or polycarbamate, which in process stage G is cleaved to obtain the corresponding di- and/or polyisocyanate.
摘要翻译：用于共混生产二 - 和/或多异氰酸酯和二醇的方法，包括制备二元醇和工艺阶段A，C，D，E，F和G的制备二 - 和/或多异氰酸酯的工艺阶段A，B，C和E，包括通过在工艺阶段A中将经处理阶段A获得的反应混合物分离成工艺阶段B和C来实现材料偶联，使环氧烷水溶液与二氧化碳反应，得到包含碳酸亚烷基酯的反应混合物，水解部分在工艺阶段B中获得的含碳酸亚烷基酯的反应混合物在工艺阶段B中与二醇的混合物，在工艺阶段D中将来自反应混合物的剩余的含有碳酸亚烃的物流从工艺阶段C脱水，通过氢化合成胺芳香族硝基化合物或腈，在工艺阶段E中，将来自工艺阶段C的脱水的含碳酸亚烷基酯混合物与单羟基醇酯交换，得到相应的碳酸二烷基酯，在工艺阶段F中获得二醇作为副产物，将在工艺阶段E中获得的含碳酸二烷基酯的反应混合物与在工艺阶段D中获得的胺反应到包含相应的单 - ，二 - 和/ 或聚氨酯，其在工艺阶段G被切割以获得相应的二 - 和/或多异氰酸酯。

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